Faculty Publications
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Item Hot dip aluminizing of 9Cr-1Mo steels and their heat treatment(Trans Tech Publications Ltd ttp@transtec.ch, 2015) Patel, J.; Huilgol, P.; Jamnapura, N.; Bhat, K.Coupons of 9Cr-1Mo steels of type SA 387 Grade 9 class 2 were hot dip aluminized using Al bath at a temperature of 700 °C for 30 seconds. The samples were further heat treated at 750 °C for durations of 1, 3 and 5 hours, respectively. The samples were characterized using X-ray diffractometry, scanning electron microscopy and energy dispersive spectroscopy. The investigation showed that as coated samples contain an aluminum top coat, a reaction layer and substrate material. Within the reaction layer, two distinct regions corresponding to Fe2Al5 and Fe4Al13 were identified. Chromium up to 2 at% was observed. After heat treatment Al coat was not existing. Two distinct layers, corresponding to a thick Fe2Al5 and a thin FeAl were observed at shorter heat treatment duration. Under longer heat treatment durations, multiple phases, namely, Fe2Al5, FeAl, Fe3Al and solid solution of Al in Fe were observed. © (2015) Trans Tech Publications, Switzerland.Item Heat treatment of friction surfaced steel-aluminum couple(Trans Tech Publications Ltd ttp@transtec.ch, 2015) Bhat, K.; Nithin; Bhat, S.; SudeendranFriction surfacing is a solid state process and it is amenable for deposition of aluminum on steel. In this investigation, the mild steel surface was coated with a layer of aluminum using friction surfacing route. The aluminum thickness was in the range of 40-50 μm. It was followed by a heat treatment step to convert aluminum layer in to an aluminide layer. Heat treatment was done in open atmosphere at 700 °C for 2 hours. Microstuctural analysis showed that the aluminide layer is mainly made of Fe2Al5 and Fe4Al13, FeAl and Fe3Al are minor in fraction. Formation of Fe2Al5 is discussed. The aluminide layer also has some amount of porosities. © (2015) Trans Tech Publications, Switzerland.Item Effect of Microstructure on the Fatigue Crack Growth Behavior in Al–Zn–Mg–Cu Alloy(Springer Science and Business Media Deutschland GmbH, 2020) Nandana, M.S.; Udaya, B.K.; Manjunatha, C.M.High-strength Al–Zn–Mg–Cu alloys are used in airframe structures, such as bulk heads, wing spars, and lug joints. In this investigation, the effect of RRA microstructure on the fatigue crack growth rate (FCGR) behavior is studied. The 7010 aluminum alloy was heat treated to two different conditions, i.e., T6 and RRA. The microstructure of the heat-treated alloy is characterized by using transmission electron microscope (TEM). The FCGR tests were performed as per ASTM E647 standard by using a 100 kN servo-hydraulic test machine. The tests were performed using standard compact tension (CT) specimens with a stress ratio, R = 0.7 using a sine wave form at 10 Hz in a standard laboratory air environment. The matrix microstructure of the RRA-treated alloy consists of fine scale η´ (MgZn2) precipitates with increased interparticle spacing when compared to closely packed η´ precipitates in the standard T6-treated alloy. The grain boundary precipitates are coarsened and discrete in the RRA-treated alloy, while it is continuous in T6 condition. An improvement in the threshold stress intensity factor range (ΔKth) by about 0.65 MPa√m is observed in RRA-treated alloy compared to the T6-treated alloy. The FCGR was observed to be lower by 2 times in RRA-treated alloy compared to T6-treated alloy over the major portion of FCGR curve. The increased free slipping distance between the matrix precipitates in RRA-treated alloy is correlated to the improved fatigue crack growth resistance of the RRA-treated aluminum alloy. © 2020, Springer Nature Singapore Pte Ltd.Item Influence of heat treatment on near-threshold fatigue crack growth behavior of high strength aluminum alloy 7010(Springer Science and Business Media Deutschland GmbH, 2020) Nandana, M.S.; Udaya, B.K.; Manjunatha, C.M.In this study, aluminum alloy 7010 was subjected to three different ageing treatments i.e., peak ageing (T6), over ageing (T7451) and retrogression and re-ageing (RRA) to study the influence of precipitate microstructure on the fatigue crack growth rate (FCGR) behavior. The microstructural modifications were studied by using TEM to examine the change in size and morphology of the precipitates. The size of the precipitates in the matrix range from 16-20nm in T7451, 5-6nm in RRA and 2-3nm in T6 alloys, respectively. The FCGR tests were performed on standard compact tension (CT) specimens as per ASTM E647 standard in a computer controlled servo-hydraulic test machine with applied stress ratio, R = 0.1 and loading frequency of 10 Hz. The crack growth was measured by adopting compliance technique using a CMOD gauge attached to the CT specimen. The fatigue crack growth rate was higher in T7451 and lowest in RRA treated alloy. The RRA treated alloy showed higher (formula presented) compared to T7451 and T6 treated alloys. The measured (formula presented) was 11.1, 10.3 and (formula presented) in RRA, T6 and T7451 alloys, respectively. In the near-threshold regime, the RRA treated alloy exhibited nearly 2-3 times reduction in the crack growth rate compared to the T6 alloy. The growth rate in the RRA alloy was one order lower than that of the T7451 condition. The surface roughness of RRA treated alloy was more pronounced. The reduction in FCGR observed in RRA alloy was correlated to partial crack closure due to tortuous crack path and partially due to increased spacing between the matrix precipitates. The reduction in near-threshold FCGR and increase in (formula presented) is expected to benefit the damage tolerant capability of the aircraft structural components under service loads. © Springer Nature Switzerland AG 2020.Item Rotating bending fatigue tests were carried out on austempered ductile iron containing 1.5 wt% nickel and 0.3 wt% molybdenum. The ductile iron was austenitized at 900 or 1050 °C and then austempered at 280 or 400 °C for different lengths of time to obtain different microstructures. The fatigue strength was correlated with the amount of retained austenite and its carbon content, which were both determined by X-ray diffraction technique. While the tensile strength decreased with increasing retained austenite content, the fatigue strength was found to increase. Carbide precipitation was found to be detrimental to fatigue strength. Lower austenitizing temperature resulted in better fatigue strength. © 1994 Chapman & Hall.(Kluwer Academic Publishers, Effect of microstructure on the fatigue strength of an austempered ductile iron) Shanmugam, P.; Prasad Rao, P.; Rajendra Udupa, K.; Venkataraman, N.1994Item Austempered ductile iron containing 0.9 Ni and 0.3 Mo and subject to low stress dry sand abrasive testing shows that wear behaviour is very sensitive to heat treatment conditions. It is concluded that large retained austenite content promotes wear resistance.(Inst of Engineers (India), Low stress dry sand abrasive wear behaviour of austempered ductile iron) Prasad Rao, P.1995Item An alloy containing 49 at.% aluminium was heat treated at different temperatures within the ? + ? two-phase field to get five different volume fractions of lamellar constituent. Creep studies were carried out on these samples at five different temperatures in the interval between 1023 and 1223 K, by impression creep technique using four levels of stresses at each temperature. For a given temperature and stress, steady state impression velocity decreased with increasing volume fraction of lamellar constituent. Activation energy for steady state creep increased linearly with lamellar content from 185 kJ/mol at 22 vol.% to 362 kJ/mol at 100 vol.%. The stress exponent was found to be around 1.2 in all the cases. The results show that a fully lamellar structure has a superior behaviour where creep is an important factor.(Carl Hanser Verlag, Effect of microstructure on the impression creep of two-phase titanium aluminide) Prasad Rao, P.; Swamy, K.Shivananda1995Item Photoconductivity has been studied in cadmium selenide thin films prepared by thermal evaporation in vacuum. Attempts have been made to correlate the photoresponse with the deposition conditions. It has been observed that as-grown films, irrespective of the cadmium content, are not photosensitive and that baking in air, especially above 723 K, leads to considerable improvement in the photoconducting properties of cadmium selenide films.(Photoconductivity in vacuum deposited cadmium selenide thin films) Rajendra, B.V.; Kasturi, V.B.; Shivakumar, G.K.2004Item Heat transfer during quenching of modified and unmodified gravity die-cast A357 cylindrical bars(2006) Prabhu, K.; Hemanna, P.Heat transfer during quenching of chill-cast modified and unmodified A357 Al-Si alloy was examined using a computer-aided cooling curve analysis. Water at 60°C and a vegetable oil (palm oil) were used as quench media. The measured temperatures inside cylindrical probes of the A357 alloy were used as inputs in an inverse heat-conduction model to estimate heat flux transients at the probe/quenchant interface and the surface temperature of the probe in contact with the quench medium. It was observed that modified alloy probes yielded higher cooling rates and heat flux transients. The investigation clearly showed that the heat transfer during quenching depends on the casting history. The increase in the cooling rate and peak heat flux was attributed to the increase in the thermal conductivity of the material on modification melt treatment owing to the change in silicon morphology. Fine and fibrous silicon particles in modified A357 probes increase the conductance of the probe resulting in higher heat transfer rates. This was confirmed by measuring the electrical conductivity of modified samples, which were found to be higher than those of unmodified samples. The ultrasound velocity in the probes decreased on modification. ©ASM International.Item Comparative study of heat transfer and wetting behaviour of conventional and bioquenchants for industrial heat treatment(2008) Fernandes, P.; Prabhu, K.N.An investigation was conducted to study the suitability of vegetable oils as bioquenchants for industrial heat treatment. The study involved the assessment of the severity of quenching and wetting behaviour of conventional and vegetable oil quench media. Quench severities of sunflower, coconut and palm oils were found to be greater than mineral oil. The quench severity of aqueous media is greater than oil media although their wettability is poor as indicated by their higher contact angles. A dimensionless contact angle parameter defined in this work is found to be a better parameter to compare the wetting behaviour with heat transfer. © 2007 Elsevier Ltd. All rights reserved.