Conference Papers

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    Thermal analysis and microstructure of ZA8 alloy solidifying against chills
    (Springer India sanjiv.goswami@springer.co.in, 2012) Ramesh, G.; Prabhu, K.N.
    Thermal analysis during solidification of ZA8 alloy against copper, hot die steel and stainless steel chills instrumented with thermocouples was carried out in the present work. The investigation showed that the chill material and coating had a significant effect on the cooling curve of the casting. When casting was solidified against chills, the liquidus and eutectic start temperature of the casting remained nearly the same whereas eutectoid transformation occurred at a higher temperature. Cooling rate curve of the casting solidified against coated chill indicated that formation of solid shell and subsequent re-melting in the case of high thermal conductivity coated chill whereas in lower thermal conductivity coated chill, the re-melting of solid shell was absent. It was found that chilling during solidification causes the morphology of dendrites transform to nearly rounded shape with refinement of lamellar eutectic.
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    Microstructure and mechanical properties new magnesium-zinc-gadolinium alloys
    (Minerals, Metals and Materials Society 184 Thorn Hill Road Warrendale PA 15086, 2016) Seetharaman, S.; Tekumalla, S.; Lalwani, B.; Patel, H.; Bau, N.Q.; Gupta, M.
    Magnesium based materials are effective for structural/component weight reduction in automotive applications. However, their real time applications are limited because of their inadequate mechanical properties, especially the absolute strength and creep resistance. In this regard, the formation of thermally stable ternary compounds is believed to positively influence the properties of Mg-Zn-RE alloys. In this study, new Mg alloys containing Zn and Gd (Mg-2.0Zn-0.5Gd and Mg-3.4Zn-0.8Gd, in at.%) were developed using disintegrated melt deposition technique followed by hot extrusion. The developed alloys were investigated for their microstructural and mechanical properties in hot-extruded conditions. The mechanical properties examined under indentation, tension and compression loads indicated improved mechanical performance due to Zn and Gd addition. The observed mechanical properties are presented using structure-property relationship. © © 2016 by The Minerals, Metals & Materials Society. All rights reserved.
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    Fabrication of stainless steel based composite by metal injection moulding
    (Elsevier Ltd, 2018) Veeresh Nayak, C.; Ramesh, M.R.; Desai, V.; Kumar Samanta, S.K.
    Metal injection moulding (MIM) is large scale manufacturing method, for creation of complex shapes and miniature parts by a combination of plastic injection moulding with the flexibility in sintering of metal particulates. In current investigation binder comprised of paraffin wax, polyethylene glycol, stearic acid and low-density polyethylene are developed for moulding of composite powders of SS316L+WC-CrC-Ni, and sintered at 1200°C under hydrogen purged atmosphere. Composites are characterised with respect to rheological, thermal properties and microstructure by scanning electron microscopy, microhardness and density. Properties of sintering temperature and heating rate on the above properties have been evaluated to obtain a defect-free composite. © 2017 Elsevier Ltd.
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    Microstructural characterization and mechanical properties of cast Al-15Zn-2Mg alloy subjected to severe plastic deformation
    (Elsevier Ltd, 2018) Manjunath, G.K.; Udaya Bhat, K.; Preetham Kumar, G.V.
    In the present work, Al-15Zn-2Mg alloy was processed by ECAP technique for grain refinement. The ECAP processing was conducted at 150 °C. Microstructural characterization was carried out in OM, SEM, TEM and XRD. To evaluate the mechanical properties, hardness measurement and tensile tests were conducted at room temperature. Microstructural characterization showed that, ECAP processing leads to decrease in the grain size of the alloy. Also, small amount of dislocations were also observed in the ECAP processed material. After ECAP processing, precipitates nucleation in the material was identified in the XRD analysis. The strength and the hardness values were increased after ECAP processing. After ECAP processing, microhardness of the material is increased from 173 Hv to 252 Hv and the UTS of the material is increased from 166 MPa to 362 MPa. After tensile testing, fracture surface of the cast material showed dendritic structure and the fracture surface of the ECAP processed material showed dimples. © 2018 Elsevier Ltd. All rights reserved.
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    Effect of FSW on microstructure and hardness of AA6061/SiC/fly ash MMCs
    (Elsevier Ltd, 2018) Patil, S.; Narendranath, S.; Dupadu, D.
    In this study 6 mm thick plates of aluminum matrix composites (AMCs) composed of AA6061/SiC (10 Wt. %) /fly ash (7.5 Wt. %) were butt welded using friction stir welding (FSW. Microstructural characterization of weld joints was conducted by using optical microscopy (OM) and scanning electron microscopy (SEM). The microstructure of the weld revealed the presence of four different zones like nugget zone (NZ), thermo mechanically affected zone (TMAZ), heat affected zone (HAZ) and base metal (BM). Nugget zone reveals homogenous distribution of fly ash and SiC particles. Rotating effect of FSW tool results in breaking of some array of grains present in the parent AMCs. Needle like phases present in the parent AMCs eliminated successfully by the incorporation of fly ash particles. Higher hardness is observed in the nugget zone compared to other zones. © 2018 Elsevier Ltd. All rights reserved.
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    Influence of Multi Axial Forging (MAF) on Microstructure and Mechanical Properties of Cu-Ti Alloy
    (Elsevier Ltd, 2018) Ramesh, S.; Shivananda Nayaka, H.S.; Gopi, K.R.
    Multi axial forging (MAF) is one among the severe plastic deformation (SPD) processes, where large strains are imposed into the component. In the present work, as-received Cu-1.5%Ti alloy was subjected to MAF for 2 and 4 cycles at room temperature. Microstructure showed grain refinement after 2 and 4 cycles. Average grain size obtained for MAF processed samples after 2 and 4 cycles are 120 μm and 40 μm, respectively compared to initial grain size of 800 μm. The Mechanical properties were analyzed for as-received and MAF processed samples. Tensile test showed increased ultimate tensile strength (493 MPa) for MAF 4-cycle sample compared to as-received (191 MPa) condition with accumulated strain of 2.18 for 4 cycles. Increase in hardness was observed for MAF processed sample of 143 Hv for 4-cycle compared to as-received sample of 67 Hv. © 2018 Elsevier Ltd.
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    Effect of equal channel angular pressing on the microstructure and mechanical properties of Al-10Zn-2Mg alloy
    (American Institute of Physics Inc. subs@aip.org, 2018) Manjunath, G.K.; Preetham Kumar, G.V.; Bhat, K.U.
    The current investigation is focused on evaluating the mechanical properties and the microstructure of cast Al-10Zn-2Mg alloy processed through equal channel angular pressing (ECAP). The ECAP processing was attempted at minimum possible processing temperature. Microstructural characterization was carried out in optical microscopy, scanning electron microscopy, transmission electron microscopy and X-ray diffraction analysis. Hardness measurement and tensile tests were employed to estimate the mechanical properties. Experimental results showed that, ECAP processing leads to noticeable grain refinement in the alloy. Reasonable amount of dislocations were observed in the ECAP processed material. After ECAP processing, precipitates nucleation in the material was detected in the XRD analysis. ECAP leads to considerable enhancement in the mechanical properties of the material. After ECAP processing, microhardness of the material is increased from 144 Hv to 216 Hv. Also, after ECAP processing the UTS of the material is increased from 140 MPa to 302 MPa. The increase in the mechanical properties of the alloy after ECAP processing is due to the dislocation strengthening and grain refinement strengthening. Finally, fracture surface morphology of the tensile test samples also studied. © 2018 Author(s).
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    Electrochemical Behaviour of ECAP-Processed AM Series Magnesium Alloy
    (Springer International Publishing, 2019) Gopi, K.R.; Shivananda Nayaka, H.
    Equal channel angular pressing (ECAP) is a technique for inducing high strain into the material to achieve ultrafine grain refinement. AM80 magnesium was processed by ECAP with processing route BC. ECAP-processed samples were tested for microstructural studies and electrochemical measurements. Potentiodynamic polarization test revealed decrease in corrosion current density due to uniform refined microstructure of the processed samples. Increment in charge transfer resistance (Rt) was observed for ECAPed samples with increase in capacitive arc diameters in Nyquist plots showing increased corrosion resistance in comparison with as-cast condition. The increment in corrosion resistance is because of grain refinement and uniform dispersal of intermetallic particles, which improved development of protective layer and bonding due to increased grain boundary density by ECAP process. © 2019, The Minerals, Metals & Materials Society.
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    Severe plastic deformation of Al-15Zn-2Mg alloy: Effect on wear properties
    (Trans Tech Publications Ltd ttp@transtec.ch, 2019) Manjunath, G.K.; Bhat, K.U.; Preetham Kumar, G.V.
    In the present work, Al-Zn-Mg alloy having highest zinc content was deformed by one of the severe plastic deformation (SPD) technique, equal channel angular pressing (ECAP) and effect of ECAP on the microstructure evolution and the wear properties were studied. ECAP was performed in a split die and the channels of the die are intersecting at an angle of 120°. ECAP was attempted at least possible temperature and the alloy was successfully ECAPed at 423 K. Below this temperature samples were failed in the first pass itself. After ECAP, significant drop in the grain size was reported. Also, ECAP leads to significant raise in the microhardness of the alloy. Predominantly, after ECAP, upsurge in the wear resistance of the alloy was noticed. To figure out the response of ECAP on the wear properties of the alloy; worn surfaces of the wear test samples were analyzed in SEM. © 2019 Trans Tech Publications Ltd, Switzerland.
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    Influence of retrogression and re-ageing heat treatment on the fatigue crack growth behavior of 7010 aluminum alloy
    (Elsevier B.V., 2019) Nandana, M.S.; Udaya Bhat, K.; Manjunatha, C.M.
    Aluminum alloys are widely used in aircraft structural components where light weight, high strength and good corrosion resistance are the primary requirements. These alloys are generally used in peak-aged (T6) condition in which they are susceptible for stress corrosion cracking. In the recent years, retrogression and re-ageing (RRA) treatment on aluminum alloy is carried out to enhance their corrosion resistance maintaining the ultimate tensile strength. The aim of this work was to study the influence of RRA treatment on the fatigue crack growth rate (FCGR) behavior. The 7010 aluminum alloy was heat treated to two different conditions i.e., T6 and RRA. The microstructures of these alloys were characterized by using TEM. Standard compact tension (CT) specimens were prepared and FCGR tests were carried out by using a 100 kN servo-hydraulic test machine as per ASTM E647-15e1. The constant amplitude FCGR tests were carried out at a stress ratio, R = 0.5 using sine wave loading pattern at 10 Hz. Crack length was monitored by following compliance technique. Microstructural studies show that RRA treated alloy contain fine and densely populated precipitates in the matrix along with coarse and discontinuous precipitates in the grain boundary. The fatigue crack growth rate was observed to reduce along with an increase in the threshold stress intensity factor range (ΔKth) for RRA treated alloy compared to the T6 alloy. The mechanisms for reduction in fatigue crack growth rate of RRA treated alloy is attributed to the microstructural modifications. The increased resistance is expected to enhance the damage tolerance capability of the alloy. © 2019 The Authors. Published by Elsevier B.V.