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  • Item
    Investigation of microstructure and mechanical properties of the Cu-3% Ti alloy processed by multiaxial cryo-forging
    (Cambridge University Press, 2018) Ramesh, S.; Shivananda Nayaka, H.; Gopi, K.R.; Sahu, S.; Kuruveri, U.B.
    A Cu-3%Ti (wt%) alloy was processed by multiaxial forging (MAF) at cryogenic temperature up to 3 cycles, imposing a total strain of 1.6. Microstructure and mechanical properties of the unprocessed and cryo-forged samples were analyzed. X-ray diffraction results showed deviation in peak broadening and peak intensity of the cryo-forged samples in comparison to that of unprocessed, which are due to texture modification caused by grain refinement during the MAF process. Microstructural analysis showed reduction in grain size from 80 m in the as-received condition to 250 nm after 3 cycles. Electron backscatter diffraction results indicated the transformation of high angle grain boundaries to low angle grain boundaries in all 3 cycles when compared to the as-received condition. Reduction in ductility was observed after 1 cycle, but with an increase in the number of cycles, both strength and ductility increased. After 3 cycles, ultimate tensile strength and hardness reached 1126 MPa and 427 Hv as compared to 528 MPa and 224 Hv for the as-received condition. Fractography analysis showed decrement in dimple size after 1 cycle, in comparison to that of the as-received condition. However, it kept on increasing for higher number of cycles. © © Materials Research Society 2018.
  • Item
    Investigation of Tribological Characteristics of Cu-Ti Alloys Processed by Multi-Axial Cryo-Forging
    (Springer, 2022) Ramesh, S.; Shivananda Nayaka, H.S.; Anne, G.; Arun, M.N.; Naik, G.M.
    Cu-XTi alloys (X = 1.5 and 4.5%) were subjected to multi-axial forging (MAF) under cryogenic condition up to three passes successfully. Characteristics of the MAF-processed alloys were analyzed using microstructural analysis, hardness and wear tests. Worn surface morphology and elemental analysis was performed by scanning electron microscopy. The hardness of samples increases with higher MAF passes due to strain hardening and grain refinement. Wear test was done for six various sliding distances (500, 1000, 1500, 2000, 2500 and 3000 m), two different loads (10 and 20 N), and two different velocities (1 and 2 m/s) using the pin-on-disk wear test rig. Wear loss of as-received samples is higher than MAF-pressed samples due to an increase in hardness, but wear loss increases as the load increases. Coefficient of friction is reduced with the increase in MAF pass, which is due to strain hardening effect. The worn surface exhibits the plastic deformation regions, delamination, plowing and formation of oxide layers, which was revealed by energy-dispersive X-ray spectroscopy analysis. Also, MAF-processed samples exhibited abrasive wear mechanism as a result of formation of oxygen layer as revealed in SEM micrographs. © 2022, ASM International.
  • Item
    Enhancing wear resistance of AZ61 alloy through friction stir processing: experimental study and prediction model
    (Institute of Physics, 2024) Anne, G.; Ramesh, S.; Sharma, P.; Maruthi Prashanth, B.H.; Aditya Kudva, S.; Kumar, P.; Sahu, S.; Bhat, N.
    In this study, friction stir processing (FSP) is proposed for the treatment of AZ61 alloy, and an artificial neural network is built to predict and compare the experimental wear results. The effects of different processing parameters, including spindle speed (800-1200 rpm), traveling speed (5-15 mm min−1), and depth of press (0.8-1.2 mm) on the microstructural evolution, mechanical properties, and wear behavior are investigated. Microstructural analysis reveals a grain size of 14 ± 2 μm for the FSP1 sample, with observed shifting of x-ray diffraction (XRD) peaks, indicative of texture development. Increasing spindle and traveling speeds increase the surface roughness, as observed by average roughness (Ra) values of 68.4 nm for a rotational speed of 800 rpm, traveling speed of 5 mm min−1, and shoulder depth of 0.8 mm (FSP1) and 116.3 nm for rotational speed of 1200 rpm, traveling speed of 15 mm min−1, and shoulder depth of 1 mm (FSP9). Microhardness values increase to 113.36 Hv for FSP1 and 79. 51 Hv for FSP9 compared to 65.92 Hv for the base material (BM) sample. The decrement in hardness from FSP1 to FSP9 can be attributed to increased heat input, resulting in coarse microstructure. Wear results show that FSP1 exhibits the lowest weight loss (0.003 g) and coefficient of friction (COF) (0.28) compared to other FSP conditions and BM samples (weight loss of 0.022 g and COF of 0.68). This work demonstrates the efficacy of friction stir processing in enhancing the wear resistance of magnesium alloys. © 2024 The Author(s). Published by IOP Publishing Ltd.