Faculty Publications
Permanent URI for this communityhttps://idr.nitk.ac.in/handle/123456789/18736
Publications by NITK Faculty
Browse
6 results
Search Results
Item Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2016) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.Magnesium alloy Mg-Al-Mn (AM70) was processed by equal channel angular pressing (ECAP) at 275 °C for up to 4 passes in order to produce ultrafine-grained microstructure and improve its mechanical properties. ECAP-processed samples were characterized for microstructural analysis using optical microscopy, scanning electron microscopy, and transmission electron microscopy. Microstructural analysis showed that, with an increase in the number of ECAP passes, grains refined and grain size reduced from an average of 45 to 1 µm. Electron backscatter diffraction analysis showed the transition from low angle grain boundaries to high angle grain boundaries in ECAP 4 pass sample as compared to as-cast sample. The strength and hardness values an showed increasing trend for the initial 2 passes of ECAP processing and then started decreasing with further increase in the number of ECAP passes, even though the grain size continued to decrease in all the successive ECAP passes. However, the strength and hardness values still remained quite high when compared to the initial condition. This behavior was found to be correlated with texture modification in the material as a result of ECAP processing. © 2016, ASM International.Item Effect of multiaxial cryoforging on microstructure and mechanical properties of a Cu-Ti Alloy(Institute of Physics Publishing helen.craven@iop.org, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Gopi, K.R.; Sahu, S.Cu-Ti alloy, processed by multiaxial forging (MAF) at cryogenic temperature with a cumulative strain up to 1.64, was investigated for microstructure and mechanical properties. The deformed microstructures were analyzed using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The average grain size of 2 ?m was achieved in the deformed sample after 3 cycles of MAF. TEM studies indicated that the shear bands width of the deformed sample after 3 cycles reduced to 1 ?m. Tests for mechanical properties indicated an increase in tensile strength and hardness and it was found to be correlated with an increase in dislocation density and grain boundary strengthening mechanism. Ultimate tensile strength (UTS) of 390 MPa, 480 MPa, and 590 MPa was observed in MAF processed samples after 1, 2, and 3 cycles, respectively. Hardness increased from 65 Hv (as-received) to 240 Hv after 3 cycles of MAF. Fractography analysis showed that, with an increase in number of MAF cycles, dimple size reduced up to 1 cycle and percentage elongation increased after 2 cycles of MAF. © 2018 IOP Publishing Ltd.Item Influence of Multidirectional Forging on Microstructural, Mechanical, and Corrosion Behavior of Mg-Zn Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.Multidirectional forging (MDF) was applied to Mg-6%Zn alloy up to 5 passes successfully at 280 °C. MDF-processed materials were characterized using optical microscope, scanning electron microscope, electron backscatter diffraction, transmission electron microscope, and x-ray diffraction. Obtained results showed a significant reduction in grain size (up to 3.8 ?m) having a large fraction of high-angle grain boundaries after 5 passes of MDF process. Maximum tensile strength of 230 MPa was achieved for 5-pass MDF-processed Mg-6%Zn alloy which is about ~ 2.0 times higher in comparison with that of homogenized alloy (117 MPa) and was attributed to higher dislocations density and grain refinement. Corrosion behavior of the alloy was investigated in 0.1 M NaCl solution using potentiodynamic polarization test, electrochemical impedance spectra analysis, and immersion tests. It was found that the corrosion rate of 5-pass MDF sample improved (0.34 mm/year) ~2.5 times in comparison with that of homogenized Mg-6%Zn alloy (0.86 mm/year) due to fine grain structure, which creates more grain boundaries that act as a corrosion barrier. © 2019, ASM International.Item Investigation of dry sliding wear properties of multi-directional forged Mg–Zn alloys(National Engg. Reaserch Center for Magnesium Alloys zhangdingfei@cqu.edu.cn, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.Effect of multi-directional forging (MDF) on wear properties of Mg–Zn alloys (with 2, 4, and 6 wt% Zn) is investigated. Dry sliding wear test was performed using pin on disk machine on MDF processed and homogenized samples. Wear behavior of samples was analyzed at loads of 10 N and 20 N, with sliding distances of 2000 m and 4000 m, at a sliding velocity of 3 m/s. Microstructures of worn samples were observed under scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and x-ray diffraction (XRD) and the results were analyzed. Mechanical properties were evaluated using microhardness test. After 5 passes of MDF, the average grain size was found to be 30 ± 4 µm, 22 ± 3 µm, and 18 ± 3 µm, in Mg–2%Zn, Mg–4%Zn, and Mg–6%Zn alloys, respectively, with significant improvement in hardness in all cases. Wear resistance was improved after MDF processing, as well as, with increment in Zn content in Mg alloy. However, it decreased when the load and the sliding distance increased. Worn surface exhibited ploughing, delamination, plastic deformation, and wear debris along sliding direction, and abrasive wear was found to be the main mechanism. © 2019Item Influence of Multiaxial Cryoforging on Microstructural, Mechanical, and Corrosion Properties of Copper-Titanium Alloy(Springer, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Sahu, S.; Gopi, K.R.; Shivaram, M.J.; Arya, S.Multiaxial forging (MAF) was used to process Cu-4.5%Ti (wt.%) alloy at cryogenic temperature up to three cycles with a cumulative strain of 1.64. Microstructures, mechanical, and corrosion properties of as-received and deformed samples were analyzed. Microstructural analysis showed that average grain size decreased from 70 µm to 200 nm, and electron backscattered diffraction (EBSD) analysis revealed the transformation of high-angle grain boundaries (HAGBs) to low-angle grain boundaries (LAGBs). Variations in intensity of peaks were observed by x-ray diffraction (XRD) technique. Microstructural investigation showed elongated grains with shear bands having width ~ 200 nm for 3-cycle sample. Tensile testing and micro-hardness tests showed improvements in ultimate tensile strength (UTS), yield strength (YS), and micro-hardness, with the increase in MAF cycles. Ultimate tensile strength and hardness increased from 605 MPa and 252 HV (for as-received) to 1284 MPa and 428 HV for three cycles of MAF-processed sample, respectively. Improvement in strength and hardness was attributed to refined grain structure. Corrosion study was carried out for different cycles of MAF-processed samples using potentiodynamic polarization, and corroded surfaces were analyzed using scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS) analysis. © 2019, ASM International.Item Investigation of Tribological Characteristics of Cu-Ti Alloys Processed by Multi-Axial Cryo-Forging(Springer, 2022) Ramesh, S.; Shivananda Nayaka, H.S.; Anne, G.; Arun, M.N.; Naik, G.M.Cu-XTi alloys (X = 1.5 and 4.5%) were subjected to multi-axial forging (MAF) under cryogenic condition up to three passes successfully. Characteristics of the MAF-processed alloys were analyzed using microstructural analysis, hardness and wear tests. Worn surface morphology and elemental analysis was performed by scanning electron microscopy. The hardness of samples increases with higher MAF passes due to strain hardening and grain refinement. Wear test was done for six various sliding distances (500, 1000, 1500, 2000, 2500 and 3000 m), two different loads (10 and 20 N), and two different velocities (1 and 2 m/s) using the pin-on-disk wear test rig. Wear loss of as-received samples is higher than MAF-pressed samples due to an increase in hardness, but wear loss increases as the load increases. Coefficient of friction is reduced with the increase in MAF pass, which is due to strain hardening effect. The worn surface exhibits the plastic deformation regions, delamination, plowing and formation of oxide layers, which was revealed by energy-dispersive X-ray spectroscopy analysis. Also, MAF-processed samples exhibited abrasive wear mechanism as a result of formation of oxygen layer as revealed in SEM micrographs. © 2022, ASM International.