Faculty Publications

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    Characterization of Mechanical and Microstructural Properties of FA and GGBS-Based Geopolymer Mortar Cured in Ambient Condition
    (Springer, 2021) Prasanna, K.M.; Tamboli, S.; Das, B.B.
    Fly ash-based geopolymer mortars require heat curing to achieve its properties, which limits its practical application at ambient conditions. The present study was aimed to accomplish the need for application of fly ash-based geopolymers for practical viability without any heat curing by inclusion of ground-granulated blast furnace slag (GGBS). The results revealed that inclusion of GGBS as a partial replacement to fly ash (FA) in geopolymer mortar, which is cured in ambient curing condition, can be able to achieve required setting time and compressive strength. Amalgamation of GGBS with class FA as binder in geopolymerization lend a hand to attain compressive strength as well as setting time which is analogous to ordinary Portland cement (OPC). Microstructural properties were studied using scanning electron microscopy. © 2021, Springer Nature Singapore Pte Ltd.
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    Automation of Curing Using Prefabricated Sensors
    (Springer Science and Business Media Deutschland GmbH, 2021) Agarwalla, A.; Das, B.B.
    Curing is one of the universal phenomena followed after casting and finishing of concrete over an extended period of time, which helps to develop the compressive strength and durability by maintaining an optimum moisture and temperature condition. It keeps the concrete hydrated, restricts volumetric shrinkage, provides resistance to abrasion, freezing and thawing. There are many ways to cure concrete but, in this article, discussion will be on automation of curing using IoT and moisture sensors and relays which will likely replicate the lab condition on site by maintaining constant moisture content in concrete by supplying required amount of water. Generally, on site the curing process is carried out for 6–7 days once or twice a day at a large interval as a result of which the free moisture content falls and the rate of hydration decreases. It results in poor compressive strength and durability compared with laboratory samples because the 7 days compressive strength is not achieved which is more important than that of 28 days compressive strength which is successfully achieved in the lab. Various technologies used in this article will help in real-time monitoring of concrete condition with ease which will further be beneficial for the construction industry. This paper will cover how these technologies are integrated to automate the whole process, and its effect on compressive strength of concrete for which a consistent mix of M20, M25, M30 was prepared to compare the result of strength of concrete at 3, 7 and 28 days of curing in three different conditions, giving the strength of in-situ automatically cured concrete sample similar to that of laboratory cured concrete sample and an increase in 16.09% of compressive strength was observed with respect to concrete cured manually in site conditions. © 2021, Springer Nature Singapore Pte Ltd.
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    An empirical model for the estimation of moisture ratio during microwave drying of plaster of Paris
    (2008) Ganesapillai, M.G.; Iyyaswami, I.; Murugesan, T.
    The drying characteristics of plaster of Paris (POP) under microwave irradiation were studied for different shapes of materials through various drying parameters like microwave power, initial moisture content, and drying time. An empirical model for the estimation of moisture ratio was developed using the drying kinetic data of POP. Further, the experimental data on moisture ratio of POP for different operating conditions were fitted with the nine basic drying model equations. Based on the observations, the constants and coefficients of the literature models were rewritten in the form of Arrhenius and logarithmic expressions considering microwave power as input variable. Fifty-eight new model expressions were derived by changing the constants and coefficients and tested using the present experimental data. From the analysis of RMSE, ?2, and EF parameters for the derived models, a suitable empirical model (Model No. 55, RMSE = 0.0874; ?2 = 0.0020; EF = 0.9999) was established to represent the present experimental data on microwave drying of POP.
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    Characterization and process optimization of microwave drying of plaster of Paris
    (2008) Ganesapillai, M.G.; Iyyaswami, I.; Murugesan, T.
    The changes in the characteristics of plaster of Paris (pop) during drying operation under microwave irradiation conditions, namely surface morphology, effective moisture diffusivity, and absorption of microwave, were studied. The drying characteristics and kinetics of the process during microwave drying of plaster were studied for rectangular-faced cuboids (80 × 70 × 15, L × B × H in mm) through various drying parameters like microwave power input, initial moisture content, and drying time. Further, the experimental data on moisture ratio of plaster for different operating conditions were obtained and the optimization of the microwave drying process parameters was performed with response surface methodology (RSM) by considering all the above-said independent variables. Based on the RSM analysis, the optimum values of the process variables were obtained as: initial moisture content (A) 60%; microwave power input (B) 180 W; and drying time (C) 480 S.
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    Moisture diffusivity and energy consumption during microwave drying of plaster of Paris
    (2010) Ganesapillai, M.G.; Iyyaswami, I.; Miranda, L.R.; Murugesan, T.
    The drying characteristics of plaster of paris (POP) under microwave conditions at different microwave power input, initial moisture content, sample thickness and drying time were studied. Further the experimental data on moisture ratio of POP for different operating conditions were obtained and calculations were made using nine basic drying model equations. The appropriate model with modified constants and coefficients to represent the drying kinetics of POP was found through the analysis of the statistical analysis. The effective moisture diffusivity of the drying process was also computed for different experimental conditions and a relationship between the drying rate constant and the effective moisture diffusivity was obtained. The energy consumption for microwave drying of plaster of paris at different experimental conditions were also computed. © 2010 The Berkeley Electronic Press. All rights reserved.
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    Studies on iron tailings towards usage for paving blocks manufacture
    (2010) Mangalpady, M.; Sampath Kumar, N.N.
    Disposal of mill tailings is one of the major problems in mining industry. Investigations are being done all over the world to utilize tailings for useful purposes. The scope of this work is to study the utilization of iron ore tailings in manufacture of concrete paving blocks. Five reference mixes were prepared using cement, jelly dust and baby jelly. Ten paving blocks were prepared from each type of mix, out of which five specimens were cured for 7 days and five were cured for 28 days. By using sand and tailings as fine aggregates, two modified mixes were prepared by replacing jelly dust partly in reference mixes. Similar to reference mix, five mix ratios were made and ten paving blocks were prepared from each type of mixtures. From each set of paving blocks, five specimens were cured for 7 days and the other five specimens were cured for 28 days. Laboratory tests were conducted to assess water absorption and compressive strength of specimens, and graphs were plotted for their comparison among each type of respective mix ratios. In all the comparisons, compressive strength of tailing based mix was higher than the respective reference mix. Similar trend is shown by the graphs plotted for water absorption. © 2010 CAFET-INNOVA TECHNICAL SOCIETY. All rights reserved.
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    Study on the strength parameters of high volume fly ash concrete and geopolymer concrete
    (2011) Shetty, A.; Anand, V.R.; Hegde, P.
    Concrete has been the most preferred construction material. It is being increasingly used day by day all over the world due to its versatility, mould ability and high compressive strength. But the large-scale production of cement is causing environmental problems on one hand and the unrestricted depletion of natural resources on the other. So the issue of sustainable development in concrete construction is addressed in this paper through development of concrete mixes by replacing certain percentage of cement with fly ash. Trials on concrete mixes with replacement of 40%, 50%, 60% and 70% of cement with fly ash are carried out and the results depict that at the replacement level of 40% cement by fly ash, the required strength is achieved. It is also observed that the rate of early strength gain is retarded as the percentage replacement of cement increases. But in case of Geopolymer concrete (100% replacement of cement by fly ash) under a curing temperature around 600C and above, the strength gain rate is very high in initial stages. It is observed that design strength is achieved within 28 hours of oven curing. © 2011 CAFET-INNOVA TECHNICAL SOCIETY. All rights reserved.
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    Synthesis and characterization of schiff base metal complexes and reactivity studies with malemide epoxy resin
    (Korean Chemical Society sunlee@kcsnet.or.kr, 2012) Lakshmi, B.; Shivananda, K.N.; Prakash, G.A.; Isloor, A.M.; Mahendra, K.N.
    A novel malemide epoxy containing Co(II), Ni(II) and Cu(II) ions have been synthesized by curing malemide epoxy resin (MIEB-13) and Co(II), Ni(II) and Cu(II) complexes of macrocyclic bis-hydrazone Schiff base. The Schiff base was synthesized by reacting 1,4-dicarbnyl phenyl dihydrazide with 2,6-diformyl-4-methyl phenol. The Schiff base and its Co(II), Ni(II) and Cu(II) complexes have been characterized by elemental analyses, spectral (IR, 1H NMR, UV-vis., FAB mass, ESR), thermal and magnetic data. The curing reaction of maleimide epoxy compound with metal complexes was studied as curing agents. The stability of cured samples was studied by thermo-gravimetric analyses and which have excellent chemical (acid/alkali/solvent) and water absorption resistance. Further, the scanning electron microscopy (SEM) and definitional scanning colorimetric (DSC) techniques were confirmed the phase homogeneity of the cured systems.
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    Effect of mineral fillers in improving mechanical properties of FKM vulcanizates
    (2013) Byravan, A.; Bangaragiri, A.
    Arun Byravan from 3M India, and Anupama Bangaragiri from NITK examine the effect of mineral fillers in improving mechanical properties of FKM vulcanizates. The selection of the formulations is done on the basis of a oil seal application and loading of the mineral fillers is varied to maintain a hardness of around 75 durometer A. Compounds have been press cured at 180°C for 10 minutes and post cured at 230°C for 24 hours to eliminate all the volatiles present in the matrix. The aging study of the compounds reveals that the property loss is within the expected range. This study helps in predicting the behavior of filled vulcanizates at these aging conditions and how the crosslinks of filled compound resist higher temperatures. Tensile loss of highly loaded compounds after aging has been found to be low as compared to the reference compound.
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    Investigating the Utility of Iron Ore Waste in Preparing Non-fired Bricks
    (Springer India sanjiv.goswami@springer.co.in, 2017) Lamani, S.R.; Mangalpady, M.; Vardhan, H.
    Iron ore waste is a major problem for mine owners due to the difficulty involved in its storage, handling and other environmental related issues. An alternative solution to this is utilisation of iron ore waste (IOW) as some value added product in construction industry. An attempt has been made in this paper in examining the possibility of making non-fired bricks from iron ore waste with some additives like cement and fly-ash. Each of the additives were mixed with IOW in different ratios and different sets of bricks were prepared. The prepared IOW bricks were cured for 7, 14, 21 and 28 days and their respective compressive strength and percentage of water absorption were determined. The results show that IOW bricks prepared with 9% and above cement and with 28 days of curing are suitable for brick making and meet the IS specifications. It was also observed that the weight of the prepared bricks with 9% cement with 28 days of curing varies between 2.35 and 2.45 kg whereas the weight of compressed fire clay bricks varies from 2.80 to 2.89 kg. Results also show that the cost of bricks prepared with cement ranging from 9 to 20% is comparable to that of commercially available compressed bricks. © 2016, The Institution of Engineers (India).