Faculty Publications
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Item Deep cryogenic treatment of plain-carbon and low-alloy steels(ASTM International service@astm.org, 2020) Sondar, P.R.; Hegde, S.R.To improve the mechanical properties of steels, cryogenic treatment is often carried out as an intermediate step between quenching and tempering. The transformation of retained austenite into martensite is the main objective and principle behind the cryogenic treatment. Generally, high-alloy and high-carbon steels are subjected to cryogenic treatment, as they produce a high fraction of retained austenite during quenching as compared with low- and medium-alloy steels. This work analyses the effect of cryogenic treatment on EN8, a plain-carbon steel, and EN47, a low-alloy steel, through microstructural characterization, hardness measurements, and tensile tests. The work shows that influence of cryogenic treatment carried out after tempering is only marginal, whereas cryogenic treatment carried out before tempering yields much better mechanical properties. Experimental results obtained in this work confirm that EN47 responds slightly better than EN8 suggesting that low-alloying additions influence the cryogenic treatment of steels. This work established that by properly applying cryogenic treatment, the strength and hardness of both EN8 and EN47 steels can be increased by about 50 MPa and 3 HRC, respectively, as compared with conventional hardening and tempering treatment. © 2021 ASTM International. All rights reserved.Item Failure Analysis of Cooling Tower Fan-Arm(Springer, 2020) Padasale, B.; Kumar, J.K.R.; Sondar, P.R.; Cadambi, S.; Hegde, S.R.This work presents failure investigation of cooling tower fan-arms commissioned in a chemical processing plant. The analysis aims at understanding the mechanism and root-cause of the failure. The investigation involves site visits, microstructural analysis, fracture surface analysis, hardness measurements, numerical stress analysis and experimental simulation. Work concludes that the fan-arms failed due to the lack of post-weld heat treatment, which caused localized stress-corrosion and pitting at critical locations that served as crack initiation sites. Fatigue loading condition and presence of residual stresses at the weld enabled easy propagation of cracks that led to recurring premature failure. Based on the root-cause and the mechanism identified in this analysis, proper pre-heating and post-weld heat treatment is recommended to relieve the residual stresses at the critical locations and thus to avoid/minimize such recurring failures in future. © 2020, ASM International.Item Failure of a Cooling Water Pump Shaft(Springer, 2021) Sondar, P.R.; Kumar, J.K.R.; Chawla, S.; Dsilva, P.C.; Hegde, S.R.This study investigates the failure of an industrial cooling water pump which experienced a drive shaft failure. As per the fail-safe design, during adverse loading of the shaft, key should fail by shear. The key, if fails, can be easily replaced to resume the operation of the pump. However, this investigation reveals that both the key and the shaft failed due to materials processing issues. A detailed failure analysis was carried out including design calculations, visual inspection, dye penetrant inspection, magnetic particle inspection, hardness test, microstructural analysis, and fractography. The study found that the hardness of the shaft varied radially from the core to the surface. The subsurface of the shaft near the keyway, happened to be significantly softer than the key. During operation, the keyway widened by plastic deformation and caused rattling of the key. Due to rattling and vibration, the key developed numerous fatigue cracks and eventually failed by crack linkages. The shaft eventually failed by torsional shear near the midpoint of the keyway. The analysis adjudged hardness variation in the shaft due to materials processing issues as the root cause of the failure. © ASM International 2020.Item Effect of spheroidization of cementite in ductile cast iron(University of Science and Technology Beijing, 2021) Basavaraj; Sondar, P.R.; Hegde, S.R.The research aims to provide an alternative to austempering treatment of ductile cast iron with a simple and cost-effective heat-treatment process. This goal was accomplished by applying a simple one-step spheroidization heat treatment to the as-cast ductile iron, which would normally possess a coarse pearlitic microstructure to a significant extent. Spheroidization experiments involving isothermal holding below the lower critical temperature (A1) were conducted followed by standard mechanical testing and microstructural characterization for an experimental ductile iron. After improving the spheroidization holding time at a given temperature, the work shows that the ductility and toughness of an as-cast ductile iron can be improved by 90% and 40%, respectively, at the cost of reducing the tensile strength by 8%. Controlled discretization of the continuous cementite network in pearlitic matrix of the ductile iron is deemed responsible for the improved properties. The work also shows that prolonged holding time during spheroidization heat treatment leads to degradation of mechanical properties due to the inhomogenous microstructure formation caused by heterogeneous decomposition and cementite clustering in the material. The main outcome of this work is the demonstration of ductile cast iron’s necking behavior due to spheroidization heat treatment. © 2020, University of Science and Technology Beijing and Springer-Verlag GmbH Germany, part of Springer Nature.Item Catastrophic failure of urea prill-tower fan(Elsevier Ltd, 2021) Hegde, S.R.; Rakshan Kumar, J.K.; Sondar, P.R.; Dsilva, P.C.This work presents failure investigation of a prill-tower fan that was in service for about 20 years in a urea plant. All the fan-blades and the plummer blocks fractured catastrophically during the plant-operation, shocked the plant personnel, and caused a huge shutdown loss. Standard failure analysis procedure involving: site visit, visual inspection, microstructural analysis, fracture analysis, analytical stress calculation and FEM analysis was followed. The investigation confirms that the fan-blades having numerous dents and nicks were operating in a mild corrosive atmosphere of ammonium hydroxide. The fracture analysis suggests that a pre-existing dent on the trailing edge of a blade corroded to form a pre-crack that aligned perpendicular to the long axis of the blade. When the pre-crack grew to a critical size, a small chunk of the blade fractured from the vicinity and ejected towards the blade-tip by centrifugal force. Because of confined space around the fan and limited blade-tip clearance, this triggered a chain reaction of blade fracture and rattled the entire array of fan-blades. The analysis establishes that the plummer blocks failed due to mechanical imbalance of the fan-shaft caused by the blade failure. The investigation concludes that presence of dents and nicks on the fan-blades is the root-cause for this catastrophic failure. Grinding-off of the surface defects to eliminate stress raisers is recommended for averting such a failure in future. © 2020 Elsevier LtdItem Failure Analysis of a Bucket Elevator Shaft(Springer, 2021) Gurudath, B.; Kumawat, K.K.; Tejaswi, V.; Sondar, P.R.; Rakshan Kumar, J.K.; Hegde, S.R.Present work investigates the in-service break down of a bucket elevator in a chemical processing plant. The elevator was used for lifting bulk Di-Ammonium Phosphate and broke down due to premature failure of a shaft made of EN19 steel. The investigation comprises a detailed metallurgical failure analysis involving site visit, visual inspection, fractography, and metallography. The investigation reveals that, about 2 years prior to the failure, the shaft was tack-welded to the sprocket hub and a gib-head key near the keyway to avoid the frequent loosening of the key. The inspection during the site visit confirms that the shaft-sprocket assembly was subjected to in-service jerky loading condition along with uneven stress distribution due to misaligned counterweight. The investigation concludes that a crack was initiated in the shaft at the heat affected zone of the tack-welded spot, propagated transversely by fatigue due to in-service cyclic loading, and terminated catastrophically by a brittle fracture during the service. Tack welding, coupled with uneven stress distribution in the shaft due to misaligned counterweight system, is adjudged the root cause of this failure. Suitable remedial measures are suggested to avoid such a failure in the future. © 2021, ASM International.Item Failure Analysis of Reciprocating CO2 Compressor(Springer, 2021) Dsilva, P.C.; Shetty, P.; Sondar, P.R.; Ganesh Kumar, B.; Hegde, S.R.This work presents failure analysis of a heavy-duty, four-stage, double-action, reciprocating CO2 compressor, which resulted in the shutdown of an ammonia plant. The failure occurred in the fourth stage of the compressor, during which the piston rod, piston rings, a suction valve, and associated valve cage are found fractured. The failure analysis includes details of site visit, visual inspection, dye penetrant test, fractography, and microstructural analysis. Furthermore, Xanthoproteic test was conducted on the extracts of the failed piston rings that confirmed the presence of bacterial cellular protein. When the morphology of the failed piston ring was studied using a scanning electron microscope, unique degradation features and the presence of bacterial metabolic products were observed conforming to the growth of bacteria. In-service biodegradation of the piston ring material (polyether ether ketone composite) is adjudged as the root cause for the compressor failure. © 2021, ASM International.Item Biodegradation of PEEK Piston Rings(Elsevier Ltd, 2021) Shetty, P.; Dsilva, P.; Sondar, P.R.; Kumar, B.G.; Hegde, S.Polyether ether ketone (PEEK) is considered a high performance thermoplastic with excellent mechanical, chemical, and thermal properties. It is generally believed that this material is chemically and biologically inert, and is used for various biomedical and industrial applications, especially in the form of fiber reinforced polymeric composites. Contrary to the general belief, the present work reports the biodegradation of PEEK piston rings that were used in a reciprocating CO2 compressor. A series of circumstantial and direct evidences were collected by following various tests and characterization methods to confirm the degradation of the piston rings by bacterial attack. The bacterial cells were extracted from the degraded piston rings, cultured in agar medium and then studied using scanning electron microscope. An experimental simulation was carried out by depositing and incubating a bacterial culture on the pristine surface of a PEEK specimen. The simulation experiment revealed an early stage of bacterial degradation in the form of cracking of the PEEK specimen surface. The results of various tests, characterization, and the experimental simulation presented in the paper suggest that PEEK based composites degrade due to enzymatic hydrolysis process by Myxococcus Xanthus, the rod–shaped soil bacteria. © 2021Item Study on low-frequency dielectric behavior of the carbon black/polymer nanocomposite(Springer, 2021) Hiremath, H.; Mathias, K.A.; Sondar, P.R.; Shrishail, M.H.; Kulkarni, S.M.Recently, polymer-based dielectric materials have become one of the key materials to play an essential role in clean energy production, energy transformation, and energy storage applications. The end usage is the energy storage capability because it is a trade-off between dielectric permittivity, dielectric loss, and dissipation factor. Hence, it is of prime importance to study the dielectric properties of polymer materials by adding filler material at a low-frequency range. In the present study, polydimethylsiloxane/carbon black nanocomposites are prepared using the solution cast method. The dielectric properties, such as dielectric constant, dielectric loss, and dissipation factors due to the concentration of filler particles and low-frequency effect on the nanocomposites, are examined. Also, different empirical models are used to estimate the dielectric permittivity of polymer nanocomposites. The low-frequency range of 100 Hz to 1 MHz and the effect of varying volume fractions of carbon black show a significant change in the dielectric properties. It is found that the nanocomposites have a higher dielectric permittivity than the base polymer material. It is also observed that an increase in filler concentration increases the dielectric permittivity, which is confirmed with an empirical model. © 2021, The Author(s).Item Failure of hydraulic lathe chuck assembly(Elsevier Ltd, 2022) Sondar, P.R.; Gurudath, B.; Ahirwar, V.; Hegde, S.R.Present work provides a detailed failure investigation of a hydraulic lathe chuck assembly that comprises a plunger, three jaws, and three jaw-carriers that are made of carburized, tempered and sub-zero treated EN36C steel. The chuck assembly suffered premature failure of the plunger and one of the jaw carriers during the service in a CNC lathe. The investigation comprises a detailed metallurgical failure analysis involving: visual inspection, fractography, metallography, and hardness measurements. The analysis concludes that plunger failed first by fatigue fracture that is originated at a sharp corner of a T-slot. The mating jaw-carrier failed in the next event due to instant misalignment and overstressing during the lathe operation. The investigation concludes that design flaw and improper heat treatment cycle as the reasons for the premature failure of the assembly. Through experimental simulation of the heat-treatment cycles using EN36C specimens, the work suggests that carburizing, cryogenic treatment and then tempering is the proper sequence for achieving the best combination of mechanical properties that should extend the service life of the chuck-assembly. © 2021 Elsevier Ltd