Sethi, M.Shenoy, U.S.Muthu, M.Bhat, D.K.2026-02-052020Frontiers of Materials Science, 2020, 14, 2, pp. 120-1322095025Xhttps://doi.org/10.1007/s11706-020-0499-3https://idr.nitk.ac.in/handle/123456789/23868We report a green and facile approach for the synthesis of NiFe<inf>2</inf>O<inf>4</inf> (NF) nanoparticles with good crystallinity. The prepared materials are studied by various techniques in order to know their phase structure, crystallinity, morphology and elemental state. The BET analysis revealed a high surface area of 80.0 m2·g?1 for NF possessing a high pore volume of 0.54 cm3·g?1, also contributing to the amelioration of the electrochemical performance. The NF sample is studied for its application in supercapacitors in an aqueous 2 mol·L?1 KOH electrolyte. Electrochemical properties are studied both in the three-electrode method and in a symmetrical supercapacitor cell. Results show a high specific capacitance of 478.0 F·g?1 from the CV curve at an applied scan rate of 5 mV·s?1 and 368.0 F·g?1 from the GCD analysis at a current density of 1 A·g?1 for the NF electrode. Further, the material exhibited an 88% retention of its specific capacitance after continuous 10000 cycles at a higher applied current density of 8 A·g?1. These encouraging properties of NF nanoparticles suggest the practical applicability in high-performance supercapacitors. © 2020, Higher Education Press.BET surface areananoparticleNiFe2O4solvothermal methodspecific capacitancesupercapacitor