Faculty Publications
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Item Influence of Multi Axial Forging (MAF) on Microstructure and Mechanical Properties of Cu-Ti Alloy(Elsevier Ltd, 2018) Ramesh, S.; Shivananda Nayaka, H.S.; Gopi, K.R.Multi axial forging (MAF) is one among the severe plastic deformation (SPD) processes, where large strains are imposed into the component. In the present work, as-received Cu-1.5%Ti alloy was subjected to MAF for 2 and 4 cycles at room temperature. Microstructure showed grain refinement after 2 and 4 cycles. Average grain size obtained for MAF processed samples after 2 and 4 cycles are 120 μm and 40 μm, respectively compared to initial grain size of 800 μm. The Mechanical properties were analyzed for as-received and MAF processed samples. Tensile test showed increased ultimate tensile strength (493 MPa) for MAF 4-cycle sample compared to as-received (191 MPa) condition with accumulated strain of 2.18 for 4 cycles. Increase in hardness was observed for MAF processed sample of 143 Hv for 4-cycle compared to as-received sample of 67 Hv. © 2018 Elsevier Ltd.Item Microstructural and mechanical characterisation of Al-Zn-Mg-Cu alloy processed by multi-directional cryo-forging(Elsevier Ltd, 2021) Ramesh, S.; Anne, G.; Naik, G.M.; Jagadeesh, C.; Shivananda Nayaka, H.S.Aim of the present investigation is to study the microstructural and mechanical properties of Al-Zn-Mg-Cu alloy before and after multi-direction forging (MDF) at cryogenic condition up to 3 cycles. Microstructure evolution of specimen was examined using optical microscope and orientation imaging microscopy as well as X-ray diffraction. Mechanical properties were measured by tensile test and Vickers micro hardness. Microstructural investigation shows that after 3 cycle of MDF average grain size was reduced to 8 μm with low angle grain boundaries (LAGBs) and high dislocation density. Mechanical examination displays an improvement in hardness, yield strength and ultimate tensile strength is due to increases in grain boundaries and strain hardening effect. After 3 cycles of MDF process with cumulative strain ςΔϵ = 3.64 led to the formation of fine grain structure, and microhardness were observed to be 168 HV. © 2021 Elsevier Ltd. All rights reserved.Item A review on wrought magnesium alloys processed by equal channel angular pressing(Inderscience Publishers, 2015) Muralidhar, M.; Narendranath, S.; Shivananda Nayaka, H.S.Magnesium and its alloys with severe plastic deformation (SPD) techniques are more attractive as structural parts in many industrial applications because of their advantages. In this paper, the importance of wrought magnesium alloys with their applications to accomplish the essential development of components is reviewed. In addition, the different approaches of equal channel angular pressing (ECAP) process for refining the grain size to achieve the ultrafine grained material on the bulk metals are discussed. Recent developments in the ECAP process are outlined clearly with their importance to overcome many complexities. Various factors like processing temperature of a specimen, die geometry, ram speed, back pressure and processing routes influencing during ECAP process of wrought magnesium alloys at different conditions such as channel angle and corner or outer arc angle are discussed. Finally, the properties of ECAP processed wrought alloys are outlined for improving the microstructure in structural parts. © © 2015 Inderscience Enterprises Ltd.Item Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2016) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.Magnesium alloy Mg-Al-Mn (AM70) was processed by equal channel angular pressing (ECAP) at 275 °C for up to 4 passes in order to produce ultrafine-grained microstructure and improve its mechanical properties. ECAP-processed samples were characterized for microstructural analysis using optical microscopy, scanning electron microscopy, and transmission electron microscopy. Microstructural analysis showed that, with an increase in the number of ECAP passes, grains refined and grain size reduced from an average of 45 to 1 µm. Electron backscatter diffraction analysis showed the transition from low angle grain boundaries to high angle grain boundaries in ECAP 4 pass sample as compared to as-cast sample. The strength and hardness values an showed increasing trend for the initial 2 passes of ECAP processing and then started decreasing with further increase in the number of ECAP passes, even though the grain size continued to decrease in all the successive ECAP passes. However, the strength and hardness values still remained quite high when compared to the initial condition. This behavior was found to be correlated with texture modification in the material as a result of ECAP processing. © 2016, ASM International.Item Microstructural Evolution and Strengthening of AM90 Magnesium Alloy Processed by ECAP(Springer Verlag, 2017) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.Equal-channel angular pressing (ECAP) was applied on AM90 magnesium alloy using processing route B C at 275?C up to four passes. Microstructural evolution and the corresponding modification in mechanical properties (strength, elongation and hardness) corresponding to the number of ECAP passes were evaluated using X-ray diffraction (XRD), electron backscatter diffraction, scanning electron microscopy, transmission electron microscopy, tensile test and microhardness test. Shear deformation was found to refine the microstructure by breaking it into smaller grains formed by dislocation reconstruction. Tensile strength and hardness were found to increase by ? 128 and 23%, respectively, for ECAP-processed 2-pass sample in comparison with that of the homogenized condition. After two passes, tensile strength and hardness started decreasing even though the grain size was still decreasing, which was found to be associated with texture modification during ECAP processing as observed by XRD analysis. © 2017, King Fahd University of Petroleum & Minerals.Item Effect of multiaxial cryoforging on microstructure and mechanical properties of a Cu-Ti Alloy(Institute of Physics Publishing helen.craven@iop.org, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Gopi, K.R.; Sahu, S.Cu-Ti alloy, processed by multiaxial forging (MAF) at cryogenic temperature with a cumulative strain up to 1.64, was investigated for microstructure and mechanical properties. The deformed microstructures were analyzed using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The average grain size of 2 ?m was achieved in the deformed sample after 3 cycles of MAF. TEM studies indicated that the shear bands width of the deformed sample after 3 cycles reduced to 1 ?m. Tests for mechanical properties indicated an increase in tensile strength and hardness and it was found to be correlated with an increase in dislocation density and grain boundary strengthening mechanism. Ultimate tensile strength (UTS) of 390 MPa, 480 MPa, and 590 MPa was observed in MAF processed samples after 1, 2, and 3 cycles, respectively. Hardness increased from 65 Hv (as-received) to 240 Hv after 3 cycles of MAF. Fractography analysis showed that, with an increase in number of MAF cycles, dimple size reduced up to 1 cycle and percentage elongation increased after 2 cycles of MAF. © 2018 IOP Publishing Ltd.Item Influence of Multidirectional Forging on Microstructural, Mechanical, and Corrosion Behavior of Mg-Zn Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.Multidirectional forging (MDF) was applied to Mg-6%Zn alloy up to 5 passes successfully at 280 °C. MDF-processed materials were characterized using optical microscope, scanning electron microscope, electron backscatter diffraction, transmission electron microscope, and x-ray diffraction. Obtained results showed a significant reduction in grain size (up to 3.8 ?m) having a large fraction of high-angle grain boundaries after 5 passes of MDF process. Maximum tensile strength of 230 MPa was achieved for 5-pass MDF-processed Mg-6%Zn alloy which is about ~ 2.0 times higher in comparison with that of homogenized alloy (117 MPa) and was attributed to higher dislocations density and grain refinement. Corrosion behavior of the alloy was investigated in 0.1 M NaCl solution using potentiodynamic polarization test, electrochemical impedance spectra analysis, and immersion tests. It was found that the corrosion rate of 5-pass MDF sample improved (0.34 mm/year) ~2.5 times in comparison with that of homogenized Mg-6%Zn alloy (0.86 mm/year) due to fine grain structure, which creates more grain boundaries that act as a corrosion barrier. © 2019, ASM International.Item Influence of Multiaxial Cryoforging on Microstructural, Mechanical, and Corrosion Properties of Copper-Titanium Alloy(Springer, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Sahu, S.; Gopi, K.R.; Shivaram, M.J.; Arya, S.Multiaxial forging (MAF) was used to process Cu-4.5%Ti (wt.%) alloy at cryogenic temperature up to three cycles with a cumulative strain of 1.64. Microstructures, mechanical, and corrosion properties of as-received and deformed samples were analyzed. Microstructural analysis showed that average grain size decreased from 70 µm to 200 nm, and electron backscattered diffraction (EBSD) analysis revealed the transformation of high-angle grain boundaries (HAGBs) to low-angle grain boundaries (LAGBs). Variations in intensity of peaks were observed by x-ray diffraction (XRD) technique. Microstructural investigation showed elongated grains with shear bands having width ~ 200 nm for 3-cycle sample. Tensile testing and micro-hardness tests showed improvements in ultimate tensile strength (UTS), yield strength (YS), and micro-hardness, with the increase in MAF cycles. Ultimate tensile strength and hardness increased from 605 MPa and 252 HV (for as-received) to 1284 MPa and 428 HV for three cycles of MAF-processed sample, respectively. Improvement in strength and hardness was attributed to refined grain structure. Corrosion study was carried out for different cycles of MAF-processed samples using potentiodynamic polarization, and corroded surfaces were analyzed using scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS) analysis. © 2019, ASM International.