Faculty Publications

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    Development, Characterization, Mechanical and Corrosion Behaviour Investigation of Multi-direction Forged Mg–Zn Alloy
    (Springer International Publishing, 2019) Anne, G.; Ramesh, S.; Kumar, G.; Sahu, S.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.
    In the present study, homogenized Mg−4%Zn (wt%) alloy was exposed to multi-direction forging (MDF) at 280 °C up to 5 passes successfully. Microstructural evolution, mechanical properties and corrosion behavior of the MDF-processed Mg−4%Zn alloy was investigated using different characterization techniques. Five passes of MDF (cumulative strain, ΣΔε = 3.45) led to the formation of ultrafine grain structure (grain size ~2.3 μm) with high angle grain boundaries (HAGBs) and high dislocation density. Corresponding ultimate tensile strength (UTS) and microhardness were observed to be 228 MPa and 88 Hv. Potentiodynamic polarization test results exhibited higher corrosion resistance (0.38 mm/y) in comparison with that of homogenized condition (1.33 mm/y). © 2019, The Minerals, Metals & Materials Society.
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    Striking the Balance between Novelty and Accuracy in Location-Based Recommendation System
    (Institute of Electrical and Electronics Engineers Inc., 2019) Agrawal, V.; Sahu, S.; Oommen, S.; Guddeti, G.R.
    With widespread popularity of Location-Based Social Networks (LSBNs), the recommendation problem in this domain has led to significant amount of research regarding its practical applications. Despite extensive studies on recommendation systems based on parameters such as GPS trajectories, user-item ratings and check-in data, few methodologies take novelty of recommendations as a significant parameter. In this paper, we attempt to provide an improved approach to recommend points of interest (POIs) to users using a graph based approach which is in accordance with their personal interests and preferences. The proposed algorithm provides users with a personalized ranked list of venues based on their past check-in data and social relationships, which is novel yet accurate at the same time. It takes into account the existing challenges and is based on two key components: User Preferences and Social Relationships that are inferred from their past check-in history and Entropy of Venues which determines the novelty of recommendations provided. In short, it returns a ranked list of 'k' venues which are most likely to suit the personal taste of the user. Experimental results demonstrate that the proposed methodology outperforms the baseline methods in terms of novelty and accuracy. © 2019 IEEE.
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    Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy
    (Springer New York LLC barbara.b.bertram@gsk.com, 2016) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.
    Magnesium alloy Mg-Al-Mn (AM70) was processed by equal channel angular pressing (ECAP) at 275 °C for up to 4 passes in order to produce ultrafine-grained microstructure and improve its mechanical properties. ECAP-processed samples were characterized for microstructural analysis using optical microscopy, scanning electron microscopy, and transmission electron microscopy. Microstructural analysis showed that, with an increase in the number of ECAP passes, grains refined and grain size reduced from an average of 45 to 1 µm. Electron backscatter diffraction analysis showed the transition from low angle grain boundaries to high angle grain boundaries in ECAP 4 pass sample as compared to as-cast sample. The strength and hardness values an showed increasing trend for the initial 2 passes of ECAP processing and then started decreasing with further increase in the number of ECAP passes, even though the grain size continued to decrease in all the successive ECAP passes. However, the strength and hardness values still remained quite high when compared to the initial condition. This behavior was found to be correlated with texture modification in the material as a result of ECAP processing. © 2016, ASM International.
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    Development and characteristics of accumulative roll bonded Mg-Zn/Ce/Al hybrid composite
    (Elsevier Ltd, 2017) Anne, G.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.B.; Sahu, S.
    Accumulative roll bonding (ARB) process have been used develop Mg-2%Zn/Ce/Al hybrid composite and microstructure, mechanical and corrosion properties were investigated. The electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) revealed that the grains are significantly reduced and reaches up to 1 ?m in Mg-2%Zn layer and 1.8 ?m in Al layer having high angle misorientation of grain boundaries after subjected to 5-passes of the ARB process. The Al17Mg12, AlMg4Zn11 and Al11Ce3 intermetallic phases were observed through the XRD analysis. Mechanical properties of the hybrid composite improved with increase in the number of ARB passes which is attributed to work hardening, grain refinement and uniform distribution of Ce particles. Presence of Ce in the hybrid composite restricts the phenomenon of dynamic recrystallization and prevents the grain growth during ARB process. The corrosion rate of Mg-Zn/Ce/Al hybrid composite (0.72 mm/y) improved about 3.3 times as compared to that of Mg-2%Zn alloy (2.37 mm/y). © 2017 Elsevier B.V.
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    Microstructure Evolution and Mechanical and Corrosion Behavior of Accumulative Roll Bonded Mg-2%Zn/Al-7075 Multilayered Composite
    (Springer New York LLC barbara.b.bertram@gsk.com, 2017) Anne, G.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.B.; Sahu, S.
    Multilayered composite of Mg-2%Zn/Al-7075 was developed by accumulative roll bonding (ARB) of wrought Mg-2%Zn and aluminum 7075 alloy. The Mg-2%Zn/Al-7075 multilayered composite exhibited density of 2295 kg/m3 and an average grain size of 1 and 1.3 ?m in Mg-2%Zn and Al-7075 layers, respectively. A thorough microstructural characterization was performed on the composites by scanning electron microscope, electron backscatter diffraction (EBSD), transmission electron microscope and phase analysis by x-ray diffraction. In addition, mechanical properties were evaluated by microhardness and tensile tests. Corrosion behavior of the multilayered composite was examined using electrochemical polarization test. EBSD analysis showed the presence of ultrafine grains with high-angle grain boundaries. The composite exhibited a significant improvement in ultimate tensile strength (~1.82 times) and elongation (~1.5 times) as compared with Mg-2%Zn alloy, after four-pass ARB process. © 2017, ASM International.
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    Development and properties evaluation of Mg-6% Zn/Al multilayered composites processed by accumulative roll bonding
    (Cambridge University Press, 2017) Anne, G.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.B.; Sahu, S.
    Accumulative roll bonding (ARB) process was used to develop Mg-6% Zn/Al and Mg-6% Zn/anodized-Al multilayered composites. Microstructural characterization was done using scanning electron microscopy, energy-dispersive X-ray spectroscopy, electron backscattered diffraction, and transmission electron microscopy. An average grain size measured in the roll-bonded layers of Al, anodized Al, and Mg-2% Zn was found to be 1.8 ?m, 1.6 ?m, and 0.6 ?m, respectively. Phases Al17Mg12, AlMg4Zn11, and Al2O3 after 5-pass of ARB were confirmed by X-ray diffraction analysis. The Mg-6% Zn/Al and Mg-6% Zn/anodized Al composites exhibited tensile strengths ?252 MPa and ?256 MPa, respectively, after a 5-pass ARB process. Hardness of the individual layers of composite increased linearly with an increase in the number of ARB passes. Fractographs of the multilayered composite illustrated the ductile failure in Al and anodized Al layers and transgranular brittle fracture in Mg-6% Zn layers. © Materials Research Society 2017.
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    Wear Properties of ECAP-Processed AM80 Magnesium Alloy
    (Springer New York LLC barbara.b.bertram@gsk.com, 2017) Gopi, K.R.; Shivananda Nayaka, H.; Sahu, S.
    AM80 magnesium alloy was subjected to equal-channel angular pressing (ECAP), and microstructural evolution was studied using scanning electron microscope (SEM). Grain size was found to decrease up to 3 µm after four passes. An increase in number of ECAP passes led to a corresponding increase in hardness of the processed samples. Unprocessed and ECAP-processed samples were subjected to wear test using pin-on-disk wear test machine to study the wear behavior. Effects of varying loads (30 and 40 N) with sliding distances (2500 and 5000 m) were studied. The results showed reduction in wear mass loss for the ECAP-processed samples in comparison with unprocessed condition. Coefficient of friction (COF) was studied for different loads, and improvement in COF values was observed for ECAP-processed samples compared to unprocessed condition. Worn surfaces were studied using SEM and energy-dispersive x-ray spectrometer, and they exhibited plastic deformation, delamination, plowing, wear debris and oxidation in the sliding direction. X-ray diffraction analysis was conducted on the worn surfaces to identify the phases. It revealed the presence of magnesium oxide and magnesium aluminum oxide which led to oxidation wear in the sliding direction. Wear mechanism was found to be abrasive and oxidation wear. © 2017, ASM International.
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    Microstructural Evolution and Strengthening of AM90 Magnesium Alloy Processed by ECAP
    (Springer Verlag, 2017) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.
    Equal-channel angular pressing (ECAP) was applied on AM90 magnesium alloy using processing route B C at 275?C up to four passes. Microstructural evolution and the corresponding modification in mechanical properties (strength, elongation and hardness) corresponding to the number of ECAP passes were evaluated using X-ray diffraction (XRD), electron backscatter diffraction, scanning electron microscopy, transmission electron microscopy, tensile test and microhardness test. Shear deformation was found to refine the microstructure by breaking it into smaller grains formed by dislocation reconstruction. Tensile strength and hardness were found to increase by ? 128 and 23%, respectively, for ECAP-processed 2-pass sample in comparison with that of the homogenized condition. After two passes, tensile strength and hardness started decreasing even though the grain size was still decreasing, which was found to be associated with texture modification during ECAP processing as observed by XRD analysis. © 2017, King Fahd University of Petroleum & Minerals.
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    Corrosion Behavior of ECAP-Processed AM90 Magnesium Alloy
    (Springer Verlag, 2018) Gopi, K.R.; Shivananda Nayaka, H.; Sahu, S.
    Magnesium AM90 alloy was subjected to equal-channel angular pressing (ECAP) using route B C. Microstructural characterization revealed refined grains having average grain size ?3?m after ECAP 4 passes. Samples were subjected to electrochemical measurements to study the corrosion behavior. Potentiodynamic polarization test showed reduced corrosion current density (Icorr) for processed samples up to ECAP 3 pass due to grain refinement. Electrochemical impedance spectroscopy showed an increase in the diameter of the capacitive arcs and charge-transfer resistance (Rt) for ECAP-processed 3 pass sample indicating the reduction in corrosion rate. Increase in corrosion resistance is due to refined microstructure and uniform distribution of secondary particles forming a protective passivation layer (Mg (OH) 2) on the sample’s surface. Immersion test indicated lower hydrogen evolution from ECAP-processed samples compared to the unprocessed condition indicating decreased corrosion rate. © 2018, King Fahd University of Petroleum & Minerals.
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    Investigation of microstructure and mechanical properties of the Cu-3% Ti alloy processed by multiaxial cryo-forging
    (Cambridge University Press, 2018) Ramesh, S.; Shivananda Nayaka, H.; Gopi, K.R.; Sahu, S.; Kuruveri, U.B.
    A Cu-3%Ti (wt%) alloy was processed by multiaxial forging (MAF) at cryogenic temperature up to 3 cycles, imposing a total strain of 1.6. Microstructure and mechanical properties of the unprocessed and cryo-forged samples were analyzed. X-ray diffraction results showed deviation in peak broadening and peak intensity of the cryo-forged samples in comparison to that of unprocessed, which are due to texture modification caused by grain refinement during the MAF process. Microstructural analysis showed reduction in grain size from 80 m in the as-received condition to 250 nm after 3 cycles. Electron backscatter diffraction results indicated the transformation of high angle grain boundaries to low angle grain boundaries in all 3 cycles when compared to the as-received condition. Reduction in ductility was observed after 1 cycle, but with an increase in the number of cycles, both strength and ductility increased. After 3 cycles, ultimate tensile strength and hardness reached 1126 MPa and 427 Hv as compared to 528 MPa and 224 Hv for the as-received condition. Fractography analysis showed decrement in dimple size after 1 cycle, in comparison to that of the as-received condition. However, it kept on increasing for higher number of cycles. © © Materials Research Society 2018.