Experimental investigation and optimization of one-part alkali-activated self-compacting concrete mixes

Abstract

Emphasizing the growing importance of sustainability, alkali-activated materials (AAMs) have emerged as a revolutionary alternative for cement in the construction sector. This study delves into the fresh, mechanical, and microstructural properties of One-Part Alkali-activated Self-compacting Concrete (OPASC) mixes. While mixtures of Ground Granulated Blast Furnace Slag (GGBFS) and Fly Ash (FA) were utilized as the precursors, powdered sodium metasilicate was employed to function as the activator. To streamline experimental design and reduce the economic demands of extensive testing, the Taguchi-Grey Relational Analysis (GRA) was utilized to identify optimal multi-response parameter levels. This method considered binder content (B) within a range of 700–800 kg/m³, water-to-binder (W/B) ratios between 0.38 and 0.42, and Na<inf>2</inf>O percentages from 5 % to 7 % as key input variables. Results indicated that the designed mixes recorded workability values satisfying the EFNARC guidelines, compressive strengths greater than 60 MPa, split-tensile strengths in the range of 3.5–4.6 MPa, and flexural strengths varying between 5.5 and 7.2 MPa. The mix parameters for the optimal mix, with the highest mean grey relational grade, were identified from the Taguchi-GRPA approach as B = 750 kg/m3, W/B = 0.4, and N = 6 %. Microstructural analysis revealed the formation of C/N-A-S-H type gels, which are instrumental in developing a compact matrix enhancing the mechanical properties. A good agreement between actual experimental results obtained for a different set of verification mixes with those predicted by regression-equations confirmed the potency of the Taguchi-GRA approach in optimizing the OPASC mix parameters. © 2024 The Authors