Control and dynamic optimization of middle vessel batch distillation column for the separation of ethanol/propanol/butanol mixture

Abstract

The middle vessel batch distillation column is an alternative to the regular batch distillation column. This configuration allows simultaneous separation of the light fraction (accumulated at top), heavy fraction (accumulated at bottom) and the intermediate fraction (accumulated in the middle vessel) in a single column. The objective of this article is to extensively analyse and discuss different control systems for the middle vessel batch distillation column (MVBDC) and dynamically optimize the column. Three control structures such as composition level cascade, composition temperature cascade, and temperature control system, have been tested and evaluated. Further, a dynamic optimization study has been performed on the control system providing the fastest separation. The optimizer is set to minimize the total energy consumed during the process. This resulted in a decrease in batch time from 26.8 to 25.2 h and a 13.5% decrease in overall energy usage. The presented dynamic optimization technique and control system design is useful for improving the performance of the MVBDC. © 2021 Institution of Chemical Engineers