Faculty Publications
Permanent URI for this communityhttps://idr.nitk.ac.in/handle/123456789/18736
Publications by NITK Faculty
Browse
14 results
Search Results
Item Microstructural characterization and mechanical properties of cast Al-15Zn-2Mg alloy subjected to severe plastic deformation(Elsevier Ltd, 2018) Manjunath, G.K.; Udaya Bhat, K.; Preetham Kumar, G.V.In the present work, Al-15Zn-2Mg alloy was processed by ECAP technique for grain refinement. The ECAP processing was conducted at 150 °C. Microstructural characterization was carried out in OM, SEM, TEM and XRD. To evaluate the mechanical properties, hardness measurement and tensile tests were conducted at room temperature. Microstructural characterization showed that, ECAP processing leads to decrease in the grain size of the alloy. Also, small amount of dislocations were also observed in the ECAP processed material. After ECAP processing, precipitates nucleation in the material was identified in the XRD analysis. The strength and the hardness values were increased after ECAP processing. After ECAP processing, microhardness of the material is increased from 173 Hv to 252 Hv and the UTS of the material is increased from 166 MPa to 362 MPa. After tensile testing, fracture surface of the cast material showed dendritic structure and the fracture surface of the ECAP processed material showed dimples. © 2018 Elsevier Ltd. All rights reserved.Item Influence of retrogression and re-ageing heat treatment on the fatigue crack growth behavior of 7010 aluminum alloy(Elsevier B.V., 2019) Nandana, M.S.; Udaya Bhat, K.; Manjunatha, C.M.Aluminum alloys are widely used in aircraft structural components where light weight, high strength and good corrosion resistance are the primary requirements. These alloys are generally used in peak-aged (T6) condition in which they are susceptible for stress corrosion cracking. In the recent years, retrogression and re-ageing (RRA) treatment on aluminum alloy is carried out to enhance their corrosion resistance maintaining the ultimate tensile strength. The aim of this work was to study the influence of RRA treatment on the fatigue crack growth rate (FCGR) behavior. The 7010 aluminum alloy was heat treated to two different conditions i.e., T6 and RRA. The microstructures of these alloys were characterized by using TEM. Standard compact tension (CT) specimens were prepared and FCGR tests were carried out by using a 100 kN servo-hydraulic test machine as per ASTM E647-15e1. The constant amplitude FCGR tests were carried out at a stress ratio, R = 0.5 using sine wave loading pattern at 10 Hz. Crack length was monitored by following compliance technique. Microstructural studies show that RRA treated alloy contain fine and densely populated precipitates in the matrix along with coarse and discontinuous precipitates in the grain boundary. The fatigue crack growth rate was observed to reduce along with an increase in the threshold stress intensity factor range (ΔKth) for RRA treated alloy compared to the T6 alloy. The mechanisms for reduction in fatigue crack growth rate of RRA treated alloy is attributed to the microstructural modifications. The increased resistance is expected to enhance the damage tolerance capability of the alloy. © 2019 The Authors. Published by Elsevier B.V.Item Effect of wire feed rate on microstructure development during bead on plate welding of microalloyed steel using P-GMAW(Elsevier Ltd, 2020) John, M.; Kumar, P.A.; Udaya Bhat, K.Welding of advanced high strength steel has been challenging because of difficulties associated with retaining high strength and toughness in the weldment. In this investigation, Ti-Nb microalloyed 800 MPa steel was subjected to bead on plate welding trials using ER70S-6 filler wire. Synergic pulsed mode was used for welding. Here the system could optimize the welding current and voltage once the selection of wire feed rate was done. Analysis of weld bead was done by measuring the weld bead parameters, observing microstructural details and calculating microhardness values. The investigation indicates that 6 m/min wire feed rate produces good weld bead, minimum reinforcement and optimum dilution. The microstructure is predominantly acicular in nature and microhardness in weld and HAZ is higher compared to the beads produced using other wire feed rates. © 2020 Elsevier Ltd. All rights reserved.Item A study on HAZ behaviour in 800 MPa cold rolled and hot rolled steel weld(Elsevier Ltd, 2021) John, M.; Perka, P.; Udaya Bhat, K.; Bhat Panemangalore, D.In the automotive sector, the demand for advanced high strength steels (AHSS) is increasing day by day. Based on the application, cold rolled and hot rolled steels are used for various components in a vehicle body. Typically, cold-rolled grades with dual-phase, DP780 steel is used in the form of welded blanks. Hot rolled grades with Ti-Nb microalloy content, like HS800 steel are used in as long members. Welding is an important step to be considered in the design of materials for mass production as required in the automobile sector. In this investigation, Pulsed Gas Metal Arc Welding (P-GMAW) is carried out on both steels with a solid filler wire of strength 800 MPa. Static tensile tests indicated that failure in both steels welds occurred in the heat-affected zone region. The crack initiation and propagation behaviour were compared in both steels. In DP780 steels, the presence of the acicular ferrite and acicular martensite resisted the crack initiation and propagation in the weld region whereas, the chaotic nature of the acicular ferrite in HS800 steel. Microstructural studies revealed that the reason for heat affected zone (HAZ) failure in HS800 steel is due to the presence of hard TiN particles with a size of more than 1 µm which causes decohesion in the matrix. In DP780 steel failure is due to the presence of tempered martensite in the subcritical heat affected zone (SCHAZ). This study divulges the influence of filler wire chemistry, dilution, and welding parameters on cold rolled and hot rolled AHSS steels used in the automotive industry. © 2021 Elsevier Ltd. All rights reserved.Item Compositionally modulated multilayer Cu-Zn alloy coatings fabricated using eco-friendly non-cyanide pulse electrochemical deposition(Elsevier Ltd, 2023) Bharadishettar, N.; Kumar, K.; Udaya Bhat, K.Pulse electrodeposition of Cu-Zn compositional modulated multilayer alloy (CMA) coatings was carried out onto AISI 304 stainless steel substrate using an environmentally friendly alkaline non-cyanide electrolytic bath. Cu-Zn alloy multilayer coating was co-electrodeposited using a trapezoidal pulse current. Multilayer coatings can have two different metals in layers or two-phase mixtures. Different sets of multilayers of 10, 20, 50, and 100 were done using a trapezoidal pulse current. In the trapezoidal pulse current module, during the higher current stage (0.1 A) Zn was deposited as compared to the lower current module (0.02 A) where Cu was deposited. Microstructural and structural analysis of the coatings confirmed nanocrystalline morphology with peaks corresponding to crystallographic planes of (002), (111), (020), and (022). Deposited coatings are hydrophilic in nature. The microhardness of the coatings is decreased with an increase in the number of layers deposited. © © 2023 Elsevier Ltd. All rights reserved.Item Microstructure Evolution in Cast Al-Zn-Mg Alloys Processed by Equal Channel Angular Pressing(Springer New York LLC barbara.b.bertram@gsk.com, 2018) Manjunath, G.K.; Udaya Bhat, K.; Preetham Kumar, G.V.In the present work, microstructure development and enhancement in the microhardness of Al-Zn-Mg alloys (with 5, 10, and 15% zinc) during equal channel angular pressing (ECAP) were investigated. Dendritic morphology was observed in the cast condition of all three alloys, and precipitates were situated along the inter-dendritic regions. After homogenization, precipitates in the inter-dendritic regions were uniformly distributed in the aluminum matrix and grain boundaries were developed. After 4 passes in route BC, large reduction in the grain size was observed. X-ray diffractometry showed that MgZn2 precipitate was developed in the ECAP-processed samples. Increase in the intensity of MgZn2 peaks was observed when the quantity of zinc is increased in the material. Also, changes in the intensity of XRD peaks were observed in ECAP-processed samples due to shear deformation. After ECAP, substantial increase in the microhardness was perceived. After four passes, microhardness increased to 109, 67, and 58% from the initial condition in A1, A2, and A3 alloys, respectively. Also, improvement in the microhardness was also observed when the quantity of zinc is increased in the material. © 2017, Springer Science+Business Media, LLC, part of Springer Nature and ASM International.Item Effect of Retrogression Heat Treatment Time on Microstructure and Mechanical Properties of AA7010(Springer New York LLC barbara.b.bertram@gsk.com, 2018) Nandana, M.S.; Udaya Bhat, K.; Manjunatha, C.M.The effect of retrogression time during retrogression and re-aging (RRA) treatment of AA7010 is evaluated by performing tensile tests and characterizing the microchemistry of the grain boundary precipitates (GBPs) using transmission electron microscope coupled with the energy-dispersive spectroscopy. Retrogression time is evaluated so that the ultimate tensile strength of the RRA-treated sample is equal to that of the T6-treated sample and the grain boundary microstructure similar to that of the over-aged (T7451) condition. The investigation reveals that the sample retrogressed at 200 °C for 20 min has UTS of 586 MPa which is equivalent to that of the T6 sample and 11.5% higher than that of the T7451 condition. The fracture toughness of the RRA-treated sample was 41 MPa?m. Microstructure of the RRA-treated sample is similar to T7451, along the grain boundaries and in the grain interior similar to that of the T6-treated sample. Energy-dispersive spectroscopy confirmed the increment of Cu content on the GBP’s with increase in the retrogression time, which is expected to improve the stress corrosion cracking resistance of the alloy. © 2018, ASM International.Item Microstructure and Mechanical Properties of Cast Al-5Zn-2Mg Alloy Subjected to Equal-Channel Angular Pressing(Springer New York LLC barbara.b.bertram@gsk.com, 2018) Manjunath, G.K.; Preetham Kumar, G.V.P.; Udaya Bhat, K.; Huilgol, P.In the present work, cast Al-5Zn-2Mg alloy was processed through equal-channel angular pressing (ECAP) in route BC up to four number of passes. Microstructure and mechanical properties were investigated on processed and unprocessed materials. In cast condition, the material was composed of dendritic structure. After homogenization treatment, large-sized grains were observed. After ECAP processing, significant grain refinement was observed. After ECAP processing, high-density dislocations and high degree of misorientation between the grains were observed. In cast material, rod-shaped precipitates were observed, while, after ECAP processing, spherical-shaped precipitates were observed. ECAP processing leads to a noticeable improvement in the mechanical properties of the material. After four passes, 122% improvement in the microhardness and 135% improvement in the ultimate tensile strength of the material were observed. After three passes, a slight decrease in the mechanical properties was observed. This is attributed to the dissolution of the metastable ?? phase, annihilation of dislocations, dynamic recrystallization and texturing during ECAP processing. Brittle fracture mode was observed in tensile testing cast and homogenized samples. After ECAP processing, fracture mode was changed into shear fracture mode. © 2018, ASM International.Item Effect of zinc content on the microstructure and mechanical properties of Al-Zn-Mg alloy(Elsevier Ltd, 2022) Manjunath, G.K.; Udaya Bhat, K.; Preetham Kumar, G.V.In the present work, Aluminium-Zinc-Magnesium alloys (5 wt%, 10 wt% and 15 wt% Zinc and 2 wt% Magnesium) were prepared by casting process in a metal die. After casting process, heat treatment was conducted to the prepared alloys. To study the consequence of Zinc on the prepared alloys microstructure and mechanical properties were investigated. In as-cast state, in all three compositions, dendrite formation was noticed. While, after homogenization heat treatment, grain boundaries were noticed. Rise in the Zinc in the material leads to enhance the secondary particles. Microhardness and tension experiments were conducted to investigate the mechanical properties. Rise in the Zinc in the material leads to enhance the microhardness and tension strength. But ductility of the material declined with rise in the Zinc in the material. © 2021Item Degradation response and bioactivity assessment of antimicrobial copper coatings in simulated hand sweat environment(Elsevier B.V., 2022) Bharadishettar, N.; Udaya Bhat, K.The antimicrobial copper coatings were deposited on AISI 304 stainless steel (SS) using electrodeposition technique for touch surface applications. Electrodeposition was performed using a non-cyanide electrolyte, with varying copper concentrations. The copper coatings were investigated for their microstructure, in vitro degradation in the simulated hand sweat environment, and antimicrobial activity in an agar medium. It is noted that all the coatings have nanostructures in their microstructure. The microstructure of the coatings along with the contact period with the bacteria affects the antimicrobial activity measured against Escherichia coli and Staphylococcus aureus. The nanostructured morphology has resulted in an increased surface area with enhanced copper toxicity. The degradation behavior of coatings in the simulated hand sweat solution was further probed using potentiodynamic polarization test and electrochemical impedance spectroscopy (EIS). © 2022 Elsevier B.V.