Faculty Publications
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Item Plasma nitriding of AISI 2205 steel: Effects of surface mechanical attrition treatment and chemical etching(Maney Publishing michael.wagreich@univie.ac.at, 2016) Gatey, A.M.; Hosmani, S.S.; Arya, S.B.; Figueroa, C.A.; Singh, R.P.In the present study, surface mechanical attrition treatment (SMAT) and plasma nitriding were conducted on AISI 2205 steel. SMAT was effective in enhancing the surface hardness of the steel by about 80%. The influence of SMAT on the corrosion behaviour of the steel was studied in a 3.5 wt-% NaCl solution. Due to the stable and thicker passive layer, improved corrosion resistance was observed for the SMATed steel. However, nitrogen diffusion during plasma nitriding was impeded by the improved passivation, especially for the lower duration (30 min) of chemical etching/cleaning (i.e. sputter cleaning in hydrogen plasma) of the specimen's surface. Furthermore, high chemical etching duration (120 min) resulted in improved surface hardness and nitriding kinetics. © 2016 Institute of Materials, Minerals and Mining.Item Role of surface mechanical attrition treatment and chemical etching on plasma nitriding behavior of AISI 304L steel(Elsevier B.V., 2016) Gatey, A.M.; Hosmani, S.S.; Figueroa, C.A.; Arya, S.B.; Singh, R.P.In the present study, the effect of surface mechanical attrition treatment (SMAT) on corrosion resistance and plasma nitriding behavior of AISI 304L stainless steel (SS) was investigated. Mechanical twins and deformation induced martensite phase were observed in the SMAT affected region. SMAT improved the corrosion resistance and nitriding kinetics of AISI 304L SS. Effective nitriding time and hence, the thickness of the nitrided layer were increased with increase in the duration of chemical etching and a decrease in the stability of passive layer on the SMATed specimens. Surface hardness of the nitrided specimens was dependent on the formation of expanded austenite (?N) and its decomposition (especially, at higher effective nitriding time). © 2016 Elsevier B.V.Item Reprocessed waste sunflower cooking oil as quenchant for heat treatment(Elsevier Ltd, 2020) Prathviraj, M.P.; Samuel, A.; Prabhu, K.N.The growing concern to minimize the use of petroleum derived mineral oil in heat treatment industries has led to the search for alternative eco-friendly quenchants. Although vegetable oils seem to be a viable option, the higher cost and inferior thermal and oxidation stability have limited their application in the heat treatment industry. The reuse of waste cooking oils for industrial heat treatment would not only make quenchants cost-efficient but also environment friendly. In this study, the cooling performance of waste sunflower cooking oil was assessed and compared with that of unused sunflower cooking and mineral oils. The waste sunflower oil was made suitable for quenching by cleaning and chemical treatment. The experiment to assess the suitability of reprocessed oil for quenching was conducted using an Inconel 600 standard probe according to ISO 9950 and ASTM D 6200 standards. The thermal history acquired while quenching of the probe was used to estimate the surface heat flux transients. The results indicated that the chemically treated waste sunflower cooking oil had a higher cooling performance than that of unused sunflower and the mineral oils. A good agreement was found between the heat flux transients and hardness data obtained with the quenched AISI 4140 steel probe. The simulation of temperature and hardness distribution indicated more uniformity along the length of the probe indicating more uniform cooling with chemically treated waste sunflower cooking oil. © 2020 Elsevier Ltd