Faculty Publications
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Item Tribological performance of wire arc additive manufactured 347 austenitic stainless steel under unlubricated conditions at elevated temperatures(Elsevier Ltd, 2020) Duraisamy, R.; Subramaniyan, S.; Kannan, A.; Siva Shanmugam, N.; Sankaranarayanasamy, K.; Ramesh, M.R.Wire Arc Additive Manufacturing (WAAM) is an effective metal additive manufacturing process. In this research, 347 Austenitic Stainless Steel (ASS) walls were manufactured with ER347 consumable material. The microstructure of the WAAM processed 347 plate is entirely heterogeneous with changing grain morphology along the building direction and this is attributed to the complex cyclic thermal history during WAAM process. The microstructure is composed of columnar, cellular and equiaxed structures at various regions. The hardness decreased gradually from bottom to top along the building direction. The volume fraction of ferrite ranged from 0.5% to 4.2% at various regions and the presence of niobium carbide (NbC) was confirmed. The aim of the current work is to provide an outline of the WAAM processed 347 steel under dry sliding conditions at elevated temperatures. The elevated temperature wear mechanism has mild oxidative wear characteristic due to the formation of tribo-oxides on the wearing and sliding surfaces. However, the average coefficient of friction (COF) is lower for the WAAM processed 347 compared to 347 substrate. In all cases after initial running-in, the wear debris from the wearing and sliding surface forms mechanically mixed composite layer of tribo-oxides (Fe2O3, Fe3O4 and Al2O3). The worn surface at 200 °C presents different wear behavior compared to the samples at 400 °C and 600 °C. The wear at 200 °C is a typical adhesive wear, while the wear at 400?600 °C is mild oxidative wear. The increase in the percentage of Fe3O4 helps to heal the wear surface by forming a mechanically mixed composite layer. The characteristics of mild oxidative wear were elucidated. © 2020 The Society of Manufacturing EngineersItem Evolution of Microstructure and High-Temperature Tribological Performance of Self-Lubricating Nickel-Based Composite Tungsten Inert Gas Coatings(Springer, 2021) Gudala, S.; Ramesh, M.R.; Siva Shanmugam, S.S.The present study aims to assess the effect of Ag/BaF2 solid lubricant encapsulation in the nickel-based composite coatings for high-temperature tribological applications. The composite coatings (NiCrSiB/WC and NiCrSiB/WC/Ag/BaF2) have successfully been fabricated on the titanium 31 substrate by tungsten inert gas (TIG) cladding technique. The influence of the TIG processing current on the microstructure, microhardness, and fracture toughness was investigated. Mechanical characteristics of the coatings were further correlated with the microstructural morphologies. The coating fabricated at 70 A exhibited significantly higher hardness than other coatings. The tribological performances of the NiCrSiB/WC/Ag/BaF2 composite coatings were superior to those of the NiCrSiB/WC coatings at both low (200 °C) and high (600 °C) temperatures. The synergistic lubrication effect of the Ag/BaF2 solid lubricant combination provided lubrication at a wide range of temperatures. The addition of these solid lubricants in the nickel-based coating helped achieve the low coefficient of friction of 0.2 and lower wear rates. Particularly, oxide phases (such as NiO, TiO, Ni3Ti3O, and W3O) formed on the worn surface at 600 °C, and the lubricant phases (Ag, Ag2F, and Ba (TiO3)) provided excellent resistance to wear. © 2021, ASM International.Item Development of Self-lubricating Nickel Based Composite Clad using Microwave Heating in Improving Resistance to Wear at Elevated Temperatures(Korean Institute of Metals and Materials, 2022) Gudala, S.; Ramesh, M.R.; Srinath, M.S.This paper reports on a study of the high-temperature tribological performance of self-lubricating nickel-based composite clad. A porous and crack free clad containing matrix, reinforcement, and lubricant phase is developed on titanium 31 alloy using microwave irradiation. The microstructure of both NiCrSiB/WC and NiCrSiB/WC/Ag/BaF2 clad revealed very good metallurgical bonding with the substrate. The average microhardness of NiCrSiB/WC and NiCrSiB/WC/Ag/BaF2 clad is 710.58 HV and 650.25 HV respectively, is comparatively higher than the titanium 31 substrate (320 HV). The addition of Ag and BaF2 solid lubricants in the clad endowing clad to operate at a broad temperature range. Compared with the NiCrSiB/WC clad, solid lubricant encapsulate clad has shown very low friction coefficient and wear rates. The sliding wear characteristics of the clad were investigated by varying load and temperatures. The results revealed that oxide phases (NiO and Cr3O) and lubricant phases (Ag and BaWO4) formed at low and high temperatures are adequate to reduce delamination and material loss. Graphical abstract: [Figure not available: see fulltext.] © 2021, The Korean Institute of Metals and Materials.Item MICROSTRUCTURE AND TRIBOLOGICAL PERFORMANCE OF SELF-LUBRICATE CLADDING PRODUCED BY TUNGSTEN INERT GAS AND MICROWAVE HYBRID HEATING TECHNIQUES(World Scientific, 2022) Gudala, S.; Ramesh, M.R.; Siva Shanmugam, N.S.; Srinath, M.S.The wear reduction of moving components is highly desirable because wear limits their reliability and service life, mainly at elevated temperatures. This study produced thick clads of NiCrSiB/WC/MoS2/BaF2 by tungsten inert gas (TIG) and microwave hybrid heating (MHH) cladding techniques, which were compared for microstructural and high-temperature tribological properties. The clad samples were subjected to sliding contact using a pin on disc tribometer at 200°C, 400°C, 600°C under 20 and 40N load. The worn surface was analyzed using FESEM, XRD and three-dimensional (3D) profilometer. The experimental results revealed a significant effect of the TIG current and MHH exposure time on the microhardness value, which predominantly depends on the morphological characteristics. The average hardness of TIG clads was found to be 1.2 times higher than the MHH clad. Because of the MoS2 and BaF2 encapsulation, the continuous lubricant layer formation compensated for improved wear resistance with good reliability and longer service life. This work provides significant insights into the wear behavior of TIG and MHH clads at elevated temperatures and the prospective applications in turbines, where inadequate wear resistance of titanium alloy is the major concern for its use. © 2022 World Scientific Publishing Company.Item Elevated temperature tribological performance of non-equiatomic CoCrNiTiWx high entropy alloy coatings developed by mechanical alloying and high-velocity oxy-fuel spray(Elsevier B.V., 2024) Addepalli, S.N.; Joladarashi, S.; Ramesh, M.R.High entropy alloys (HEA) have applications in multiple fields owing to their exceptional mechanical and physical properties. In the current study, mechanical alloyed CoCrNiTiWx (x; a molar fraction, x = 0.5 and 1.5) HEA feedstock powders were deposited on maraging steel substrate using high-velocity oxy-fuel spray (HVOF). The phase evolution and the microstructure of the milled powders and as-sprayed coatings were analysed by X-ray diffraction (XRD) and scanning electron microscope (SEM). The tribological behaviour of CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings at elevated temperatures was studied extensively using a Pin-on-Disc tribometer. The CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings retained the BCC solid solution phases formed during the milling stage. However, additional oxide and intermetallic phases were formed owing to the in-flight oxidation and high temperatures experienced during the HVOF deposition. The deposited coatings exhibited a lamellar structure and good mechanical bonding with the substrate. The porosities of CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings were found to be 1.69 ± 0.32 % and 1.51 ± 0.37 % respectively.Consequently, the CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings displayed average microhardness values of 863 ± 52 HV0.3 and 1025 ± 39 HV0.3, respectively. Further, the wear rates of coatings exhibited a significant reduction at elevated temperatures, owing to the formation of TiO2, NiCr2O4 oxide tribofilms for CoCrNiTiW0.5, and CoCr2O4, NiWO4, WO3 oxides for CoCrNiTiW1.5. The specific wear rate of CoCrNiTiW0.5 HEA coating dropped by 73.6 % from 22.7 ± 2.6 × 10−6 mm3/N-m to 5.99 ± 1.9 × 10−6 mm3/N-m, while CoCrNiTiW1.5 dropped by 78.8 % from 11.86 ± 3.5 × 10−6 mm3/N-m to 2.51 ± 1.5 × 10−6 mm3/N-m, with a rise in the temperature from RT to 600 °C. Likewise, The frictional coefficients of CoCrNiTiW0.5 HEA dropped from 0.504 ± 0.015 to 0.397 ± 0.005, while CoCrNiTiW1.5 HEA dropped from 0.578 ± 0.025 to 0.471 ± 0.004, with a rise in temperature from RT to 600 °C. At room temperature, the wear mechanisms of the as-sprayed CoCrNiTiWx coatings were dominated by adhesive wear. However, at elevated temperatures, a shift towards oxidative wear was observed. © 2023 Elsevier B.V.Item Enhanced tribological performance of laser directed energy deposited Inconel 625 achieved through laser surface remelting(Elsevier B.V., 2024) Praharaj, A.K.; Chaurasia, J.K.; Gurugubelli, R.C.; Bontha, S.; Suvin, P.S.Inconel 625 (IN625) is an essential material for the manufacture of turbine blades and seals, aircraft ducting systems, engine components, and pressure valves. Laser Directed Energy Deposition (LDED) process has shown the potential to fabricate IN625 parts with superior mechanical properties and higher corrosion resistance when compared to those fabricated using conventional manufacturing techniques. However, the poor surface quality limits the practical application of LDED fabricated parts, especially in sectors that demand high tribological performance. To this end, this study focuses on improving the surface quality and tribological performance of LDED fabricated IN625 components using Laser Surface Remelting (LSR) as a postprocessing operation. The tribological performance was evaluated using a linear reciprocating ball-on-flat wear test setup. The surface roughness, remelting depth (RD), microstructure, hardness, and tribological performance (coefficient of friction and wear rate) of the remelted (RM) samples were compared with that of as-deposited (AD) samples. Microstructural characterization revealed that LSR resulted in grain refinement, reduced dendrite size, and primary dendritic arm spacing (PDAS). Laser scanning speed effects RD, dendrite size and PDAS via its effect on cooling rates. SEM + EDS analysis confirmed the presence of Laves phase in both AD and RM samples. XRD analysis of RM samples showed an increase in the amount of Laves phase. The refinement in microstructural features and the increased amount of Laves phase among the RM samples led to improvement in microhardness when compared to AD samples. Wear test results revealed a reduction in the coefficient of friction (COF) and wear rate after LSR with wear mechanism being either abrasive or delamination. Reduction in the size of dendrites and refinement in grain size are attributed to the enhanced tribological performance after LSR. © 2023 Elsevier B.V.Item Effect of Heat Treatment on Microstructure and Dry Sliding Wear Behavior of Laser Directed Energy Deposited Inconel 625(Springer, 2025) Praharaj, A.K.; Chaurasia, J.K.; Suvin, P.S.; Narayanan, J.A.; Paul, C.P.; Balla, V.K.; Chakrapani, S.K.; Bontha, S.Laser directed energy deposition (LDED) is a promising technology for manufacturing and repair of Inconel 625 (IN625) components used in critical sectors requiring enhanced tribological performance due to harsh operating environments. Hence, the current work focuses on the evaluation of the tribological performance of LDED-built IN625 with the implementation of different heat treatment methods, i.e., solution treatment (ST), direct aging (AG), and solution treatment + aging (ST + AG). A detailed microstructural analysis, hardness, and wear testing were performed for the as-deposited (AD) and heat-treated (HT) samples, and the results were compared. The analysis revealed coarser grains in the case of ST and ST + AG samples, whereas finer grains for AD and AG samples, indicating grain coarsening after solution treatment. Further, the brittle laves phase gets dissolved after ST, whereas the AG and ST + AG samples resulted in the precipitation of metal carbides and strengthening phases. The microhardness of the ST sample (193.2 HV) was lower compared to the AD (211.6 HV) sample, whereas the AG and ST + AG samples exhibited 25.6 and 9.3% higher hardness than the AD sample. Considering tribological performance, the AG sample illustrated a maximum reduction of 61.4% in the coefficient of friction (COF) and 36.5% in wear rate when compared to the AD sample. This could be attributed to the presence of finer grains and strengthening phases. © ASM International 2025.Item Tribological performance and 3-D surface characterisation of age-hardened Al2090-based ceramic composites(SAGE Publications Ltd, 2025) Sharath, B.N.; Mahesh, V.; Mahesh, V.; Kattimani, S.; Harursampath, D.This study investigates the synergistic influence of boron nitride (BN) tertiary ceramic additives and age-hardening treatment on the microhardness and wear resistance of Al2090-based hybrid composites, fabricated using the stir casting method. X-ray diffraction (XRD), scanning electron microscopy (SEM), and atomic force microscopy (AFM) studies are carried out to assess the phases present, microstructure, and surface properties, respectively. The metallurgical investigations confirm a relatively superior uniformity in the distribution of particles and the ageing of precipitation at 150°C, vis-à-vis the other temperatures explored in this study. The experimental examinations conducted as per ASTM (E8 and G99) standards revealed a significant improvement in both the hardness and the primary tribological properties, when micron-sized boron carbide, graphite, and boron nitride were used as reinforcements. Age-hardened samples, especially the hybrid composite HS-2 with 5 wt.% each of boron carbide, graphite, and boron nitride, demonstrated an enhanced hardness of 25.23% and lower surface roughness (44.3 nm) compared to Al2090 (AS), due to the presence of load-bearing ceramic reinforcements. Increasing the applied load led to higher wear rates and coefficients of friction for Al2090. However, heat-treated hybrid metal matrix composites (HMMCs) exhibited a contrary behaviour, suggesting enhanced durability. The investigation highlighted the better wear resistance of heat-treated and near-optimally reinforced HMMCs, indicating their potential candidature for wear-resistant aerospace applications. © IMechE 2025.Item Investigation on high-temperature tribological performance of laser directed energy deposited Inconel 625 for aerospace applications(Elsevier Ltd, 2025) Praharaj, A.K.; Bontha, S.; Balla, V.K.; Chakrapani, S.K.; Suvin, P.S.Laser directed energy deposition (LDED) is an emerging technique for fabricating superalloy based aero engine components. Hence, the current work investigates the tribological performance of LDED processed IN625 at room temperature (RT) and high temperature (HT) conditions of 850 °C to replicate the operating environment of aero engine components. The comparison with conventionally processed (CP) sample confirmed that as-deposited (AD) sample showed similar friction behavior to the CP sample but slightly improved wear performance. The COF and wear rate of AD sample reduced significantly at HT compared to RT due to the evolution of stable oxide layer. NiO, Fe2O3, and Cr2O3 were the major phases in oxide layer. The work indicates suitability of LDED to fabricate wear resistant surfaces. © 2024 Elsevier LtdItem Tribological characteristics of HVOF sprayed Fe-based composite coatings at elevated temperatures(SAGE Publications Ltd, 2025) T V, C.; Joladarashi, S.; Ramesh, M.R.This study evaluates the tribological performance of Fe-based composite coatings for aerospace and automotive applications, focusing on wear resistance at elevated temperatures. The coatings, comprising 15% WC-Co and Cr3C2 in an SS316L matrix, were deposited onto maraging steel via HVOF spraying. Microstructural analysis and adhesive strength testing confirmed strong particle bonding, with the coatings achieving a hardness of 711 ± 14?HV. Dry sliding wear behaviour was assessed using a ball-on-disc tribometer with alumina as the counterface under 10?N and 30?N loads at 25?°C, 300?°C, and 600?°C. Results indicated a decrease in the coefficient of friction and specific wear rate with increasing load and temperature. At 600?°C, wear rates were reduced by ?97.56% (10?N) and ?97.12% (30?N) than uncoated steel. Abrasive wear dominated at room temperature, while adhesive and oxidative wear mechanisms emerged at 600?°C, attributed to protective glaze layer formation. © The Author(s) 2025.