Faculty Publications

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  • Item
    Development, Characterization, Mechanical and Corrosion Behaviour Investigation of Multi-direction Forged Mg–Zn Alloy
    (Springer International Publishing, 2019) Anne, G.; Ramesh, S.; Kumar, G.; Sahu, S.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.
    In the present study, homogenized Mg−4%Zn (wt%) alloy was exposed to multi-direction forging (MDF) at 280 °C up to 5 passes successfully. Microstructural evolution, mechanical properties and corrosion behavior of the MDF-processed Mg−4%Zn alloy was investigated using different characterization techniques. Five passes of MDF (cumulative strain, ΣΔε = 3.45) led to the formation of ultrafine grain structure (grain size ~2.3 μm) with high angle grain boundaries (HAGBs) and high dislocation density. Corresponding ultimate tensile strength (UTS) and microhardness were observed to be 228 MPa and 88 Hv. Potentiodynamic polarization test results exhibited higher corrosion resistance (0.38 mm/y) in comparison with that of homogenized condition (1.33 mm/y). © 2019, The Minerals, Metals & Materials Society.
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    Effects of combined multiaxial forging and rolling process on microstructure, mechanical properties and corrosion behavior of a Cu-Ti alloys
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.; Sahu, S.; Arya, S.
    Combined multiaxial forging (MAF) and rolling was performed on Cu-3% Ti (wt%) alloy at room temperature with emphasis on microstructural evolution, improvement in mechanical properties, and corrosion resistance. Microstructural changes were confirmed from various characterization techniques, and co-related with mechanical properties. TEM analysis revealed high shear band density in the 3 pass MAF + 90% rolled sample appearing due to high strain. EBSD analysis revealed transformation to low angle grain boundaries from high angle grain boundaries. Maximum microhardness and UTS reached to 340 HV and 960 MPa, respectively in the processed samples. Significant grain refinement was observed in MAF processed Cu-3%Ti alloy, and after combined MAF + rolling, higher dislocation density and refinement of shear bands were observed. In addition, potentio-dynamic polarization test was used to study the corrosion behavior of the alloy. Scanning electron microscope (SEM) was used to analyze the corroded surface morphology. © 2019 IOP Publishing Ltd.
  • Item
    Influence of Multidirectional Forging on Microstructural, Mechanical, and Corrosion Behavior of Mg-Zn Alloy
    (Springer New York LLC barbara.b.bertram@gsk.com, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.
    Multidirectional forging (MDF) was applied to Mg-6%Zn alloy up to 5 passes successfully at 280 °C. MDF-processed materials were characterized using optical microscope, scanning electron microscope, electron backscatter diffraction, transmission electron microscope, and x-ray diffraction. Obtained results showed a significant reduction in grain size (up to 3.8 ?m) having a large fraction of high-angle grain boundaries after 5 passes of MDF process. Maximum tensile strength of 230 MPa was achieved for 5-pass MDF-processed Mg-6%Zn alloy which is about ~ 2.0 times higher in comparison with that of homogenized alloy (117 MPa) and was attributed to higher dislocations density and grain refinement. Corrosion behavior of the alloy was investigated in 0.1 M NaCl solution using potentiodynamic polarization test, electrochemical impedance spectra analysis, and immersion tests. It was found that the corrosion rate of 5-pass MDF sample improved (0.34 mm/year) ~2.5 times in comparison with that of homogenized Mg-6%Zn alloy (0.86 mm/year) due to fine grain structure, which creates more grain boundaries that act as a corrosion barrier. © 2019, ASM International.