Synthesis, crystal structure, and spectral analysis of antimony thiourea tetra chloride
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Date
2010
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Abstract
The synthesis of antimony thiourea tetra chloride (ATTC) single crystals by solution technique at room temperature is reported. The complex crystallizes in the orthorhombic space group Pnma with four formula units ofSb[CS(NH <inf>2</inf>)<inf>2</inf>]<inf>2</inf>Cl<inf>3</inf>·Cl in the unit cell. The structure has been solved by direct methods and refined to a final-R value of 0.0393. The synthesized crystals are characterized by FT-IR, UV-visible and TGA-DTA techniques. Copyright © Taylor & Francis Group, LLC.
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Keywords
antimony complex, crystal structure, synthesis, thermogravimetric
Citation
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2010, 40, 10, pp. 812-820