Faculty Publications
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Item Elevated Temperature Solid Particle Erosion Performance of Plasma-Sprayed Co-based Composite Coatings with Additions of Al2O3 and CeO2(Springer New York LLC barbara.b.bertram@gsk.com, 2017) Nithin, H.S.; Desai, V.; Ramesh, M.R.In this paper, investigation into solid particle erosion behavior of atmospheric plasma-sprayed composite coating of CoCrAlY reinforced with Al2O3 and CeO2 oxides on Superni 76 at elevated temperature of 600 °C is presented. Alumina particles are used as erodent at two impact angles of 30° and 90°. The microstructure, porosity, hardness, toughness and adhesion properties of the as-sprayed coatings are studied. The effects of temperature and phase transformation in the coatings during erosion process are analyzed using XRD and EDS techniques. Optical profilometer is used for accurate elucidation of erosion volume loss. CoCrAlY/CeO2 coating showed better erosion resistance with a volume loss of about 50% of what was observed in case of CoCrAlY/Al2O3/YSZ coating. Lower erosion loss is observed at 90° as compared to 30° impact angle. The erosion mechanism evaluated using SEM micrograph revealed that the coatings experienced ductile fracture exhibiting severe deformation with unusual oxide cracks. Reinforced metal oxides provide shielding effect for erodent impact, enabling better erosion resistance. The oxidation of the coating due to high-temperature exposure reforms erosion process into oxidation-modified erosion process. © 2017, ASM International.Item Effect of Ball Milling on the Tensile Properties of Aluminum-Based Metal Matrix Nanocomposite Developed by Stir Casting Technique(SAE International, 2021) Ravikumar, K.S.; Ghanaraja, S.; Ramesh, M.R.Combining ball milling with stir casting in the synthesis of nanocomposites is found effective in increasing the strength and ductility of the nanocomposites. In the first step, the nanoparticles used as reinforcement are generated by milling a mixture of aluminum (Al) and manganese dioxide (MnO2) powders. A mixture of Al and MnO2 powders are mixed in the ratio of 1:2.4 by weight and milled at 300 rpm in a high-energy planetary ball mill for different durations of 120 min, 240 min, and 360 min to generate nano-sized alumina (Al2O3) particles. It is supposed that the powders have two different roles during milling, firstly, to generate nano-sized Al2O3 by oxidation at the high-energy impact points due to collision between Al and MnO2 particles, and secondly, to keep nano-sized Al2O3 particles physically separate by the presence of coarser particles. In the second step, 0.5 weight percent (wt%), 1 wt%, 1.5 wt%, and 2 wt% of the generated Al2O3 nanoparticles are reinforced in molten aluminum-magnesium (Al-Mg) alloy matrix via stir casting to synthesize nanocomposites. The effect of milling on the microstructure of the powder mixture before and after milling has been studied with the use of a scanning electron microscope (SEM) and X-ray diffraction analysis (XRD). The microstructure of the cast composites is examined under SEM, and the fractured surface of the tensile specimens is analyzed through SEM fractographs. Ball milling of reinforcement before adding to the melt brings considerable improvement in the integration and uniform dispersion of the milled particle in the Al-Mg alloy matrix melt, which leads to improvement in the strength and ductility of the cast nanocomposites. ©Item Tribological behaviour of natural fibre 3D braided woven fabric reinforced PLA composites(SAGE Publications Ltd, 2021) Kanakannavar, S.; Jeyaraj, J.; Ramesh, M.R.This study aims to investigate the potential of natural fibre 3D braided woven fabric (NFBF) reinforced PLA (poly lactic acid) composites for tribological applications. Composites with different fibre contents are prepared using film stacking process and hot press methods. Friction co-efficient and wear rate of the composites are analysed using pin-on-disc tribometer under dry contact sliding condition and various operating conditions (velocity and load) for a fixed sliding distance of 3000 m. The morphology of the worn surfaces is studied using scanning electron microscope (SEM). The reinforcement of fibre with the PLA reduced the polymer film generation and improved the surface roughness significantly. Wear rate of the composites are decreased drastically compared to pure PLA. Composite with 35 wt.% of NFBF reinforcement showed better wear characteristics. © IMechE 2020.Item Effect of Milling on the Hardness and Wear Behaviour of Cast Al6061 Reinforced with Al2O3 Nanoparticles(Springer Science and Business Media Deutschland GmbH, 2022) Ravikumar, K.S.; Ghanaraja, S.; Ramesh, M.R.Alumina nanoparticles is generated through planetary ball milling of powder mix compraise of aluminium (Al) and manganese dioxide (MnO2). The powder mix of Al and MnO2 is considered in the weight proportion of 1:2.416 and milled for 120, 240 and 360 min. In the milling jar, the powder mix will experience impact force while collusion with ball-powder-ball and ball-powder-wall of the jar. These impact force will cause cyclic deformation and fracture of the powder mix, which results in the synthesis of nano alumina. The morphology of the powder mix prior to milling and post milling for different times has been studied by scanning electron microscope and X-ray diffraction. Cast composites have been synthesized via liquid metallurgy technique using Al6061 as matrix and generated alumina particles by milling is considered as reinforcement. Comparative study have been conducted between the composites prepared by considering Al6061 as matrix and as received powder as reinforcement with the composites prepared by considering Al6061 as matrix and alumina generated through the milling as reinforcement. The reinforcement added to the the matrix in the varying proportions of 0.5, 1 and 1.5 wt% of particles before milling and after milling. The effect particles size related to hardness and wear property of cast composites are studied. It was found that the wear resistance increased monotonically with hardness. © 2021, The Author(s), under exclusive licence to Springer Nature Switzerland AG.Item Effect of temperature on wear and friction performance of WC-Co and Cr3C2 reinforced with 17-4PH Fe-based composite coatings(Springer Science and Business Media Deutschland GmbH, 2024) Chandramouli, T.V.; Joladarashi, S.; Ramesh, M.R.; Rahman, M.R.Surface protection is crucial in industrial equipment and tools to prevent wear and friction in harsh environments, particularly at high temperatures, where anti-friction coatings are essential for optimal performance. The present research investigates the tribological properties of high-velocity oxy-fuel sprayed coatings of 17-4PH stainless steel reinforced with tungsten carbide and chromium carbide powders. The coatings are deposited onto a maraging steel substrate. A dry sliding wear test was performed using an alumina ball as a counter body under various test temperatures (25 °C, 300 °C, and 600 °C) and loads (10 N and 30 N). The coating is characterized by employing SEM, XRD, micro-hardness tester, particle analyzer, and bond strength tester, and the mechanism of wear reduction was discussed. The post-wear analysis was carried out on the wear track using SEM/EDS and 3D non-contact optical profilometers. The micro-hardness and bond strength of both (17-4PH-30%WC-Co and 17-4PH-30%Cr3C2) coatings are compared. The test results revealed that at all temperatures and loads, 17-4PH-30%WC-Co coating shows better wear resistance and lower friction coefficient than the 17-4PH-30%Cr3C2 coating. The significant influence of the tribo-oxide layer at high temperatures, which contributed to decreasing wear rate and coefficient of friction, was premeditated. © 2023, International Institute of Welding.Item Fabrication and Characterization of Silicon Dioxide-Reinforced Polydimethylsiloxane Composite Coating for Corrosion Protection of Galvanized Iron(SAE International, 2024) Kumar, P.; Ramesh, M.R.; Doddamani, M.The present work highlights the significance of nanocomposite coatings for their ease of processing and applicability in combating corrosion. Ongoing research is dedicated to the development of an effective nanocomposite hydrophobic coating. A hydrophobic nanocomposite coating was deposited on galvanized iron (GI) using a sol-gel route with polymethylsiloxane (PDMS) reinforced with nano-SiO2. Surface morphology and chemical composition analysis, conducted with scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDAX) and Fourier transform infrared spectroscopy (FTIR), revealed the coating's structural and compositional attributes. The resulting hydrophobic coating exhibits a water contact angle (WCA) of 104.1°, indicating a 30.45% increase compared to bare GI. Subsequent to these characterizations, the adhesion of the coated GI, rated as 4B per ASTM D3359, is followed by commendable resistance to corrosion, as evidenced by electrochemical tests. The corrosion rate for the coated GI sheet is notably low, at 62.78 × 10-3 mpy, underscoring its anti-corrosive efficacy. © 2024 SAE International.Item Microstructure, Mechanical Properties, and Tribological Properties of Fe-Based Composite Coatings Reinforced with WC-Co and Cr3C2(Springer, 2025) Chandramouli, T.V.; Joladarashi, S.; Ramesh, M.R.; Rahman, M.R.Fe-based (stainless steel 316L) coatings are widely employed in the aerospace, chemical processing, petrochemical, and marine industries owing to their low and stable price, excellent corrosion resistance, and durability. However, at elevated temperatures, their performance is limited due to wear. Thus, the current investigation incorporates tungsten carbide (WC-Co) and chromium carbide (Cr3C2) into the Fe-based coating to enhance its wear resistance at high temperatures. SS316L reinforced by 30% of WC-Co and Cr3C2 by mechanical mixture, then sprayed using high-velocity oxy fuel spraying method. Coating characteristics, such as microstructures and phase analysis, were measured using FESEM/EDS and XRD. Coating density, microhardness, and bond strength were examined by water immersion, Vickers indentation, and ASTM C-633 methods, respectively. A ball-on-disk tribometer was employed to conduct wear examination at various temperatures (25, 300, and 600 °C) and loads (10 and 30 N) against the alumina counter body. The wear rate and friction coefficient of SS316L-30%WC-Co decrease from 25 to 600 °C, while the wear rate of SS316L-30%Cr3C2 increases with temperature up to 300 °C and then decreases at 600 °C. The oxide phase adheres strongly to underlying surfaces forming a protective layer (Cr2O3, NiWO4, Fe2O3, and NiMO4), changing the mode of wear mechanism. At higher temperatures and loads, the coating exhibited oxidation modified adhesive wear, and coatings provide excellent wear resistance along with reduction in friction. This research provides a novel approach for future standardization and evaluation of coatings on metal alloys for industrial applications. © ASM International 2024.Item Surface enhancement of SS304 for high-temperature wear resistance using laser cladded Mo-alloyed stellite 6 coatings(Elsevier B.V., 2025) Aprameya, C.R.; Joladarashi, S.; Ramesh, M.R.Severe wear often limits the high-temperature durability of SS304 components, necessitating the development of surface-engineered solutions. In this investigation, Mo-reinforced Stellite 6 claddings were developed using Laser Directed Energy Deposition (L-DED) to provide enhanced surface protection. Claddings with (3, 6, and 9 wt%) Mo reinforcement enhanced hardness by 2.9, 3.1, and 3.3 times, respectively, compared to the SS304 substrate. This improvement is attributed to Mo-induced solid solution strengthening and the formation of hard intermetallic phases. Dry sliding wear tests were conducted at RT and 600 °C under (10 and 20 N) loads. Wear characterisation of the clads was performed using OM, XRD, FE-SEM, EDX, and Raman spectroscopy. At RT, claddings primarily exhibited abrasive wear with minor plastic deformation. However, at 600 °C, the wear mechanism evolved into a combination of severe adhesive, oxidative, abrasive, and plastic deformation modes, with oxidative wear governing the tribological behavior. Stellite 6 with 9 wt% Mo clads exhibited better tribological performance than the other two variants, owing to the development of oxide glaze layers of Cr2O3, NiO, CoO2, and Co3O4. Enhanced performance of the claddings is attributed to solid solution strengthening, Cr-rich carbide formation, increased dislocation density, and the L-DED technology enabling refined microstructure and strong metallurgical bonding. These findings highlight the potential for further advancements in Mo-reinforced Stellite 6 L-DED claddings for high-temperature wear applications. © 2025 Elsevier B.V.