Faculty Publications
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Item Joining of Inconel-625 alloy through microwave hybrid heating and its characterization(Elsevier Ltd, 2015) Badiger, R.I.; Narendranath, S.; Srinath, M.S.Joining of bulk metals using microwave energy is being explored as a new processing method in the era of high technology applications. The present work investigates the results of on-going project in which joining of Inconel-625 alloy has been effectively carried out through microwave hybrid heating. Characterization of the microwave developed joints is done through SEM, XRD, UTM and Vicker's microhardness tester. The microstructural analysis through scanning electron microscope exhibits a fully fused weld interface free from interfacial cracks. XRD study reveals the formation of carbides of Ni, Cr and Mo in the joint interface. The average Vicker's microhardness in the joint region observed was 360 ± 20 Hv. Assessment of tensile strength shows an ultimate tensile strength of 328 MPa with 9.04% elongation. Further the fractured joints are subjected to fractography study which possibly reveals a mixed mode fracture. © 2015 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.Item Evaluation of WEDM performance characteristics of Inconel 706 for turbine disk application(Elsevier Ltd, 2015) Sharma, P.; Dupadu, D.; Narendranath, S.Inconel 706 is a newly developed superalloy, which offers high mechanical strength alongwith easy fabricability thus making it suitable for turbine disk applications. Although Inconel 706 exhibits a substantial increase in stress rupture and tensile yield strength compared to other superalloys, its conventional machining yields poor surface finish and low dimensional accuracy of the machined components. Hence, wire electrical discharge machining (WEDM) of Inconel 706 has been performed and various performance attributes such as material removal rate (MRR), surface roughness (SR), recast surface, topography, microhardness, microstructural and metallurgical changes of the machined components have been evaluated. The experimental results revealed that servo voltage, pulse on time, and pulse off time greatly influence the MRR and SR. Due to high toughness of Inconel 706, no micro cracks were observed on the machined surface. Micro voids and micro globules are significantly reduced at low pulse on time and high servo voltage. But, there is a propensity of thick recast layer formation at high pulse on time and low servo voltage. EDAX analysis of recast surface exposed the existence of Cu and Zn which have migrated from the brass wire. The subsurface microhardness was changed to 80. ?m due to significant thermal degradation. © 2015 Elsevier Ltd.Item Effect of Wire Material on Productivity and Surface Integrity of WEDM-Processed Inconel 706 for Aircraft Application(Springer New York LLC barbara.b.bertram@gsk.com, 2016) Sharma, P.; Dupadu, D.; Narendranath, S.Inconel 706 is a recently developed superalloy for aircraft application, particularly in turbine disk which is among the most critical components in the gas turbine engines. Recently, wire electrical discharge machining (WEDM) attained success in machining of gas turbine components which require complex shape profiles with high precision. To achieve the feasibility in machining of these components, the research work has been conducted on Inconel 706 superalloy using WEDM process. And, the effect of different wire materials (i.e., hard brass wire, diffused wire, and zinc-coated wire) on WEDM performance characteristics such as cutting speed, surface topography, surface roughness, recast layer formation, residual stresses, and microstructural and metallurgical alterations have been investigated. Even though, zinc-coated wire exhibits improved productivity, hard brass wire was found to be beneficial in terms of improved surface quality of the machined parts. Additionally, lower tensile residual stresses were obtained with hard brass wire. However, diffused wire has a moderate effect on productivity and surface quality. Under high discharge energy, higher elemental changes were observed and also the white layer was detected. © 2016, ASM International.Item Effect of wire diameter on surface integrity of wire electrical discharge machined Inconel 706 for gas turbine application(Elsevier Ltd, 2016) Sharma, P.; Dupadu, D.; Narendranath, S.Inconel 706 superalloy has established itself in the field of gas turbine industry because of its easy fabricability combined with high mechanical strength. Due to its high stress rupture and tensile yield strength, conventional machining of this superalloy exhibits poor surface and low dimensional accuracy of the machined components. It is well known that most of the gas turbine components include complex shaped profile with high precision and hence, wire electrical discharge machining (WEDM) of Inconel 706 has been performed to achieve the feasibility in manufacturing of complex shaped components for gas turbine application. In the current investigation, the effect of wire diameter on WEDM performance characteristics such as cutting speed, surface roughness, surface topography, recast layer formation, microhardness, microstructural and metallurgical changes have been evaluated. It was investigated that smaller diameter wire is advantageous over the larger diameter wire since it improves productivity as well as surface quality of the machined components under the same settings of control parameters. In addition, smaller diameter wire has shown comparatively lower recast layer thickness, minimum hardness alteration and shorter manufacturing time. The XRD result has confirmed the presence of residual stress within WED machined component. © 2016 The Society of Manufacturing EngineersItem Estimation of spatially dependent heat flux transients during quenching of inconel probe in molten salt bath(ASTM International, 2017) Pranesh Rao, K.M.; Prabhu, K.N.Several industrial heat treatment processes, such as martempering and austempering, require a quench bath to be maintained at a temperature ranging between 150°C–600°C. Molten salts, molten alkali, and hot oils are the preferred quenchants for these processes. Molten salts and molten alkali are preferred over hot oil because they possess properties like wide operating temperature range, excellent thermal stability, and tolerance for contaminants. In the present work, the performance of a molten potassium nitrate (KNO3) quench bath was analyzed with an Inconel probe that measured 60 mm in height and 12.5 mm in diameter. The probe was heated to 850°C and subsequently quenched in a bath maintained at 450°C. Cooling curves at different locations of the probe were recorded using the K-type thermocouples inserted into the probe. Spatially dependent transient heat flux at the metal/quenchant interface was estimated using inverse heat conduction technique. The existence of two stages of quenching—boiling stage and convection stage—was confirmed by analyzing the heat flux. The heat transfer coefficient was calculated based on heat flux obtained by the inverse method. The nonuniformity in heat transfer along the length of the probe was quantified by calculating the range of surface temperatures at each instance. The hardness distribution in an AISI 4140 steel was predicted using the temperature distribution in the Inconel probe and obtained using inverse method. Uneven distribution of hardness predicted in the probe was attributed to the nonuniform cooling of the probe during quenching. © © 2017 by ASTM International.Item Analysis and Optimization of WEDM Performance Characteristics of Inconel 706 for Aerospace Application(Springer Netherlands rbk@louisiana.edu, 2018) Sharma, P.; Dupadu, D.; Narendranath, S.Wire Electrical Discharge Machining (WEDM) has established itself for manufacturing of precise and complex shape components for aerospace application due to the high quality requirement of aerospace components such as normal residual stress, no cracks, no recast layer, no porosity; still there is a need to optimize the control parameter settings and evaluate the performance characteristics of the WEDM process. The experiments have been conducted on Inconel 706 which is a newly-developed superalloy specially for aircraft application. A hybrid approach has been used to optimize the material removal rate (MRR) as well as surface roughness (SR) and significant control parameters have been identified using analysis of variance (ANOVA). Microstructure analysis revealed the formation of microglobules, melted debris and microholes on the machined surface, but no microcrack was detected due to the high toughness of the alloy. Energy dispersive X-ray spectroscopy (EDAX) has been carried out to study the metallurgical changes in the WED machined surface. The topography analysis of the curved surface revealed the best surface quality of the machined component at low pulse on time and high pulse off time. A thick recast layer of 39.6 µm was observed at high pulse on time and low servo voltage. Microhardness of the machined surface was changed up to a depth of 70 µm due to cyclic thermal loading during the WEDM process. © 2017, Springer Science+Business Media Dordrecht.Item Microstructure and mechanical properties of Inconel-625 welded joint developed through microwave hybrid heating(SAGE Publications Ltd info@sagepub.co.uk, 2018) Badiger, R.I.; Narendranath, S.; Srinath, M.S.Application of microwave energy for processing of bulk metals is effectively utilized to join Inconel-625 plates through hybrid heating technique using Inconel-625 powder as an interface filler material. Post welding characterization of microwave developed joints through X-ray diffraction shows the development of carbides of niobium and chromium as well as intermetallic phases along with the primary ?-phase face-centered cubic matrix. Microstructural examination reveals the formation of Laves phase along the grain boundaries in the fusion zone. Microwave-induced joints exhibit average microhardness of 245 ± 20 HV and 0.7% porosity in the fusion zone. Average ultimate tensile strength and flexural strength of the developed joints were estimated at 375 and 377 MPa respectively. Average impact toughness of microwave-induced joints is observed to be 18 J. © IMechE 2017.Item Corrosion protection of low-cost carbon steel with SS-309Mo and Inconel-625 bimetallic weld overlay(Institute of Physics Publishing helen.craven@iop.org, 2019) Mudha, A.A.; Shashikala, H.D.; Nagaraja, H.S.The dissimilar weld overlay coatings of components can lead to corrosion. In the present work, two different weld overlay layers (SS-309Mo and Inconel-625) are deposited on IS2062 grade B carbon steel, in order to avoid distortions and improve corrosion resistance. The microstructural investigations revealed that the intermediate layer SS-309Mo on carbon steel prevents the dilution by aiding crack-free weld overlay of Inconel-625 on the top. The corrosion behaviour of the coatings is studied using Linear Polarization Resistance and the Electrochemical Impedance Spectroscopy. The corrosion rate of the coatings decreased by two orders of magnitude compared to that of low carbon steel substrate. The corrosion rate of the deposited Inconel-625 along with intermediate SS-309Mo is 1.16×10-3 and is comparable to that of bare Inconel-625 (1.12×10-3 mmpy). Further, the immersion tests for 14 days show that, the depositions are stable with the formation of the passive film. ©2019 IOP Publishing Ltd.Item Optimization of Process Parameters by Taguchi Grey Relational Analysis in Joining Inconel-625 Through Microwave Hybrid Heating(Springer New York LLC barbara.b.bertram@gsk.com, 2019) Badiger, R.I.; Narendranath, S.; Srinath, M.S.The quality of welded joints developed using microwave hybrid heating (MHH) technique is largely influenced by properties of the constituents employed in the process. This article investigates the influence of process parameters on tensile strength and flexural strength of Inconel-625 plates welded through MHH. Experiments were planned according to Taguchi L 16 orthogonal array by considering three factors: separator, susceptor and filler powder particle size. Ultimate tensile strength and flexural strength of the specimens welded at 600 and 900 W were chosen as response characteristics. Application of Taguchi-based GRA has been effectively used to optimize multi-performance characteristics of the process. ANOVA results indicate that size of interface filler powder is the most significant factor in determining the joint strength followed by separator and susceptor. Further to corroborate the optimal parameter setting for maximum strength values, metallurgical characterization of the specimens is carried out through XRD and SEM. Specimens processed at 600 W exhibited superior properties compared to their counterparts developed at 900 W. © 2018, Springer Science+Business Media, LLC, part of Springer Nature and ASM International.Item Compositional and Bath Temperature Effects on Heat Transfer During Quenching in Molten NaNO3–KNO3 Salt Mixtures(Springer, 2020) Pranesh Rao, K.M.P.; Prabhu, K.N.The present study involved the assessment of cooling severity of molten NaNO3–KNO3 mixtures which are widely used as quench media for austempering and martempering operations. An Inconel probe instrumented with thermocouples was quenched in molten NaNO3–KNO3 binary mixtures of varying concentration maintained at different quench bath temperatures. The temperature data acquired at various locations in the Inconel probe during quenching was used to calculate the spatially dependent transient heat flux at the metal–quenchant interface. Two critical points corresponding to peak heat extraction rates during the nucleate boiling stage and transition from boiling to convection stage were identified for each quench medium. The variation of average heat flux and average surface temperature corresponding to these critical points was mapped with variation in bath temperature and composition of the quench medium. AISI 4140 steel probes were quenched in these quench media maintained at 300 and 350 °C. The average hardness values measured in steel probes agreed with the cooling performance of these quench media determined using Inconel probe. The degree of uniformity in heat transfer as indicated by the spatial variation of normalized heat energy decreased with the increase in the concentration of KNO3 in the quench medium. A mechanism of boiling heat transfer during quenching based on thermochemical decomposition of the salt was proposed. © 2020, ASM International.