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Item Workability Study on Austempered AISI 1018(Institute of Physics Publishing helen.craven@iop.org, 2018) Nagendhra, S.; Rami Reddy, A.S.; Preetham Kumar, G.V.Workability of a material is a complex technological concept that is related to both material and process characteristics. Austempering is a heat treatment process that is applied to ferrous metals, mostly steel and ductile iron. The present work was carried out to study the workability and the properties of AISI 1018 steel in austempering and annealing condition and then comparing with each other. Workability testing was carried out using collar type specimen by compressing it till the crack. Workability diagrams have been plotted as a function of axial and hoop strains at failure. The result shows that, the austempering process increases the tensile strength and hardness as well as the workability. Thus the austempering process has an effect on strength and hardness. © Published under licence by IOP Publishing Ltd.Item Abstract Studies have been conducted on the effect of overstressing in rotary bending fatigue on the fatigue properties of an annealed and austempered ductile iron containing 1.5 Ni–0.3 Mo. For various R ratios S–N curves were determined and the fatigue limit estimated. It was found that the fatigue limit was a function of the level of overstressing and cycle ratio. In the case of austempered samples a beneficial effect of overstressing was observed at a certain level of overstressing. This was related to the work hardening behaviour of the austenite phase. In annealed samples, a reduction in the fatigue limit was observed at all levels of overstressing. Copyright © 1995, Wiley Blackwell. All rights reserved(EFFECT OF OVERSTRESSING ON FATIGUE BEHAVIOUR OF AUSTEMPERED DUCTILE IRON) Prasad Rao, P.; Padmaprabha1995Item Local stress and strain variations in the deformation zone can be ascertained by measuring hardness. Hardness is correlated with strain and stress. The expressions discussed later are useful in determining the local variations in stress and strain from hardness measurement. It is a simple method compared to visioplasticity. One can estimate the forces required for a forming process. It helps in the choice of equipment, design of tooling and selection of lubricant for the particular process.(Indian Academy of Sciences, Hardness-stress-strain correlation in aluminium - A simpler alternative to visioplasticity in metal forming) Dharmaveera, N.; Srinivasan, K.1996Item Studies on the photoconductivity of vacuum deposited ZnTe thin films(2010) Rao, K.G.; Bangera, K.V.; Shivakumar, G.K.The present paper reports the analysis of photoconductivity of vacuum deposited zinc telluride (ZnTe) thin films as a function of substrate temperature and post-deposition annealing. Detailed analyses were first carried out to understand the effect of substrate temperature and annealing on the structure, composition, optical and electrical properties of the films. The films deposited at elevated substrate temperatures showed faster and improved photoresponse. Post-deposition annealing was found to further enhance the photoresponse of the films. Attempts have been made to explain the improvement in the photoresponse on the basis of structural and compositional changes, taking place in the films, due to the substrate temperature and annealing. © 2010 Elsevier Ltd. All rights reserved.Item Effect of annealing on the structural and nonlinear optical properties of ZnO thin films under cw regime(2013) Nagaraja, K.K.; Pramodini, S.; Poornesh, P.; Nagaraja, H.S.We report on the studies of the effects of annealing on the structural and third-order nonlinear optical properties of ZnO thin films deposited on quartz substrates by the RF magnetron sputtering technique. The films were annealed in the temperature range 400-1000 °C. The third-order nonlinear optical studies were carried out using the z-scan technique under continuous wave (cw) He-Ne laser irradiation at 633 nm wavelength. The effects of annealing on the structural properties were examined using x-ray diffraction and atomic force microscopy (AFM). The (0 0 2) preferred orientation increased with increase in annealing temperature up to 800 °C. The crystalline phases of SiO2 were observed at higher annealing temperatures. The appearance of an extraneous phase was confirmed by AFM images and optical transmittance spectra. The samples exhibited nonlinear absorption and nonlinear refraction under the experimental conditions. The negative sign of the nonlinear refractive index n2 indicated that the films exhibit self-defocusing property due to thermal nonlinearity. The nonlinear refractive index n2, the nonlinear absorption coefficient ?eff and the third-order optical susceptibility ?(3) were found to be of the highest orders. The estimated value of third-order optical susceptibility ?(3) was of the order of 10-3 esu. Multiple diffraction rings were observed when the samples were exposed to the laser beam. The appearance of rings was due to the refractive index change and thermal lensing. With increase in laser intensity, the variations of the self-diffraction ring patterns were studied experimentally. The films also exhibited strong optical limiting properties under cw laser excitation, and reverse saturable absorption was the dominant process leading to the observed nonlinear behaviour. © 2013 IOP Publishing Ltd.Item Influence of substrate temperature and post deposition annealing on the properties of vacuum deposited ZnSe thin films(2013) Rao, K.; Bangera, K.V.; Shivakumar, G.K.The effects of substrate temperature and post deposition annealing on the structural, optical and electrical properties of vacuum deposited ZnSe thin films are presented here. The chemical composition of the films varied drastically with substrate temperature which in turn caused changes in various properties of the films. The grain size of the films increased with substrate temperature and also after annealing. The electrical properties of the films were found to be varying as a function of chemical composition and grain size. © 2012 Elsevier Ltd.Item Effect of annealing on the properties of Bi doped ZnO thin films grown by spray pyrolysis technique(Academic Press, 2014) Sadananda Kumar, N.; Bangera, K.V.; Shivakumar, G.K.The effect of annealing temperature on the structural, optical and electrical properties of transparent and conducting Bi doped ZnO (BZO) films deposited on glass substrate by spray pyrolysis technique was investigated. The BZO thin films were annealed in the temperature range from 450 °C to 550°C for 4 h in air atmosphere. The grain size of the BZO films increased with increasing annealing temperature. The annealed BZO films were electrically stable and there was a drastic change in the electrical conductivity after annealing. The films annealed at 500°C showed better conductivity and optical transmittance. © 2014 Elsevier Ltd. All rights reserved.Item Effect of annealing on the properties of zinc oxide nanofiber thin films grown by spray pyrolysis technique(Springer Nature, 2014) Sadananda Kumar, N.; Bangera, K.V.; Shivakumar, G.K.Zinc oxide nanofiber thin films have been deposited on glass substrate by spray pyrolysis technique. The X-ray diffraction studies revealed that the films are polycrystalline with the hexagonal structure and a preferred orientation along (002) direction for films annealed for 1 h at 450 °C. Further increase in annealing time changes the preferred orientation to (100) direction. The scanning electron microscopic analysis showed the formation of ZnO nanofiber with an average diameter of approximately 800 nm for annealed films. The compositional analysis of nanofiber ZnO thin films were studied by time of flight secondary ion mass spectroscopy, which indicated oxygen deficiency in the films. The optical properties of annealed films have shown a variation in the band gap between 3.29 and 3.20 eV. The electrical conductivity of the as grown and annealed films showed an increase in the conductivity by two orders of magnitude with increase in annealing duration. © 2013, The Author(s).Item Influence of annealing on the linear and nonlinear optical properties of Mn doped ZnO thin films examined by z-scan technique in CW regime(Elsevier B.V., 2016) Nagaraja, K.K.; Pramodini, S.; Poornesh, P.; Rao, A.; Nagaraja, H.S.We present the studies on the influence of annealing on the third-order nonlinear optical properties of RF magnetron sputtered manganese doped zinc oxide (MZO) thin films with different doping concentration. It is revealed that the incorporation of Mn into ZnO and annealing lead to prominent changes in the third order nonlinearity. Nonlinear optical measurements were carried out by employing the z-scan technique using a continuous wave (CW) He-Ne laser of 633 nm. The z-scan results reveal that the films exhibit self-defocusing thermal nonlinearity. The third-order nonlinear optical susceptibility ?(3) was found to be of the order of 10-3 esu and 10-2 esu for annealed MZO thin films at 200 °C and 400 °C respectively. The dependence of grain size on the observed nonlinearity was revealed by atomic force microscopy analysis. Optical limiting studies were carried out for a range of input power levels and an optical limiting of about ?8 mW was observed indicating the possible application for photonic devices. © 2016 Elsevier B.V. All rights reserved.Item The effect of annealing temperature on the structural, morphological, mechanical and surface properties of intermetallic NiTi alloy thin films(Elsevier B.V., 2016) Reddy, B.N.K.; Udayashankar, N.K.In this work, we report our studies on intermetallic NiTi thin films grown on silicon (1 0 0) substrates by glancing angle DC-magnetron sputtering technique using separate sputter targets Ni and Ti. The as prepared intermetallic NiTi thin films were vacuum annealed for one hour at four different temperatures, i.e. 350, 450, 550 and 650 °C. The crystallization and surface morphology were studied using X-ray diffraction technique (XRD), Field Emission Scanning Electron Microscopy (FESEM) and Atomic Force Microscopy (AFM). It was observed that the annealing temperatures had a significant influence on structural, morphological, mechanical and surface properties of intermetallic NiTi thin films. XRD studies revealed that the degree of crystallization increased with the increase in annealing temperature. The surface mean height (Ra), root mean square (RMS) and maximum peak to valley height (P-V) values have been obtained by AFM characterization. Nanoindentation tests on annealed intermetallic NiTi thin films were performed at room temperature. The hardness and elastic moduli increased from 8.32 to 10.24 GPa and from 154.60 to 164.49 GPa, respectively, with respect to the increase in annealing temperature. X-ray photo-electron spectroscopy (XPS) was used to study the composition and surface chemistry of the annealed films. From HR-XPS investigations, it was observed that intermetallic NiTi thin films had higher affinity to form Titanium dioxide (TiO2) layer on the film surface leaving a Nickel enriched matrix immediately behind the metal oxide layer. © 2016 Elsevier B.V.