Faculty Publications

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    Investigation of microstructure and mechanical properties of the Cu-3% Ti alloy processed by multiaxial cryo-forging
    (Cambridge University Press, 2018) Ramesh, S.; Shivananda Nayaka, H.; Gopi, K.R.; Sahu, S.; Kuruveri, U.B.
    A Cu-3%Ti (wt%) alloy was processed by multiaxial forging (MAF) at cryogenic temperature up to 3 cycles, imposing a total strain of 1.6. Microstructure and mechanical properties of the unprocessed and cryo-forged samples were analyzed. X-ray diffraction results showed deviation in peak broadening and peak intensity of the cryo-forged samples in comparison to that of unprocessed, which are due to texture modification caused by grain refinement during the MAF process. Microstructural analysis showed reduction in grain size from 80 m in the as-received condition to 250 nm after 3 cycles. Electron backscatter diffraction results indicated the transformation of high angle grain boundaries to low angle grain boundaries in all 3 cycles when compared to the as-received condition. Reduction in ductility was observed after 1 cycle, but with an increase in the number of cycles, both strength and ductility increased. After 3 cycles, ultimate tensile strength and hardness reached 1126 MPa and 427 Hv as compared to 528 MPa and 224 Hv for the as-received condition. Fractography analysis showed decrement in dimple size after 1 cycle, in comparison to that of the as-received condition. However, it kept on increasing for higher number of cycles. © © Materials Research Society 2018.
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    Effects of combined multiaxial forging and rolling process on microstructure, mechanical properties and corrosion behavior of a Cu-Ti alloys
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.; Sahu, S.; Arya, S.
    Combined multiaxial forging (MAF) and rolling was performed on Cu-3% Ti (wt%) alloy at room temperature with emphasis on microstructural evolution, improvement in mechanical properties, and corrosion resistance. Microstructural changes were confirmed from various characterization techniques, and co-related with mechanical properties. TEM analysis revealed high shear band density in the 3 pass MAF + 90% rolled sample appearing due to high strain. EBSD analysis revealed transformation to low angle grain boundaries from high angle grain boundaries. Maximum microhardness and UTS reached to 340 HV and 960 MPa, respectively in the processed samples. Significant grain refinement was observed in MAF processed Cu-3%Ti alloy, and after combined MAF + rolling, higher dislocation density and refinement of shear bands were observed. In addition, potentio-dynamic polarization test was used to study the corrosion behavior of the alloy. Scanning electron microscope (SEM) was used to analyze the corroded surface morphology. © 2019 IOP Publishing Ltd.
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    Surface modification of multi-directional forged biodegradable Mg-Zn alloy by ball burnishing process: Modeling and analysis using deep neural network
    (Elsevier Ltd, 2021) Ramesh, S.; Anne, G.; Bhat, N.; Aithal, G.; Shivananda Nayaka, H.; Arya, S.
    This research investigates the feasibility of improving surface integrity of the Mg-2%Zn alloy via a novel combined process of multidirectional forging (MDF) with ball burnishing technique. Mg-2%Zn alloy was subjected to multidirectional forging up to 5 passes at 280 °C and same sample is ball burnished with depth of press of 0.3 mm, feed of 300 mm/min and force of 250 N for 1 pass. Microstructure (optical and transmission electron microscope), phases (X ray diffraction), roughness (atomic force microscope) and mechanical properties (microhardness and tensile) were analyzed for cast, MDF processed and MDF + ball burnished samples. The study also defines a new reliability simulation framework to predict the roughness and hardness of the MDF + ball burnished samples using Deep Neural Network (DNN) approach. For the analysis, depth of press, feed and number of passes served as inputs for the DNN model. After configuring and training procedure of the model, the predicted roughness and microhardness of the MDF + ball burnished were compared with the results of experimental data. A large increase of microhardness was observed for MDF-5 + BB-1 (5 pass MDF processed Mg-2%Zn alloy + Ball burnished sample), found to be 98 Hv and surface roughness of 306 nm was achieved. According to the results, the obtained R-squared value is very close to the 99.5 percentage from the model for predicting roughness and hardness which is a promising result. Corrosion behavior of the AS-1, MDF-5 and MDF-5 + BB-1 was evaluated in Hank's balanced salt solution. Corrosion rate of the MDF-5 + BB-1 samples were found to be 0.87 mm/y which is 7 times better than that of AS-1 samples (6.10 mm/y). Grain refinement and residual stresses were higher in the MDF-5 + BB-1 sample, which helped significantly to enhance corrosion resistance. © 2021 The Society of Manufacturing Engineers
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    On the microstructure, texture and electrochemical properties of severely deformed and artificially aged lightweight AA2050 Al-Cu-Li alloy
    (Institute of Physics, 2024) Jagadeesh, C.; Shivananda Nayaka, H.; Sekar, P.; Ramesh, S.; Anne, G.
    Lightweight 3rd generation Al-Cu-Li alloy AA2050 was severely deformed via Multi Axial Forging (MAF) at 170 °C followed by artificial aging at 150 °C. Effect of MAF and post MAF aging on microstructure and precipitation was investigated using transmission electron microscopy (TEM). Formation of deformation bands and large dislocation cells were evident on MAF processed samples. Post MAF peak aging resulted in the distribution of fine T1 precipitates in grain interiors with reduction in grain boundary precipitation. Bulk texture studies reveal the formation of strong Goss and S texture components upon MAF processing. Further, low temperature artificial aging doesn’t exhibit significant changes in texture characteristics, either in terms of texture intensities or texture components. Polarization studies showed that peak aged samples exhibited better corrosion resistance compared to un-aged samples. Overall, 12 pass MAF processed and peak aged samples showed higher corrosion resistance. Further, corrosion surface morphologies examination revealed the change in corrosion mechanisms with thermomechanical treatments. Improved corrosion resistance after MAF and peak aging widens the requirements in aerospace and aircraft applications for such engineering alloys. © 2024 The Author(s). Published by IOP Publishing Ltd.
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    Reciprocating wear behavior of multi-directionally forged and aged Al-Cu-Li alloy
    (Institute of Physics, 2024) Jagadeesh, C.; Shivananda Nayaka, H.; Ramesh, S.; Anne, G.
    Al-Cu-Li alloys have drawn attention because of their decreased density, which is a result of the growing need for lightweight material systems in aerospace and aircraft applications. The alloy was subjected to multi-directional forging (MDF) and post-MDF artificial aging. Reciprocating sliding wear tests were conducted to investigate the effects of these processes on wear properties under different load conditions. After MDF, a decrease in wear resistance was noticed, on the other hand, 12 pass MDF treated samples showed improved wear resistance upon aging treatment. Wear scars and counter ball surfaces were examined using scanning electron microscope (SEM) to understand the wear mechanism and wear mode. The findings demonstrated that, at lower loads, adhesion and abrasion were the main wear processes; at greater loads, delamination, adhesion, and abrasion were clearly visible. The study revealed that the MDF and subsequent aging have a substantial effect on the wear behavior of Al-Cu-Li alloy and is an effective thermomechanical processing route to enhance wear resistance. © 2024 The Author(s). Published by IOP Publishing Ltd