Faculty Publications
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Item Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2016) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.Magnesium alloy Mg-Al-Mn (AM70) was processed by equal channel angular pressing (ECAP) at 275 °C for up to 4 passes in order to produce ultrafine-grained microstructure and improve its mechanical properties. ECAP-processed samples were characterized for microstructural analysis using optical microscopy, scanning electron microscopy, and transmission electron microscopy. Microstructural analysis showed that, with an increase in the number of ECAP passes, grains refined and grain size reduced from an average of 45 to 1 µm. Electron backscatter diffraction analysis showed the transition from low angle grain boundaries to high angle grain boundaries in ECAP 4 pass sample as compared to as-cast sample. The strength and hardness values an showed increasing trend for the initial 2 passes of ECAP processing and then started decreasing with further increase in the number of ECAP passes, even though the grain size continued to decrease in all the successive ECAP passes. However, the strength and hardness values still remained quite high when compared to the initial condition. This behavior was found to be correlated with texture modification in the material as a result of ECAP processing. © 2016, ASM International.Item Effect of multiaxial cryoforging on microstructure and mechanical properties of a Cu-Ti Alloy(Institute of Physics Publishing helen.craven@iop.org, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Gopi, K.R.; Sahu, S.Cu-Ti alloy, processed by multiaxial forging (MAF) at cryogenic temperature with a cumulative strain up to 1.64, was investigated for microstructure and mechanical properties. The deformed microstructures were analyzed using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The average grain size of 2 ?m was achieved in the deformed sample after 3 cycles of MAF. TEM studies indicated that the shear bands width of the deformed sample after 3 cycles reduced to 1 ?m. Tests for mechanical properties indicated an increase in tensile strength and hardness and it was found to be correlated with an increase in dislocation density and grain boundary strengthening mechanism. Ultimate tensile strength (UTS) of 390 MPa, 480 MPa, and 590 MPa was observed in MAF processed samples after 1, 2, and 3 cycles, respectively. Hardness increased from 65 Hv (as-received) to 240 Hv after 3 cycles of MAF. Fractography analysis showed that, with an increase in number of MAF cycles, dimple size reduced up to 1 cycle and percentage elongation increased after 2 cycles of MAF. © 2018 IOP Publishing Ltd.Item Influence of Multidirectional Forging on Microstructural, Mechanical, and Corrosion Behavior of Mg-Zn Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.Multidirectional forging (MDF) was applied to Mg-6%Zn alloy up to 5 passes successfully at 280 °C. MDF-processed materials were characterized using optical microscope, scanning electron microscope, electron backscatter diffraction, transmission electron microscope, and x-ray diffraction. Obtained results showed a significant reduction in grain size (up to 3.8 ?m) having a large fraction of high-angle grain boundaries after 5 passes of MDF process. Maximum tensile strength of 230 MPa was achieved for 5-pass MDF-processed Mg-6%Zn alloy which is about ~ 2.0 times higher in comparison with that of homogenized alloy (117 MPa) and was attributed to higher dislocations density and grain refinement. Corrosion behavior of the alloy was investigated in 0.1 M NaCl solution using potentiodynamic polarization test, electrochemical impedance spectra analysis, and immersion tests. It was found that the corrosion rate of 5-pass MDF sample improved (0.34 mm/year) ~2.5 times in comparison with that of homogenized Mg-6%Zn alloy (0.86 mm/year) due to fine grain structure, which creates more grain boundaries that act as a corrosion barrier. © 2019, ASM International.Item Influence of equal channel angular pressing and laser shock peening on fatigue behaviour of AM80 alloy(Elsevier B.V., 2019) Praveen, T.R.; Shivananda Nayaka, H.S.; Swaroop, S.AM80 magnesium alloy was processed with Equal Channel Angular Press (ECAP)for grain refinement. Laser shock peening without coating (LSPwC)were executed on ECAP processed sample at 8 GW cm?2 and further grain refinement were observed at surface. SEM image expose the grain refinement at different stage of processing, and fine grains of sub-micron size were observed at surface level after ECAP + LSPwC. Residual stress were measured using X-ray diffraction, sin2(?)method and compressive residual stress was found after ECAP. LSPwC intensify the compressive residual stress at surface. Increases in magnitude of residual stresses were noticed with 200 and 300% of LSPwC. Increase in surface roughness were noticed from 0.6 to 6.8 ?m by increasing the percentage of LSPwC coverage. Fatigue tests were acknowledged the effect of ECAP and ECAP + LSPwC on reliability of grain refinement technique. ECAP sample showed fatigue life of 7539 cycles against as received. Highest fatigue life of 85,268 life cycles was observed with ECAP + LSPwC by 100% of coverage. Further process of LSPwC for 200 and 300%, fatigue life was significantly decreases to 22,987 and 384 cycles respectively. SEM images of fractured surface exhibits effect of ECAP and LSPwC on crack initiation and propagation for failure. © 2019 Elsevier B.V.Item Influence of Multiaxial Cryoforging on Microstructural, Mechanical, and Corrosion Properties of Copper-Titanium Alloy(Springer, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Sahu, S.; Gopi, K.R.; Shivaram, M.J.; Arya, S.Multiaxial forging (MAF) was used to process Cu-4.5%Ti (wt.%) alloy at cryogenic temperature up to three cycles with a cumulative strain of 1.64. Microstructures, mechanical, and corrosion properties of as-received and deformed samples were analyzed. Microstructural analysis showed that average grain size decreased from 70 µm to 200 nm, and electron backscattered diffraction (EBSD) analysis revealed the transformation of high-angle grain boundaries (HAGBs) to low-angle grain boundaries (LAGBs). Variations in intensity of peaks were observed by x-ray diffraction (XRD) technique. Microstructural investigation showed elongated grains with shear bands having width ~ 200 nm for 3-cycle sample. Tensile testing and micro-hardness tests showed improvements in ultimate tensile strength (UTS), yield strength (YS), and micro-hardness, with the increase in MAF cycles. Ultimate tensile strength and hardness increased from 605 MPa and 252 HV (for as-received) to 1284 MPa and 428 HV for three cycles of MAF-processed sample, respectively. Improvement in strength and hardness was attributed to refined grain structure. Corrosion study was carried out for different cycles of MAF-processed samples using potentiodynamic polarization, and corroded surfaces were analyzed using scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS) analysis. © 2019, ASM International.Item Microstructural Study and Mechanical Characterization of ECAP Processed C70600 Alloy(Springer, 2022) Sachin, S.; Shivananda Nayaka, H.S.Copper–Nickel alloy C70600 was processed by equal channel angular pressing (ECAP), at room temperature, up to 8 passes, to study the mechanical properties and metallurgical behavior Microstructural studies showed grain refinement up to fourth ECAP pass. Microhardness value increased by 45% after 4 ECAP passes. With further increase in ECAP passes, samples attained a saturated state. Similar trend was observed in Ultimate tensile strength with an increase of 54% as compared to homogenized sample and reached a maximum value of 562 MPa. Increase in mechanical property was attributed to strengthening by grain refinement and dislocation strengthening. XRD analysis showed the absence of precipitate in the deformed specimens. © 2022, The Institution of Engineers (India).Item Effect of Multi-directional Forging on the Evolution of Microstructural and Mechanical Properties of Lightweight Al-Cu-Li Alloy AA2050(Springer, 2023) Jagadeesh, C.; Shivananda Nayaka, H.S.; Ramesh, S.; Praveen, T.R.Microstructural evolution and the mechanical properties of recently developed lightweight AA2050 Al-Cu-Li alloy have been presented. A processing route of multi-directional forging (MDF) at 170 °C followed by artificial aging at 150 °C was employed. Systematic EBSD analysis revealed significant grain refinement with grain size reducing from 74.3 ± 12 to 22.1 ± 2.8 µm after 12 passes of MDF. Transformation of deformation bands into subgrains with dynamic recrystallization has led to grain refinement. TEM results show the presence of large dislocation clusters and deformation bands in MDF processed samples with a large number of fine precipitates in peak aged MDF processed samples. XRD analysis shows variation in peak intensities and occurrence of peak shifts due to induced lattice strain upon MDF. A substantial increase in microhardness and strength was observed with a minor trade-off with ductility after 12th MDF pass. Further, enhancement in strengths and microhardness were observed in post-MDF aged samples. Experimental results show the combined effect of strain hardening, grain size reduction, and precipitate hardening which influence the material strength. A combination of MDF and artificial aging has shown great potential to enhance the strength and ductility of AA2050. © 2023, ASM International.Item Enhancing mechanical properties of Ti-64 alloy through ECAE: lubricant optimization, microstructural evolution and optimal process parameters(Springer-Verlag Italia s.r.l., 2025) Castelino, M.R.; Mallikappa, N.; Karinka, S.; Vijayan, V.; Shivananda Nayaka, H.S.; Valder, J.This study explores the application of Equal Channel Angular Extrusion (ECAE) in enhancing the microstructural and mechanical properties of Ti-64 alloy. Finite Element (FE) analysis validates experimental outcomes, revealing a significant reduction in grain size, improved strength, and hardness. Microstructural analysis indicates dynamic recrystallization, transforming larger alpha (?) grains into smaller ones. Tensile testing demonstrates increased yield and ultimate strength in ECAE-treated specimens due to decreased grain size and heightened dislocation density. Lubricant optimization achieves low friction coefficients (0.02 and 0.04), reinforcing ECAE effectiveness. FE simulations and ANOVA analysis identify influential factors, leading to optimal parameter combinations. Isothermal ECAE successfully reduces grain size, resulting in substantial improvements in yield strength, ultimate strength, and hardness. These findings highlight ECAE's efficacy in enhancing the mechanical properties of Ti-64 alloy, with specific applications in biomaterials, particularly dental implants and bone support, as well as aerospace fasteners, where Ti-64 contributes to increased fuel efficiency, reduced emissions, and enhanced structural integrity. © The Author(s), under exclusive licence to Springer-Verlag France SAS, part of Springer Nature 2024.