Faculty Publications
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Item Effect of surface roughness on metal/quenchant interfacial heat transfer and evolution of microstructure(Elsevier Ltd, 2007) Prabhu, K.N.; Fernandes, P.In the present work, the effect of surface roughness on heat transfer rates in various quenchants was determined. The heat flux transients at the probe/quenchant interface were estimated by inverse modeling of heat conduction during end quenching of stainless steel probes with three different surface roughness (grooved, Ra = 3.0 and 1 ?m). Heat transfer during quenching was correlated with the hardness obtained for medium carbon AISI 1060 steel specimens. The effect of surface roughness on heat transfer rate during quenching in water and brine was significant for rough surface whereas its effect on heat transfer rate is only marginal in high viscosity oil quenchants. A fully martensitic structure was observed with grooved surface subjected to water quenching. With a smooth surface a mixed microstructure was obtained. The oil quenched specimens were found to be less sensitive to surface roughness. © 2005 Elsevier Ltd. All rights reserved.Item Severity of quenching and kinetics of wetting of nanofluids and vegetable oils(2009) Jagannath, V.; Prabhu, K.N.In the present work, the suitability of vegetable oil blends with mineral oil and alumina based nanofluids as quench media for industrial heat treatment was investigated. Sunflower oil, palm oil, and mineral oil were used for preparing the blends. Alumina based nanofluids of varying concentrations ranging from 0.01-4 % were used. The size of alumina particles was about 50 nm. The severity of quenching and heat transfer coefficients were estimated during quenching of copper probes. Heat transfer coefficients were estimated using a lumped heat capacitance model. The static contact angle was measured on copper substrates having a surface texture similar to the probes used for estimation of heat transfer coefficients. A dynamic contact angle analyzer was used for this purpose. The measured contact angles of nanofluids on copper were high compared to oils, indicating poor wetting by quench media that are polar in nature. Wetting characteristics had a significant effect on heat transfer coefficients estimated during quenching. Copyright © 2009 by ASTM International.Item Comparison of Grossmann and lumped heat capacitance methods for assessment of heat transfer characteristics of quench media(2011) Prabhu, K.N.; Ali, I.The suitability of Grossmann and lumped heat capacitance (LHC) methods for estimation of quench severity of nanofluids, brine solutions and a laboratory detergent based medium was investigated. The study involved the assessment of the effect of section thickness of the probe on heat transfer coefficients for different quench media. Computer aided cooling curve analysis during quenching of type 304 stainless steel probes was carried out. The measured thermal history data were used to estimate heat transfer coefficients by Grossmann and LHC methods. The LHC method based on a 10 mm diameter stainless steel probe was found to be applicable for characterising media having quench severity less than 20 m-1. Although Grossmann method is based on the concept of average heat transfer coefficient, it can be used for quench media having varying severity of quenching. Grossmann method is found to be more sensitive to the effect of section thickness on heat transfer. © 2011 IHTSE Partnership.Item Characterisation of water base copper nanoquenchants by standard cooling curve analysis(2011) Ramesh, G.; Prabhu, K.N.Water base copper nanofluids having concentrations varying from 0?001 to 0?1 vol.-% were prepared and used as quench media for immersion quenching. Cooling curve analyses were carried out by using a standard ISO/DIS 9950 quench probe. An inverse heat conduction model is employed to estimate the metal/nanoquenchant interfacial heat flux transients from the measured temperature field and thermophysical properties of the quench probe material. The addition of copper nanoparticles had a significant effect on the occurrence of the vapour blanket stage and nucleate boiling stage. Furthermore, all six cooling curve parameters were found to be altered by adding nanoparticles to water. The contact angle of water decreased from 67 to 39° by adding 0?1 vol.-% of copper nanoparticles indicating the improved wettability of nanofluids. The heat flux curve shows a maximum initially then drops rapidly during quenching. The peak cooling rate and heat flux of water increased by adding copper nanoparticles up to 0?01 vol.-%. Both parameters decreased with further increase in concentration of nanoparticles. The results suggest that the quench severity of water could be altered by adding copper nanoparticles. © 2011 IHTSE Partnership.Item Effect of boundary heat transfer coefficient and probe section size on cooling curves during quenching(ASTM International, 2012) Ramesh, G.; Prabhu, K.N.In the present work the effect of boundary heat transfer coefficient and section size of quench probe material on cooling curves was investigated by using finite difference heat transfer based SolidCast software. Simulations were carried out at different combinations of heat transfer coefficient and quench probe diameter and thermal history at the geometric center of the probe was estimated to generate cooling curves. Simulation results show that both boundary heat transfer coefficient and quench probe diameter had a significant effect on the average cooling rate. A relationship between Grossmann quench severity (H), thermal conductivity of material, size of the probe, and average cooling rate was established. By using this model, for a known quench medium, probe size, and material it is possible to predict the average cooling rate of the probe. On the other-hand, for a given material and required cooling rate, cooling severity required from the quench media could be predicted and accordingly an appropriate quench medium can be selected. © 2012 by ASTM International.Item Wetting kinematics and spreading behaviour of water based aluminium nanofluids during immersion quenching(2013) Ramesh, G.; Prabhu, K.In the present work, wetting kinematics of water based aluminium nanofluids having nanoparticle concentrations varying from 0.001 to 0.5 vol.-% during immersion quenching of Inconel 600 probe was investigated by measuring the contact resistance. The contact resistance between the quench probe and counter electrode during quenching indicated that the duration of the film of water vapour decreased with increasing nanoparticle concentration as well as absence of stable vapour film formation with 0.05, 0.1 and 0.5 vol.-% of nanoparticles. The phenomenon of a repeated wetting process was observed during quenching in nanofluids. Further, quenching in 0.1 and 0.5 vol.-% nanofluids indicated the formation of a nanoparticle porous layer and its deposition on the quench probe. The spreading behaviour was studied by measuring the dynamic contact angle of nanofluids droplets on Inconel 600 substrate. Contact angle measurement showed that the addition of aluminium nanoparticles did not have a significant effect on the relaxation of contact angle of water droplet. However, lower static contact angles were obtained for nanofluids indicating improved wetting. © 2013 IHTSE Partnership.Item Dimensionless cooling performance parameter for characterization of quench media(2013) Ramesh, G.; Prabhu, K.The effect of varying thermal properties and boundary heat transfer coefficients on temperature profiles inside cylindrical quench probes was simulated during immersion cooling. The results of simulation indicated that, for assessment of the cooling performance of the quench media, the ratio of the quench probe diameter to its thermal conductivity should be less than 0.0005 m2K/W. A simple dimensionless cooling parameter (D 2CR/??T) was proposed to assess the cooling performance of quench media. © 2013 The Minerals, Metals & Materials Society and ASM International.Item Ultrafast dynamics of autoionizing states in O2 probed by laser-field-assisted XUV photoionization(2013) Zhu, C.; Ko, D.H.; Kang, K.S.; Lee, J.; Lee, J.-H.; Umesh, G.; Krishnakumar, E.; Nam, C.H.Dynamics of the autoionizing states in O2 was investigated using the method of laser-field-assisted extreme-ultraviolet photoionization. Harmonics, ranging from 9th to 21st orders generated in Kr with 25 fs laser pulses at 820 nm, were employed to carry out photoionization of O2. Distinct autoionization features in the photoelectron spectrum, stemming from the resonant excitation of superexcited states of O2 by the 11th harmonic, were observed. The superexcited states, referred to as autoionizing states, were identified to be the ?? = 0, n = 5 Rydberg states converging to the b 4?g- state of O 2+. Infrared laser pulses were utilized as the probe to monitor time-varying characteristics of photoionization and autoionization of O2. A decay time of 21 fs was obtained for the autoionizing states of O2 by deconvoluting the pump-probe results in O2 and Ar. © 2013 American Physical Society.Item Effect of thermal conductivity and viscosity on cooling performance of liquid quench media(Maney Publishing Suite 1C, Joseph's Well, Hanover Walk Leeds LS3 1AB, 2014) Ramesh, G.; Prabhu, K.In this present work, the effect of the thermophysical properties of quenchants on its cooling performance was investigated. Water, brine solutions, polymer solutions and mineral oils were chosen to have quench media with varying thermophysical properties. Cooling curve analyses were carried out by using standard ISO/DIS 9950 quench probe. Grossmann H quench severity of the quench media was determined from the relation of H and cooling rate. Cooling curve analysis results showed that the change in thermophysical properties of the quench media had significant effect on the cooling history of the quench probe. The viscosity of the quenchant used for immersion quenching is the most important factor that controls the cooling performance of the quenchant compared to thermal conductivity of the quench medium. © 2014 IHTSE Partnership.Item Wetting kinetics, kinematics and heat transfer characteristics of pongamia pinnata vegetable oil for industrial heat treatment(Elsevier Ltd, 2014) Ramesh, G.; Prabhu, K.The suitability of pongamia pinnata vegetable oil as cooling medium for quench heat treatment was investigated. Wetting kinetics, kinematics and heat transfer characteristics of pongamia oil during immersion quenching of hot Inconel probe were determined and compared with palm and mineral oils. A comparison of the relaxation of contact angle indicated early attainment of equilibrium contact angle for pongamia oil droplet on Inconel substrate. The equilibrium contact angle value of pongamia oil was in between mineral and palm oils. However, the spreading kinetics was faster with pongamia oil. Pongamia oil showed the formation of a stable vapour film on the probe surface during quenching. This phenomenon was not observed in palm oil and other vegetable oils reported in literature. Pongamia pinnata oil exhibits uniform nature of wetting front, intermediate rewetting temperature and less variations in rewetting temperatures during quenching. The hardening power of pongamia oil was higher than palm and mineral oils and the cooling of the probe was more uniform during quenching in pongamia oil. The heat transfer characteristics of pongamia oil were found to be superior to palm and mineral oils after film/transition boiling. Pongamia oil showed lower heat transfer but more uniform cooling during film boiling. © 2014 Elsevier B.V.