Faculty Publications
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Item Mixing and solid-liquid mass transfer characteristics in a three phase pulsed plate column with packed bed of solids in interplate spaces-a novel aerobic immobilized cell bioreactor(2011) Shetty K, V.S.; Srinikethan, G.Background: The pulsed plate column (PPC) with packed bed of solids in the interplate spaces finds use as a three phase aerobic bioreactor and is a potential heterogeneous catalytic reactor. Good knowledge of the extent of mixing in the liquid phase and solid-liquid mass transfer coefficient are essential for modeling, design and optimization of these columns. The present work aims at the study of liquid phase mixing and solid-liquid mass transfer characteristics in a three phase PPC. Results: Residence time distribution studies were performed. Dispersion number was found to increase with increase in liquid superficial velocities, frequency of pulsation, amplitude of pulsation and the vibrational velocities. Increase in frequency and amplitude of pulsation, and hence increase in vibrational velocity, resulted in increase of the solid-liquid mass transfer coefficient. Conclusions: The mixing behaviour in this contactor approximated a mixed flow behaviour. The three phase PPC was found to outperform many other kinds of three phase contactors in terms of solid liquid mass transfer characteristics. Empirical correlations developed can be used for the determination of solid-liquid mass transfer coefficients for three phase PPC and hence can facilitate the design, scale-up and modeling of these columns, when used as chemical or biochemical reactors. © 2011 Society of Chemical Industry.Item Primary Fragmentation Behavior of Indian Coals and Biomass during Chemical Looping Combustion(American Chemical Society service@acs.org, 2018) Pragadeesh, K.S.; Ruben Sudhakar, D.R.Devolatilization and fragmentation are important physical phenomena occurring during solid fuel chemical looping combustion (CLC). Primary fragmentation during devolatilization strongly affects the rate of fuel conversion, emissions, and fine particulates generation in a fuel reactor of a fluidized bed CLC unit, thus forming a critical design input. The present study focuses on investigating the primary fragmentation behavior of large coal and biomass (wood) particles during the devolatilization phase of CLC. Three types of coals (two Indian coals, one Indonesian coal) and one type of Casuarina wood of three sizes in the range of 8-25 mm, at different fuel reactor bed temperatures (800, 875, and 950 °C) are studied for primary fragmentation. Iron ore with 64% Fe is used as the oxygen carrier bed material, with steam as the fluidizing medium in the fuel reactor. The fragmentation behavior is expressed in terms of the number of fragments, fragmentation index, frequency of fragmentation, and particle size distribution of fragments at different residence times of coal during devolatilization in the fuel reactor. Under the conditions of study, the number of fragments increases with an increase in particle size and temperature, for all fuels studied. Also, it is found that the number of fragments increases with the decrease in compressive strength of both coal and biomass particles. The Indian coals are found to fragment in the earlier stages of devolatilization, while the Indonesian coal and the biomass particles begin to fragment in the later stages of devolatilization. The maximum fragmentation index is found with Indian coal - IC1, which has the highest fixed carbon content among the fuels studied, and the least value is observed in biomass. Different modes of fragmentation exhibited by each fuel type is discussed. Indian coals do not show any volumetric changes as such, whereas Indonesian coal indicates some degree of volumetric expansion. © 2018 American Chemical Society.Item Residence Time Distribution Studies in a Modified Rotating Packed Disc Contactor: Mathematical Modeling and Validation(De Gruyter Open Ltd, 2020) Kalnake, R.P.; Murthy, D.V.R.; Achar, A.; Raval, K.A modified rotating packed disc contactor (RPDC) with the maximum working volume of 65 liter is designed for biological waste water treatment. A hollow disc with radial vanes mounted on the disc was a modified design of this contactor. Stimulus-response experiments were conducted in the contactor to understand liquid mixing behavior under different operating conditions. The recycle stream was also used in the operation of the contactor. Experiments were conducted for different number of discs, rotational speeds and recycle ratios. The disc design and recycle ratio had marked influence on the mixing behavior. An increase in disc rotation and recycle ratio produced a well-mixed flow behavior. Moreover, the surface area available in the RPDC was about 4 times more than the surface area available in a standard rotating biological contactor (RBC) operating at similar conditions. A mathematical model was developed for the flow behavior under recycle and a good agreement was found between the model and experimental results. © 2020 Walter de Gruyter GmbH, Berlin/Boston 2020.Item Numerical investigation of engulfment flow at low Reynolds numbers in a T-shaped microchannel(American Institute of Physics Inc. claims@aip.org, 2020) Madana, V.S.T.; Ali, B.Microreactors play a major role in the intensification of industrial processes. The performance of microfluidic devices depends on the flow behavior and flow regimes present in such systems. In this work, single-phase flow behavior and associated flow regimes in a T-shaped microchannel are numerically analyzed using computational fluid dynamics (CFD). To predict the single-phase flow regimes, three dimensional transient CFD simulations are performed. The critical Reynolds number (Re) at which flow regime transition and onset of engulfment occur is identified (Recritical = 300). To achieve engulfment flow at lower Re, the inlet geometry of the microchannel is modified as a convergent (C)-divergent (D) section and its effect on engulfment flow is analyzed. When the C/D ratio is 9:1, the predicted pressure drop (?p) is found to be minimum (Recritical = 75, ?p = 5.4 kPa). The understanding of the engulfment flow regime is exploited through residence time distribution (RTD). The predicted RTD profiles indicate strong recirculation among vortices. The mixing index is calculated to quantify RTD, and it is found to be minimum when the C/D ratio is 9:1. The mixing performance is further verified by introducing buoyant particles in Lagrangian manner using discrete phase modeling. The predicted dynamics are qualitatively and quantitatively analyzed through Poincaré maps and Shannon's entropy for various convergent-divergent inlets to characterize mixing. Once again, the C/D ratio of 9:1 supports in enhancing mixing in the microchannel. Hence, the proposed micromixer based on geometric modifications at the inlet helps achieve the engulfment flow regime at low Re. © 2020 Author(s).Item Computational investigation of flow field, mixing and reaction in a T-shaped microchannel(Taylor and Francis Ltd., 2021) Madana, V.S.T.; Ali, A.A.Microfluidics plays an essential role in process intensification, carrying out reactions safely and enhancing mass and heat transfer coefficients. In this work, hydrodynamics, mixing and reaction in the microchannel are investigated numerically and experimentally. To predict the flow field, three dimensional transient CFD simulations are performed. The irreversibility induced by the flow is used to quantify the liquid circulation. To improve the flow field, the geometry of the microchannel is modified by placing obstacles. It is found that geometric modifications have a significant effect on the hydrodynamics and hence mixing and reaction. The axial and lateral mixing are analyzed for various obstacles using Residence Time Distribution (RTD). The mixing index is calculated to characterize lateral mixing and to find an optimum configuration that supports flow field and mixing. Further, the implications of these obstacles on a fast neutralization reaction in the microchannel are studied. © 2020 Taylor & Francis Group, LLC.Item Numerical Simulation to Predict the Effect of Process Parameters on Hardness during Martempering of AISI4140 Steel(Springer, 2021) Pranesh Rao, K.M.P.; Prabhu, K.N.Martempering is a widely practiced industrial heat treatment process to harden steel parts with minimum distortion. A numerical experiment to predict hardness distribution in AISI 4140 steel cylinders of various diameters during martempering is presented in this work. Apart from the diameter (D), the effect of other process variables such as heat transfer coefficient (h), bath temperature (Tb), and residence time (tr) was also studied. The relationship between hardness distribution and the aforementioned process variables was highly nonlinear. An artificial neural network (ANN) model with a single hidden layer and 30 hidden layer neurons was thus developed to predict the hardness distribution in martempered AISI 4140 steel cylinders. The increase in bath temperature, diameter, and residence time decreased the average hardness, and an increase in the heat transfer coefficient increased the average hardness of martempered AISI 4140 cylinders. The weights of the ANN model were used to calculate the relative importance of all input variables and they followed a decreasing order of Tb>D>tr>h. © 2021, ASM International.Item Experimental and computational investigation of solid suspension and gas dispersion in a stirred vessel(American Institute of Physics Inc., 2022) Ali, A.A.; Kumar, B.; Madana, V.S.T.Hydrodynamics and residence time distribution (RTD) of fluid elements are key parameters to characterize the performance of stirred vessel. They are governed by geometric and operating parameters of the stirred vessel (SV). In the present work, the performance of the stirred vessel is studied using computational fluid dynamics (CFD) with realizable k-ϵ turbulence model. The multiple reference frame and sliding mesh approach are used for impeller motion. The solid-liquid flow and associated solid suspension characteristics are predicted using the two-fluid model (Euler-Granular). The performance of the stirred vessel is characterized by analyzing predicted velocity magnitude, solid concentration (suspension quality), and solid sedimentation. This is compared with the stirred vessel with draft tube baffle configuration (three inner baffles and six outer baffles). The recirculatory flow in draft tube SV helps to achieve uniform suspension and less sedimentation. Further, CFD simulations are carried out in Lagrangian way to analyze chaotic mixing among fluid elements. This is qualitatively analyzed using Poincaré map and quantitatively evaluated using Shannon entropy. The extent of chaotic mixing in draft tube SV is found to be high. The performance of the stirred vessel is further investigated through stimulus-response tracer techniques (RTD) to detect design flaws such as bypass and dead zones. This is analyzed for a wide range of operating parameters and identified optimum conditions (flow rate, impeller speed) for the operation of SV. The four different outlet pipe locations are chosen in SV. The bypass and dead volume are analyzed accordingly, and an optimum outlet pipe location is found. To reduce the extent of non-ideal parameters, three different gas source locations are considered and gases are dispersed in the form of bubbles. The gas dispersion at optimum gas injection point is found to reduce non-ideal parameters and improve the design of stirred vessel. © 2022 Author(s).