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    Evaluation of hydrogen-assisted cracking susceptibility in modified 9cr-1mo steel welds
    (Springer, 2020) Chakraborty, G.; Rejeesh, R.; Ramana, O.V.; Albert, S.K.
    The hydrogen-assisted cracking susceptibility of modified 9Cr-1Mo steel weld is evaluated by Y-groove and gapped bead-on-plate test. It is found that a combination of pre + post heat is able to prevent cracking. However, the pre + post heat temperature combination determined from G-BOP test to prevent cracking (200 °C) is found to be higher than that in Y-groove test (100 °C). This is attributed to the higher weld restraint experienced in G-BOP than Y-groove test. For both the tests, the weld metal is found to be more susceptible to cracking than the heat affected zone. In addition to the diffusible hydrogen content of the welding consumables, diffusible hydrogen present in the G-BOP specimens prepared with different preheating and combinations of pre + post heat is also estimated by maintaining identical cooling conditions. The diffusible hydrogen in the weld for which no cracking is reported for G-BOP test (200 °C pre + post heat) is less than 1 ml/100 g. Considering the high restraint conditions present in the G-BOP test, it can be concluded that to prevent HAC in P91 steel, the choice of welding parameters (hydrogen content in welding consumable, heat input, pre/post-heating) should be such that diffusible hydrogen in the weld is brought down to below 1 ml/100 g. © 2019, International Institute of Welding.
  • Item
    Experimental study on failure and fracturing attributes of granite after thermal treatments with different cooling conditions
    (Elsevier B.V., 2022) Srinivasan, V.; Hasainar, H.; Singh, T.N.
    Thermal damage is one of the fundamental mechanisms affecting the stability of rocks encountered in many deep geo-engineering ventures such as nuclear waste isolation, geothermal extraction etc. In the present study, the findings on influence of heating and subsequent cooling conditions on the fracturing and mechanical behaviour of an Indian granite are discussed. The granite samples from Jalore region of India were heated from room temperature to 600 °C followed by slow cooling and water quenching treatments. It was observed that rapid cooling through quenching had a greater impact on strength, elastic properties than slow cooling rate. Moreover, a drastic shift in terms of fracturing thresholds was witnessed, as a function of both temperature and sudden thermal shock experienced by rock at higher cooling rate. The simultaneous AE monitoring results suggested an early crack damage at higher thermal regimes. With help of microscopic observations, it was observed that inter-granular crack boundaries widened with increasing thermal damage experienced by minerals under both cooling conditions. However, the fracturing process was intense under rapid cooling treatment due to the invasion of water due to quenching which accelerated severe intra-crack growths, especially at higher thermal stress because of the rapid cooling rate than the slow cooling. The increased intensity of thermal cracks with temperatures and with variation in cooling rate was inferred as the primary reason for decay of rock characteristics. This was very well supplemented by decay in strength properties and changes in fracturing attributes of the tested granite as inferred from acoustic monitoring. © 2022