Faculty Publications
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Item Effect of aging and protective coating on the corrosion behavior of 6061 Al / SiCp composite in chloride solutions(Trans Tech Publications Ltd ttp@transtec.ch, 2011) Rajasekaran, S.; Udayashankar, N.K.; Nayak, J.Metal matrix composites considered especially for marine application are typically aluminum-based. Utilization of the composites in marine environments requires adequate corrosion resistance. In this work, the effect of aging and aluminum as resistive coating on the corrosion behavior of 6061 Al / SiC p composite in 1N and 3.5N NaCl solution in the temperature range of 30°C-50°C is studied by means of electrochemical techniques, scanning electron microscope (SEM) and weight loss measurements. Aging results in precipitation of intermetallics in the matrix, this in turn leads to galvanic and pitting corrosion. Pitting initiation and propagation as the main corrosion mechanism was driven by the aging kinetics which is ruled by the reduction in the retained vacancy concentration and at the same time by dislocation density due to the presence of SiCp. Sputtered aluminum coating on the composite effectively resists the pitting initiation and propagation and hence corrosion process. Also the intermetallic precipitates are unexposed to the Chloride solution by the presence of aluminum coating. Hence aluminum coating acts as corrosion resistive coating for the 6061 Al / SiCp aged composites. © (2011) Trans Tech Publications.Item Effect of SiC Reinforcement on Microstructure and Mechanical Properties of Aluminum Metal Matrix Composite(Institute of Physics Publishing helen.craven@iop.org, 2018) Ajagol, P.; Anjan, B.N.; Marigoudar, R.N.; Preetham Kumar, G.V.Aluminum reinforced with silicon carbide composites areextensively used in automobile industries and aerospaceowing to their favourable microstructure and improved mechanical behaviour with respect to pure aluminium but at a lower cost. Aluminium is remarkable for the low density and its ability to resist corrosion. The aim of present study istoevaluate the mechanical and microstructural properties of aluminum with silicon carbide (average particle size 30-45μm) reinforced in varying weight percentages (wt %) ranging from 0-15 wt% in a step of 5% each. Ultimate tensile strength, micro hardness and density of the fabricated composites were investigated as a function of varying SiC wt%. Microstructure analysis was carried out on casted composites using optical microscopy and scanning electron microscopy. From micrographs it is clear that fair distribution of reinforcing particles in the matrix and also observed some clustering and porosity in the cast material. Results revealed that, the addition of SiC reinforcement in the aluminum matrix increases the hardness and ultimate tensile strength gradually from 23 HV to 47 HV and 84 MPa to 130 MPa respectively. © Published under licence by IOP Publishing Ltd.Item Steam as coolant and lubricant in turning of metal matrix composites(2008) Shetty, R.; Pai B, R.B.; Kamath, V.; Rao, S.S.Green cutting has become focus of attention in ecological and environmental protection. Steam is cheap, pollution-free and eco-friendly, and then is a good and economical coolant and lubricant. Steam generator and steam feeding system were developed to generate and feed steam. Comparative experiments were carried out in cutting AA6061-15 vol.% SiC (25 ?m particle size), with cubic boron nitride (CBN) insert KB-90 grade under the conditions of compressed air, oil water emulsion, steam as coolant and lubricant, and dry cutting, respectively. The experimental results show that, with steam as coolant and lubricant, gradual reduction in the cutting force, friction coefficient, surface roughness and cutting temperature values were observed. Further, there was reduction in built up edge formation. It is proved that use of water steam as coolant and lubricant is environmentally friendly. © 2008 Zhejiang University and Springer-Verlag GmbH.Item Taguchi's technique in machining of metal matrix composites(Brazilian Society of Mechanical Sciences and Engineering, 2009) Shetty, R.; Pai B, R.B.; Rao, S.S.; Nayak, R.This paper presents the study on Taguchi's optimization methodology, which is applied to optimize cutting parameters in turning of age hardened Al6061-15% vol. SiC 25 ?m particle size metal matrix composites with Cubic boron nitride inserts (CBN) KB-90 grade using steam as cutting fluid. Analysis of variance (ANOVA) is used to study the effect of process parameters on the machining process. This procedure eliminates the need for repeated experiments, time and conserves the material by the conventional procedure. The turning parameters evaluated are speed, feed, depth of cut, nozzle diameter and steam pressure. A series of experiments are conducted using PSG A141 lathe (2.2 KW) to relate the cutting parameters on surface roughness, tool wear, cutting force, feed force, and thrust force. The measured results were collected and analyzed with the help of the commercial software package MINITAB15. As well, an orthogonal array, signal-to-noise ratio is employed to analyze the influence of these parameters. The method could be useful in predicting surface roughness, tool wear, cutting force, feed force and thrust force as a function of cutting parameters. From the analysis using Taguchi's method, results indicate that among the all-significant parameters, steam pressure is the most significant parameter. © 2009 by ABCM.Item Corrosion inhibition of 6061 Al-15 vol. pct. SiC(p) composite and its base alloy in a mixture of sulphuric acid and hydrochloric acid by 4-(N,N-dimethyl amino) benzaldehyde thiosemicarbazone(2011) Geetha, G.M.; Nayak, J.; Nityananda Shetty, A.N.The corrosion inhibition characteristics of 4-(N,N-dimethylamino) benzaldehyde thiosemicarbazone (DMABT) on the corrosion behavior of 6061 Al-15 vol. pct. SiC(p) composite and its base alloy were studied at different temperatures in acid mixture medium containing varying concentrations of hydrochloric acid and sulphuric acid using Tafel extrapolation technique and ac impedance spectroscopy (EIS). The effect of inhibitor concentration, temperature and concentration of the acid mixture media on the inhibitor action was investigated. It was found that inhibition efficiencies increase with the increase in inhibitor concentration, but decrease with the increase in temperature and with the increase in concentration of the acid media. Thermodynamic parameters for dissolution process were determined. The adsorption of DMABT on both the composite and base alloy was found to be through physisorption obeying Freundlich adsorption isotherm. © 2010 Elsevier B.V. All rights reserved.Item Abrasive wear behavior of granite-filled glass-epoxy composites by SiC particles using statistical analysis(2011) Basavarajappa, .S.; Manjunath Yadav, S.M.; Kumar, S.; Arun, K.V.; Narendranath, S.This experimental investigation deals with the evaluation of abrasive wear behavior of Glass Epoxy (G-E) composites on pin-ondisc test rig. A plan of experiments, based on the Taguchi Design of Experiments, was performed to acquire data in controlled way. An orthogonal array and the analysis of variance were employed to investigate the percentage of contribution of various process parameters like sliding speed, applied load, sliding distance and their interactions affecting the abrasive wear volume loss of composites. The correlations between the various factors affecting the abrasive wear behavior of composites were obtained by using multiple linear regression equations. The obtained results indicate that applied load and sliding distance were the wear factors that have the highest physical as well as statistical influence on the abrasive wear behavior of both filled and unfilled G-E composites. A good agreement between the predicted and actual wear resistance was observed within±12%. © Taylor & Francis Group, LLC.Item Hardness and electrochemical behavior of ceramic coatings on inconel(International Association of Physical Chemists, 2012) Sujaya, C.; Shashikala, H.D.; Umesh, G.; Hegde, A.Thin films of ceramic materials like alumina and silicon carbide are deposited on Inconel substrate by pulsed laser deposition technique using Q-switched Nd: YAG laser. Deposited films are characterized using UV-visible spectrophotometry and X-ray diffraction. Composite microhardness of ceramic coated Inconel system is measured using Knoop indenter and its film hardness is separated using a mathematical model based on area-law of mixture. It is then compared with values obtained using nanoindentation method. Film hardness of the ceramic coating is found to be high compared to the substrates. Corrosion behavior of substrates after ceramic coating is studied in 3.5% NaCl solution by potentiodynamic polarization and electrochemical impedance spectroscopy measurements. The Nyquist and the Bode plots obtained from the EIS data are fitted by appropriate equivalent circuits. The pore resistance, the charge transfer resistance, the coating capacitance and the double layer capacitance of the coatings are obtained from the equivalent circuit. Experimental results show an increase in corrosion resistance of Inconel after ceramic coating. Alumina coated Inconel showed higher corrosion resistance than silicon carbide coated Inconel. After the corrosion testing, the surface topography of the uncoated and the coated systems are examined by scanning electron microscopy. © 2012 by the authors; licensee IAPC, Zagreb, Croatia.Item Hardness and electrochemical behavior of ceramic coatings on CP titanium by pulsed laser deposition(2012) Sujaya, C.; Shashikala, H.D.Thin films of alumina and silicon carbide are deposited on titanium substrate by the pulsed laser deposition technique using Nd: YAG laser. Deposited films are characterized using x-ray diffraction, scanning electron microscopy, energy-dispersive x-ray spectroscopy, absorption spectroscopy and nanoindentation. Film hardness of the ceramic coating is found to be high compared to that of the substrates. Corrosion behavior of substrates after ceramic coating is studied in 3. 5% NaCl solution by potentiodynamic polarization and electrochemical impedance spectroscopy measurements. Experimental results show an increase in corrosion resistance of titanium after being coated with a ceramic material. © 2012 Allerton Press, Inc.Item Microstructural characterization and hardness evaluation of friction stir welded composite AA6061-4.5Cu-5SiC (Wt.%)(Defense Scientific Information and Documentation Centre, 2013) Shettigar, A.K.; Salian, G.; Herbert, M.A.; Rao, S.Recent developments in advanced materials research have led to the emergence of new materials having features like low density, high strength to weight ratio, excellent mechanical properties, heat and corrosion resistance. In friction stir welding (FSW), a non-consumable rotating welding tool is used to generate the frictional heat and plastic deformation of the material in the welding zone, which is in the solid state. The advantages of FSW as compared to the fusion welding are high joint strength, less defect weld, uniform distribution of grain structure in the weld zone and low power consumption. AA6061 with 4.5 % weight of copper and 5 % weight of SiC composite material has been prepared to conduct experiment and carry out characterization, evaluation of the mechanical properties. Micro-structural characterization of the weld zone is carried out by scanning electron microscope (SEM). Evaluation of hardness was also carried out across the weld zone. A successful method for FSW of AA6061-4.5(wt.%) Cu-5(wt.%) SiC has been developed. © 2013, DESIDOC.Item Corrosion inhibition of aluminum type 6061 Al-15 vol. pct. SiC(p) composite in 0.5-M sodium hydroxide solution by 4-amino-5-phenyl-4H-1,2,4-triazole-3-thiol(Emerald Group Publishing Ltd. Howard House Wagon Lane, Bingley BD16 1WA, 2014) Reena Kumari, P.D.; Nayak, J.; Nityananda Shetty, A.Purpose: The purpose of this paper is to report the studies on the corrosion inhibition property of 4-amino-5-phenyl-4H-1,2,4-triazole-3-thiol (APTT) for the corrosion of 6061 Al-15 vol. pct. SiC(p) composite. Design/methodology/approach: The corrosion behavior of 6061 Al-15 vol. pct. SiC(p) composite was studied at different temperatures in 0.5-M sodium hydroxide (NaOH) solution in the presence of APTT by potentiodynamic polarization (PDP) and electrochemical impedance spectroscopic techniques. The effect of inhibitor concentration and temperature on the inhibitor effect of APTT was studied. The surface morphology of the metal surface was investigated by scanning electron microscopy. The activation parameters for the corrosion of the composite and base alloy, as well as the thermodynamic parameters for the adsorption of APTT on the composite and alloy surfaces, were calculated. Findings: The inhibition efficiency of APTT increases with the increase in the concentration of the inhibitor and decreases with the increase in temperature. The adsorption of APTT on the composite was found to be through physisorption, obeying Langmuir's adsorption isotherm. APTT acts as a mixed inhibitor with predominant cathodic action on the composite. Practical implications: APTT can be used as an inhibitor for the corrosion of 6061 Al-15 vol. pct. SiC(p) composite in the NaOH medium. Originality/value: This paper provides information regarding the corrosion inhibition property of APTT on 6061 Al-15 vol. pct. SiC(p) composite. An attempt was made to explain the mechanism of the inhibition action by APTT. © Emerald Group Publishing Limited.