4-(3-Chlorophenyl)-3-[(2,6-difluorobenzyl)sulfanyl]-5-(3,4, 5-trimethoxyphenyl)-4H-1,2,4-triazole
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Date
2011
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Abstract
In the title compound, C<inf>24</inf>H<inf>20</inf>ClF<inf>2</inf>N <inf>3</inf>O<inf>3</inf>S, the essentially planar triazole ring (r.m.s. deviation = 0.001 Å) forms dihedral angles of 22.35 (10), 68.17 (10) and 42.01 (10)°with the mean planes of the trimethoxyphenyl, chlorophenyl and difluorophenyl rings, respectively. A weak intramolecular C-H?? interaction occurs. In the crystal, molecules are linked into sheets lying parallel to the bc plane by C-H?O and C-H?N hydrogen bonds. The crystal packing also features weak C-H?? interactions.
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Keywords
data-to-parameter ratio = 21.6, mean ?(C-C) = 0.003 Å, R factor = 0.049, single-crystal X-ray study, T = 100 K, wR factor = 0.110
Citation
Acta Crystallographica Section E: Structure Reports Online, 2011, 67, 12, pp. o3422-o3423
