Faculty Publications

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    Microstructure and Adhesion Strength of Ni3Ti Coating Prepared by Mechanical Alloying and HVOF
    (Pleiades Publishing compmg@maik.ru, 2018) Reddy, N.C.; Ajay Kumar, B.S.; Ramesh, M.R.; Koppad, P.G.
    In the present work we report the development of Ni3Ti intermetallic compound by high energy ball milling of Ni and Ti powders. The ball milled powders were taken at various intervals (4, 6, 8, 10, and 11 h) to analyze the formation of NixTix intermetallic compounds. The ball milled powders were analyzed using scanning electron microscopy and X-ray diffraction. The layered shaped powder particles of Ni3Ti phase were formed after 11 h of ball milling, which was confirmed by X-ray peaks. Further High-Velocity Oxy-Fuel (HVOF) process was used to coat Ni3Ti and Ni3Ti + (Cr3C2 + 20NiCr) on MDN 420 steel. Both the coated materials displayed excellent cohesion with minimal porosity less than 2%. The tensile adhesion strength test was carried out on these coatings to check the bond strength. Out of the two the Ni3Ti coating showed excellent bond strength of 41.04 MPa compared to that of Ni3Ti + (Cr3C2 + 20NiCr) coating. © 2018, Pleiades Publishing, Ltd.
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    Influence of microwave hybrid heating on the sliding wear behaviour of HVOF sprayed CoMoCrSi coating
    (Institute of Physics Publishing helen.craven@iop.org, 2018) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    CoMoCrSi superalloy powder (Tribaloy-T400) consists of intermetallic laves phase and primary eutectic phase of Co-rich solid solution. Processing of Tribaloy-T400 powder is carried out through high-energy ball milling (HEBM) technique to obtain a higher volume fraction of intermetallic laves phases. The feedstock is sprayed using high-velocity-oxy-fuel (HVOF) process on titanium grade-15 substrate. The coating microstructure is homogenized by microwave hybrid heating technique. Characterization of feedstock, as-sprayed and microwave fused coatings is done by using Scanning Electron Microscopy (SEM), Energy dispersive spectroscopy (EDS) and x-ray Diffraction (XRD). Porosity, surface roughness, microhardness, and bond strength are measured. Adhesive wear behavior of the coatings under the dry sliding condition is evaluated at an applied load of l0 and 20 N and temperature of 200, 400 and 600 °C Fused coating exhibit higher wear resistance than the as-sprayed coatings and substrate. The hard intermetallic laves phases which are amorphous (bulk metallic glass) in nature strengthen the coating at high temperatures. © 2018 IOP Publishing Ltd.
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    Experimental investigation and optimization of machining parameters for sustainable machining
    (Taylor and Francis Inc. 325 Chestnut St, Suite 800 Philadelphia PA 19106, 2018) Varghese, V.; Ramesh, M.R.; Dupadu, D.
    A detailed investigation on the effects of cutting parameters and different cooling environments on machinability of austenitic stainless steel AISI 304 is presented in this study. The need for sustainable manufacturing and better surface quality urged to explore the merits of cryogenic cooling over the other conventional cooling techniques. The end milling experiments were designed based on three parameter and three-level design considering dry, wet, and cryogenic machining environments to have a comparative study. The machinability studies such as surface roughness, tool wear, cutting forces, chip morphology, and chip reduction coefficient were investigated and compared with different machining environments. The machining parameters were optimized using Taguchi-based grey relational analysis. The cryogenic machining had the most influence on milling of AISI 304 steel and resulted in the reduction of cutting forces, surface roughness, and chip reduction coefficient in comparison with the conventional wet and dry machining. © 2018, © 2018 Taylor & Francis.
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    Influence of deep cryogenic treatment on performance of cemented carbide (WC-Co) inserts during dry end milling of maraging steel
    (Elsevier Ltd, 2019) Varghese, V.; Ramesh, M.R.; Dupadu, D.
    Cryogenic treatment has developed as a technique to improve the life of the cutting tool, especially tungsten carbide inserts. The present study investigates the effect of cryogenic treatment of cemented carbide (WC-Co) inserts at the different soaking period of 18 h (CT-18), 24 h (CT-24) and 32 h (CT-32) at a sub-zero temperature of ?196 °C. The soaking period plays a crucial role in improving the wear resistance of the cryogenically treated tools. It is vital to determine the critical soaking period for the cryogenic treatment of cemented carbides. The mechanical and metallurgical characterization of cryogenically treated cemented carbide insert is carried out to understand the changes in the microstructure, grain size, chemical composition, microhardness and electrical conductivity after cryogenic treatment. The end milling experiments on maraging steel under dry environment are carried out using cryogenically treated inserts at different holding time and untreated inserts (UT). The machining performance of treated and untreated inserts are compared with respect to tool wear, surface roughness and cutting forces. The results revealed that cryogenic treatment is effective in resisting tool wear even at high spindle speeds. The cryogenically treated inserts exhibited higher tool life, better surface finish and lower cutting forces during machining at different spindle speeds. The optimum soaking time for cryogenic treatment of WC-Co inserts is found to be 24 h (CT-24) beyond which there is no improvement in microhardness and wear resistance. © 2018
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    Characterisation and performance evaluation of TiSiN &tiAlSiN coatings by RF magnetron sputtering deposition during end milling of maraging steel
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Varghese, V.; Ramesh, M.R.; Dupadu, D.; Shaik, H.
    Monolayer nanostructured thin films of TiSiN & TiAlSiN were deposited on WC-Co milling inserts using RF magnetron sputtering for metal cutting. The alloy targets of TiSi (80/20 at%) & TiAlSi (34/56/10 at%) were used for the deposition in an Ar + N atmosphere. The deposition time and parameters are optimized to develop a uniform and homogenous coating. The mechanical and metallurgical properties are characterized to analyze the wear resistance of the coating. The machinability studies on MDN 250 maraging steel is carried out using TiSiN and TiAlSiN coated WC-Co inserts under dry and wet environment. The machining responses such as surface roughness, cutting force, tool wear and tool life are analyzed by varying spindle speed. The results showed that TiAlSiN coating had a higher wear resistance and machining performance compared to the TiSiN coating owing to the high hardness and plasticity index of the coating. © 2020 IOP Publishing Ltd.
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    Investigation on the performance of AlCrN and AlTiN coated cemented carbide inserts during end milling of maraging steel under dry, wet and cryogenic environments
    (Elsevier Ltd, 2019) Varghese, V.; K, A.; Ramesh, M.R.; Dupadu, D.
    The present study investigates the machining performance of AlCrN and AlTiN coated cemented carbide inserts during end milling of MDN 250 maraging steel. The mechanical and metallurgical characterization is carried out to determine the properties of the PVD coatings developed. The end milling experiments under dry, wet and cryogenic environment is carried out using coated uncoated inserts (UC) at different spindle speeds to evaluate the machining performance in terms of tool life, surface roughness and cutting forces. The coated inserts showed higher tool life, better surface finish, and low cutting forces during machining at different spindle speeds. It is found that the AlCrN coating had a better wear resistance and machining performance in comparison with AlTiN coating. The cryogenic environment reduced the surface roughness & cutting force and improved the tool life of the cutting tool compared to conventional dry and wet environment. It is revealed that coated tools along with cryogenic cooling can be employed for high-speed machining applications. © 2019 The Society of Manufacturing Engineers
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    Effect of microwave heating on microstructure and elevated temperature adhesive wear behavior of HVOF deposited CoMoCrSi-Cr3C2 coating
    (Elsevier B.V., 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    This research reports the improvement of high-temperature sliding wear resistance of a grade 15 titanium alloy protected by an HVOF sprayed CoMoCrSi-Cr3C2 coating. The coatings have been tested in as-sprayed condition and after a post-deposition microwave heating step. The powder feedstock has been manufactured by high energy ball milling. X-ray diffraction (XRD) and Scanning Electron Microscopy (SEM) equipped with the Energy Dispersive Spectroscopy (EDS) methods were used for coatings characterization. Surface roughness, microhardness, adhesion strength, and porosity of coatings were also measured. The wear test was conducted at an applied load of l0 N and 20 N with varying temperatures of 200 °C, 400 °C, and 600 °C under dry sliding conditions. Co3Mo2Si, Co7Mo6, Mo3Si, Co3Mo, and Co2Mo3 were the intermetallic laves phases generated in the CoMoCrSi feedstock during HEBM process. The microwave-fused coating exhibited metallurgical bonding, homogeneous structure, less porosity, and greater hardness as compared to as-sprayed coating. Microwave-treated coating revealed better wear property than an as-sprayed coating. This was mainly due to the intermetallic formation and metallurgical bonding in coatings. The fused coatings exhibit tribo-oxide layers during sliding action which was the main phenomenon of improving the wear resistance of the fused composite coatings. © 2019 Elsevier B.V.
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    Experimental investigation of cryogenic end milling on maraging steel using cryogenically treated tungsten carbide-cobalt inserts
    (Springer, 2019) Varghese, V.; Ramesh, M.R.; Dupadu, D.
    The cryogenic machining and cryogenic treatment have already emerged as the sustainable manufacturing process of the future generation. The cryogenic treatment improves the cutting tool life, but the high cutting temperature developed during high-speed machining reduces the effect of cryogenic treatment of cutting tool. This study investigates the possible improvements in cutting tool life by combining cryogenic cooling and cryogenic treatment. The authors believe that these two techniques can replace conventional machining approaches using dry and wet machining conditions using coated carbide tools. The tungsten carbide-cobalt inserts are cryogenically treated (CT) at a soaking temperature of ? 195.8 °C for a period of 24 h and are used to evaluate milling performance under dry, wet, and cryogenic cutting environments. The machining experiments are conducted on maraging steel MDN 250 using one factor at a time approach by varying spindle speed and keeping feed rate and depth of cut as constant. The cutting force, surface roughness, tool wear, and subsurface microhardness are some of the machining responses evaluated and compared with an untreated cutting tool (UT). The tool life improved up to 24% during cryogenic machining using CT tools at a spindle speed of 270 rpm. © 2019, Springer-Verlag London Ltd., part of Springer Nature.
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    Comparison of Microstructural and Sliding Wear Resistance of HVOF Coated and Microwave Treated CoMoCrSi-WC + CrC + Ni and CoMoCrSi-WC + 12Co Composite Coatings Deposited on Titanium Substrate
    (Springer Science and Business Media B.V. editorial@springerplus.com, 2020) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    CoMoCrSi-WC + CrC + Ni and CoMoCrSi-WC + 12Co composite coatings are coated on titanium substrate by high velocity oxygen fuel method (HVOF). Prior to spraying, CoMoCrSi feedstock are processed through high energy ball milling (HEBM) in order improve the intermetallic laves phases and to reduce its particle size. The processed feedstock exhibits amorphous nature by improving laves phases and particle size of 60.12 ?m. Microwave heating energy is utilized as post heat treatment technique to improve the mechanical and metallurgical properties of as-sprayed coatings. Fused coatings reveals better properties in terms of surface roughness, porosity, microhardness and adhesion strength compared to as-sprayed coatings. Metallurgical bonding is observed in case of fused coatings due to diffusion of substrate elements. Frictional and wear behaviors have been investigated by a pin on disc apparatus at temperatures of 200 °C, 400 °C, and 600 °C under normal loads of 10 N and 20 N. Both wear trace and friction coefficients of the fused coatings are smaller than as-sprayed coatings and substrate at all test temperatures. The wear traces of fused coatings decreased with increasing the surface temperature due to the lubricant effect of cobalt oxides formed on the sliding surface. As a result, cobalt based cermet coatings are highly recommended as a durability improvement coating for the protection of sliding surface, such as high speed spindle. © 2020, Springer Nature B.V.
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    Effect of Ball Milling on the Tensile Properties of Aluminum-Based Metal Matrix Nanocomposite Developed by Stir Casting Technique
    (SAE International, 2021) Ravikumar, K.S.; Ghanaraja, S.; Ramesh, M.R.
    Combining ball milling with stir casting in the synthesis of nanocomposites is found effective in increasing the strength and ductility of the nanocomposites. In the first step, the nanoparticles used as reinforcement are generated by milling a mixture of aluminum (Al) and manganese dioxide (MnO2) powders. A mixture of Al and MnO2 powders are mixed in the ratio of 1:2.4 by weight and milled at 300 rpm in a high-energy planetary ball mill for different durations of 120 min, 240 min, and 360 min to generate nano-sized alumina (Al2O3) particles. It is supposed that the powders have two different roles during milling, firstly, to generate nano-sized Al2O3 by oxidation at the high-energy impact points due to collision between Al and MnO2 particles, and secondly, to keep nano-sized Al2O3 particles physically separate by the presence of coarser particles. In the second step, 0.5 weight percent (wt%), 1 wt%, 1.5 wt%, and 2 wt% of the generated Al2O3 nanoparticles are reinforced in molten aluminum-magnesium (Al-Mg) alloy matrix via stir casting to synthesize nanocomposites. The effect of milling on the microstructure of the powder mixture before and after milling has been studied with the use of a scanning electron microscope (SEM) and X-ray diffraction analysis (XRD). The microstructure of the cast composites is examined under SEM, and the fractured surface of the tensile specimens is analyzed through SEM fractographs. Ball milling of reinforcement before adding to the melt brings considerable improvement in the integration and uniform dispersion of the milled particle in the Al-Mg alloy matrix melt, which leads to improvement in the strength and ductility of the cast nanocomposites. ©