Faculty Publications
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Item Joining of Inconel-625 alloy through microwave hybrid heating and its characterization(Elsevier Ltd, 2015) Badiger, R.I.; Narendranath, S.; Srinath, M.S.Joining of bulk metals using microwave energy is being explored as a new processing method in the era of high technology applications. The present work investigates the results of on-going project in which joining of Inconel-625 alloy has been effectively carried out through microwave hybrid heating. Characterization of the microwave developed joints is done through SEM, XRD, UTM and Vicker's microhardness tester. The microstructural analysis through scanning electron microscope exhibits a fully fused weld interface free from interfacial cracks. XRD study reveals the formation of carbides of Ni, Cr and Mo in the joint interface. The average Vicker's microhardness in the joint region observed was 360 ± 20 Hv. Assessment of tensile strength shows an ultimate tensile strength of 328 MPa with 9.04% elongation. Further the fractured joints are subjected to fractography study which possibly reveals a mixed mode fracture. © 2015 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.Item Microstructure and mechanical properties of Inconel-625 welded joint developed through microwave hybrid heating(SAGE Publications Ltd info@sagepub.co.uk, 2018) Badiger, R.I.; Narendranath, S.; Srinath, M.S.Application of microwave energy for processing of bulk metals is effectively utilized to join Inconel-625 plates through hybrid heating technique using Inconel-625 powder as an interface filler material. Post welding characterization of microwave developed joints through X-ray diffraction shows the development of carbides of niobium and chromium as well as intermetallic phases along with the primary ?-phase face-centered cubic matrix. Microstructural examination reveals the formation of Laves phase along the grain boundaries in the fusion zone. Microwave-induced joints exhibit average microhardness of 245 ± 20 HV and 0.7% porosity in the fusion zone. Average ultimate tensile strength and flexural strength of the developed joints were estimated at 375 and 377 MPa respectively. Average impact toughness of microwave-induced joints is observed to be 18 J. © IMechE 2017.Item Optimization of Process Parameters by Taguchi Grey Relational Analysis in Joining Inconel-625 Through Microwave Hybrid Heating(Springer New York LLC barbara.b.bertram@gsk.com, 2019) Badiger, R.I.; Narendranath, S.; Srinath, M.S.The quality of welded joints developed using microwave hybrid heating (MHH) technique is largely influenced by properties of the constituents employed in the process. This article investigates the influence of process parameters on tensile strength and flexural strength of Inconel-625 plates welded through MHH. Experiments were planned according to Taguchi L 16 orthogonal array by considering three factors: separator, susceptor and filler powder particle size. Ultimate tensile strength and flexural strength of the specimens welded at 600 and 900 W were chosen as response characteristics. Application of Taguchi-based GRA has been effectively used to optimize multi-performance characteristics of the process. ANOVA results indicate that size of interface filler powder is the most significant factor in determining the joint strength followed by separator and susceptor. Further to corroborate the optimal parameter setting for maximum strength values, metallurgical characterization of the specimens is carried out through XRD and SEM. Specimens processed at 600 W exhibited superior properties compared to their counterparts developed at 900 W. © 2018, Springer Science+Business Media, LLC, part of Springer Nature and ASM International.Item Role of ZSM5 catalyst and char susceptor on the synthesis of chemicals and hydrocarbons from microwave-assisted in-situ catalytic co-pyrolysis of algae and plastic wastes(Elsevier Ltd, 2022) Suriapparao, D.V.; Tanneru, T.; Rajasekhar Reddy, B.R.; Yerrayya, A.; Bhasuru, B.A.; Pandian, P.; Prakash, S.R.; Sankar Rao, C.; Sridevi, V.; Desinghu, J.The synergetic effect between algae biomass in co-pyrolysis with synthetic plastics (polypropylene (PP), polyethylene (PE), and expanded polystyrene (EPS)) was investigated in this work. Individual feedstock pyrolysis and co-pyrolysis of algae with PP, PE, and EPS were conducted at a constant supply of microwave energy (420 J/s). Pyrolysis char was used as a susceptor in all the experiments. The average heating rate was varied in the range of ∼50–60 °C/min for achieving the final pyrolysis temperature of 600 °C. In catalytic co-pyrolysis, the ZSM-5 catalyst was used for upgrading the physicochemical properties of pyrolysis oil. The use of catalyst promoted the excessive cracking of biomass in co-pyrolysis, leading to higher gas and coke residue comparatively. The viscosity, density, and flash point of oil obtained in catalytic co-pyrolysis were significantly reduced. While the oil obtained from individual pyrolysis of algae is rich in phenolic derivatives, and that of PP, PE has aliphatic hydrocarbons, and EPS has monoaromatic hydrocarbons as major compounds. The synergistic role of plastic and biomass in co-pyrolysis was observed in the formation of products and oil composition. The bio-oil from catalytic co-pyrolysis is composed of aliphatic oxygenates, aliphatic hydrocarbons, cyclic aliphatic hydrocarbons, and phenolics. The chemicals and hydrocarbons present in the oil have a carbon number in the range of C6 to C30. An increase in carbon and hydrogen elemental composition was observed in bio-oil obtained from co-pyrolysis. © 2021 Elsevier LtdItem Understanding of synergy in non-isothermal microwave-assisted in-situ catalytic co-pyrolysis of rice husk and polystyrene waste mixtures(Elsevier Ltd, 2022) Sridevi, V.; Suriapparao, D.V.; Tukarambai, M.; Terapalli, A.; Ramesh, R.; Sankar Rao, C.S.; Gautam, R.; Moorthy, J.V.; Suresh Kumar, C.Rice husk (RH) and polystyrene (PS) wastes were converted into value-added products using microwave-assisted catalytic co-pyrolysis. The graphite susceptor (10 g) along with KOH catalyst (5 g) was mixed with the feedstock to understand the products and energy consumption. RH promoted the char yield (20–34 wt%) and gaseous yields (16–25 wt%) whereas PS enhanced the oil yield (23–70 wt%). Co-pyrolysis synergy induced an increase in gaseous yields (14–53 wt%) due to excessive cracking. The specific microwave energy consumption dramatically decreased in co-pyrolysis (5–22 kJ/g) compared to pyrolysis (56–102 kJ/g). The pyrolysis index increased (17–445) with the increase in feedstock quantity (5–50 g). The obtained oil was composed of monoaromatics (74%) and polyaromatics (18%). The char was rich in carbon content (79.5 wt%) and the gases were composed of CO (24%), H2 (12%), and CH4 (22%). © 2022 Elsevier LtdItem Effect of dry torrefaction pretreatment of the microwave-assisted catalytic pyrolysis of biomass using the machine learning approach(Elsevier Ltd, 2022) Ramesh, R.; Suriapparao, D.V.; Sankar Rao, C.S.; Sridevi, V.; Kumar, A.This study employs the Leave-One-Out cross-validation approach to build a machine-learning model using polynomial regression to predict pyro product yield through microwave-assisted pyrolysis of sawdust over KOH catalyst and graphite powder a susceptor. The determination of coefficient (R2) validates the developed models. All the developed models achieved a high prediction accuracy with R2 > 0.93, which signifies that the experimental values are in good agreement with the predicted one. The dependence of the catalyst loading and pretreatment temperature on dominating process parameters such as heating rate, pyrolysis temperature, susceptor thermal energy, and pyro products, namely bio-oil, biochar, and biogas, are explored. The yield of biochar is reduced; however, bio-oil and biogas are enhanced as the catalyst loading increased. On the other hand, increasing the temperature of pretreated sawdust decreased bio-oil and biogas yields while increasing biochar yields. Further, microwave conversion efficiency, and susceptor thermal energy increased with increased catalyst quantity and pretreatment temperatures of sawdust. It was observed that the average heating rate was increased by increasing the catalyst quantity while maintaining the same pyrolysis time until pretreatment temperatures of 150 °C were reached, after which the heating rate dropped due to the continuous microwave energy input to the system. © 2022 Elsevier LtdItem Microwave-assisted In-situ catalytic co-pyrolysis of polypropylene and polystyrene mixtures: Response surface methodology analysis using machine learning(Elsevier B.V., 2023) Kamireddi, D.; Terapalli, A.; Sridevi, V.; Tukaram Bai, M.T.; Surya, D.V.; Sankar Rao, C.S.; Jeeru, L.R.Polypropylene (PP) and Polystyrene (PS) are the major plastic fractions found in mixed plastic waste. Hence, the current study was focused to convert PP and PS into useful products via microwave-assisted pyrolysis (MAP). In addition, the understanding of feedstock conversion, product yields, and energy requirements in pyrolysis, co-pyrolysis, and catalytic co-pyrolysis was investigated. Experiments were conducted at a constant microwave power of 450 W till the reaction temperature reached up to 600 °C. When PS pyrolyzed, a heating rate of 56 °C/min resulted in 80 wt% of oil yield. Whereas PP pyrolysis produced 42 wt% of oil at a heating rate of 76 °C/min. In the PP: PS co-pyrolysis, the heating rate was decreased to 52 °C/min by yielding 51 wt% of oil. In catalytic co-pyrolysis of PP: PS with KOH resulted in variation in product yields and heating rate. An increase in PS quantity at a constant mass of PP resulted in the enhancement of oil yields from 58 to 84 wt% and a decrease in gas yields. The specific microwave power in the catalytic co-pyrolysis (7–18 W/g) is lower compared to the non-catalytic case (22–30 W/g). Whereas, the pyrolysis time in non-catalytic pyrolysis (7–11 min) is lower compared to catalytic co-pyrolysis (14–37 min). The addition of a catalyst resulted in a decrease (23–50%) in microwave conversion efficiency than that of the non-catalytic case (60–85%). The difference in predicted and actual result analysis proved co-pyrolysis synergy in product formation and energy consumption. © 2023 Elsevier B.V.Item Characterization of Inconel 625-SS 304 Weldments Developed by Selective Microwave Hybrid Joining Technique for Promising Applications(Springer, 2024) Kamble, D.L.; Sahu, R.K.; Narendranath, S.Production of dissimilar weldments using microwave hybrid heating is currently gaining immense impetus in the field of advanced welding. This is because such heat source could provide benefits like cost-effectiveness, rapid, volumetric, uniform and selective heating, and efficient throughput which would be significant to various industries. Till-date researchers have carried out joining of dissimilar general purpose engineering materials using microwave hybrid heat source. But attention has not been paid on the joining and characterization of dissimilar exotic-general purpose materials using the aforementioned heat source and the promising applications of the weldments. Therefore, the present article is focused on the joining of dissimilar materials- Inconel 625 and SS 304 alloys using selective microwave hybrid joining (SMHJ) technique. In SMHJ, nickel-based powder is used as a filler material, Silicon carbide (SiC) block and SiC powder are used as susceptor to increase the initial temperature. The developed weldments through SMHJ are characterized using various physico-chemical diagnostic methods. The results reveal the average micro-hardness of joint was found to be 303 ± 17 HV owing to the presence of various carbides and nitrides phase like NbC, Cr23C6, Cr2Ni3, Ni8Nb, and Fe3Ni2 in the joint zone which is evident from XRD. The average UTS of the joints found to be 448.6 MPa with an elongation of 10.93% and flexural strength observed to be 435 MPa. Further, fractography study reveals, the joint regions have mixed mode of failure. The failure was attributed to the existence of secondary phases in the joint zone. © ASM International 2023.Item Effective electronic waste valorization via microwave-assisted pyrolysis: investigation of graphite susceptor and feedstock quantity on pyrolysis using experimental and polynomial regression techniques(Springer, 2024) Mistry, C.; Surya, D.V.; Ramesh, R.; Basak, T.; Kumar, P.S.; Sankar Rao, C.S.; Gautam, R.; Sridhar, P.; Choksi, H.; Remya, N.Waste printed circuit board (WPCB) was subjected to microwave-assisted pyrolysis (MAP) to investigate the energy and pyrolysis products. In MAP, pyrolysis experiments were conducted, and the effects of WPCB to graphite mass ratio on three-phase product yields and their compositions were analyzed. In addition, the role of the initial WPCB mass (10, 55, and 100 g) and susceptor loading (2, 22, and 38 g) on the quality of product yield was also evaluated. By using design of experiments, the effects of graphite susceptor addition and WPCB feedstock quantity was investigated. A significant liquid yield of 38.2 wt.% was achieved at 38 g of graphite and 100 g of WPCB. Several other operating parameters, including average heating rate, pyrolysis time, microwave energy consumption, specific microwave power used, and product yields, were optimized for the MAP of WPCB. Pyrolysis index (PI) was calculated at the blending of fixed quantity WPCB (100 g) and various graphite quantities in the following order: 2 g (21) > 20 g (20.4) > 38 g (19.5). The PI improved by increasing the WPCB quantity (10, 55, and 100 g) with a fixed quantity of graphite. This work proposes the product formation and new reaction pathways of the condensable compounds. GC–MS of the liquid fraction from the MAP of WPCBs without susceptor resulted in the generation of phenolic with 46.1% relative composition. The addition of graphite susceptor aided in the formation of phenolic and the relative composition of phenolics was found to be 83.6%. The area percent of phenol increased from 42.8% (without susceptor) to 78.6% (with susceptor). Without a susceptor, cyclopentadiene derivative was observed in a very high composition (~ 31 area %). © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2023.Item Hospital plastic waste valorization through microwave-assisted Pyrolysis: Experimental and modeling studies via machine learning(Elsevier Ltd, 2025) Ramesh, R.; Sankar Rao, C.; Surya, D.V.; Kumar, A.The COVID-19 pandemic generated a global upsurge in hospital plastic waste (HPW) as a consequence of the widespread utilization of personal protective equipment (PPE) composed of diverse polymer materials. The constant demand for PPE worldwide led to the accumulation of substantial volumes of high-polymer-based plastic waste. To tackle this challenge, researchers delved into the conversion of HPW into valuable chemicals through a process known as microwave-assisted pyrolysis (MAP). This method entails the transformation of HPW into high-quality char and liquid oil, which can serve as a source of fuel. In this study, our primary focus was to understand how the ratio of HPW (hospital plastic waste) to susceptor weight influenced the yields and characteristics of the resulting products in the context of the MAP process. To facilitate the experimental setup, a Central Composite Design (CCD) was employed. The impact of varying HPW weights and susceptor quantities on the production of value-added products was investigated. The analysis of condensed organic vapor decomposition revealed an increase in liquid yields (73.6 wt %, 76.6 wt %, 80.7 wt %) as the graphite content increased at a constant 30 g HPW. Conversely, gas yield decreased with higher susceptor and HPW quantity. Keeping the graphite constant at 4g, the gas yield declined (32.5 wt %, 30.7 wt %, and 24.7 wt %) as HPW increased. Additionally, gas yield exhibited a drop (32.5 wt % to 18.1 wt %) with an increase in both graphite and HPW. Furthermore, the residual yield decreased (from 1.7 wt % to 1.2 wt %) with a 30 g increase in HPW. In-depth analysis incorporated machine learning techniques to understand the behavior of response variables about susceptor and HPW quantities. The optimization of the MAP process for HPW encompassed various supplementary operational parameters, including susceptor thermal energy, average heating rate, microwave energy, specific microwave power, and product yields. Moreover, the residue generated from the MAP of HPW underwent characterization through X-ray diffraction (XRD), FTIR, and BET analysis. © 2025 Elsevier Ltd