Faculty Publications

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    HVOF sprayed Ni3Ti and Ni3Ti+(Cr3C2+20NiCr) coatings: Microstructure, microhardness and oxidation behaviour
    (Elsevier Ltd, 2018) Reddy, N.C.; Kumar, B.S.A.; Reddappa, H.N.; Ramesh, M.R.; Koppad, P.G.; Kord, S.
    This paper reports the development of Ni3Ti and Ni3Ti+(Cr3C2+20NiCr) coatings on AISI 420 stainless steel (MDN-420) and titanium alloy ASTM B265 (Ti-15) by HVOF technique. Microstructure, microhardness and high temperature oxidation behaviour of coatings were investigated. Microstructure of coatings was dense and displayed layers depicting lamellar structure. The microhardness of coatings was significantly higher than that of substrate owing to higher density and cohesive strength between individual splats of coating materials. Cyclic oxidation studies conducted on Ni3Ti and Ni3Ti+(Cr3C2+20NiCr) coatings showed oxide scale was composed of various oxides like NiO, NiCr2O4 and Cr2O3 phases. The formation of compact and protective NiO phase in case of Ni3Ti coatings; NiO and Cr2O3 phases in Ni3Ti+(Cr3C2+20NiCr) coatings stabilised the weight gain exhibited slow oxidation rate at higher temperatures. © 2017 Elsevier B.V.
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    Experimental Investigation on Effects of Wire Electro Discharge Machining of Ti50Ni45Co5 Shape Memory Alloys
    (Springer Netherlands rbk@louisiana.edu, 2018) Soni, H.; Narendranath, S.; Ramesh, M.R.
    TiNiCo shape memory alloy is most popular shape memory alloy for biomedical applications due to their outstanding properties such as shape memory effect, pseudoelasticity and transformation temperature. Machining of such kind of alloys is very difficult through conventional machining process is very difficult because they may affect their internal properties of these alloys. However conventional machining processes give poor surface quality during the machining hence non-conventional machining processes such as (wire electro discharge machining, water jet machining and electro discharge machining etc.) are more suitable for machining of such kind of alloy. From the literature it has been found that Wire electro discharge machining (WEDM) is more suitable non-conventional machining process for such kind of alloy. Present study exhibits the effects WEDM characteristics of Ti50Ni45Co5 shape memory alloy. L-9 orthogonal array has been created by using Taguchi as a design method for machining of selected alloy and machined surface characterization has been carried out at the optimized process parameters with respect to microstructures, surface topography, microhardness, XRD analysis and residual stresses. To find the optimum setting of the input process parameters a couple of optimization techniques are used, namely principal component analysis (PCA) and Gray relational analysis (GRA) technique. 125?s pulse on time (Ton), 35?s pulse off time (Toff) and 40V servo voltage (SV) were found as an optimal setting for the higher material removal rate (MRR) with better surface roughness (SR) in the present study. Moreover, characterization of the machined surface is performed with respect to microstructures, surface topography, microhardness analysis, XRD and residual stresses. Harder surface observed near the cutting edge and TiNio3 Tio2 and CuZn were noticed on the surface of machined component through XRD analysis. However, compressive residual stress has been noticed on the machined surface during WEDM process. © 2018, Springer Science+Business Media B.V., part of Springer Nature.
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    Influence of deep cryogenic treatment on performance of cemented carbide (WC-Co) inserts during dry end milling of maraging steel
    (Elsevier Ltd, 2019) Varghese, V.; Ramesh, M.R.; Dupadu, D.
    Cryogenic treatment has developed as a technique to improve the life of the cutting tool, especially tungsten carbide inserts. The present study investigates the effect of cryogenic treatment of cemented carbide (WC-Co) inserts at the different soaking period of 18 h (CT-18), 24 h (CT-24) and 32 h (CT-32) at a sub-zero temperature of ?196 °C. The soaking period plays a crucial role in improving the wear resistance of the cryogenically treated tools. It is vital to determine the critical soaking period for the cryogenic treatment of cemented carbides. The mechanical and metallurgical characterization of cryogenically treated cemented carbide insert is carried out to understand the changes in the microstructure, grain size, chemical composition, microhardness and electrical conductivity after cryogenic treatment. The end milling experiments on maraging steel under dry environment are carried out using cryogenically treated inserts at different holding time and untreated inserts (UT). The machining performance of treated and untreated inserts are compared with respect to tool wear, surface roughness and cutting forces. The results revealed that cryogenic treatment is effective in resisting tool wear even at high spindle speeds. The cryogenically treated inserts exhibited higher tool life, better surface finish and lower cutting forces during machining at different spindle speeds. The optimum soaking time for cryogenic treatment of WC-Co inserts is found to be 24 h (CT-24) beyond which there is no improvement in microhardness and wear resistance. © 2018
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    Microstructure and tribological characteristics of APS sprayed NiCrBSi/flyash cenosphere/Cr2O3 and NiCrBSi/flyash cenosphere/Mo composite coatings at elevated temperatures
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Nagabhushana, N.; Rajanna, S.; Mathapati, M.; Ramesh, M.R.; Koppad, P.G.; Reddy, N.C.
    In the present investigation NiCrBSi/flyash/Cr2O3 and NiCrBSi/flyash/Mo composite coatings are developed using atmospheric plasma spray technique on superni 76 alloy. Coatings are characterized in terms of microstructure, phase analysis, and microhardness. Tribological properties of the coatings are evaluated using a pin on disc tribometer. Test is conducted under dry sliding conditions at room temperature, 200 °C, 400 °C, and 600 °C respectively. Microstructure and worn surfaces of the coatings are analyzed by utilizing Scanning Electron Microscope (SEM) where in phase analysis is carried out using x-ray diffractometer (XRD). XRD results revealed the presence of ?-Ni as primary phase along with Ni3B, Cr7C3, SiO2 and Al2O3 as minor phases in both the NiCrBSi/flyash/Cr2O3 and NiCrBSi/flyash/Mo coatings. Among the two coatings, Mo composite coating exhibited lower porosity and higher microhardness. The friction coefficient of both the coatings decreased with increasing temperature. The wear rate is found to decrease at lower temperatures but increased at a higher temperature (>400 °C) for Cr2O3 composite coating wherein Friction coefficient is decreased with increase in the temperature for Mo composite coatings. The worn surface analysis conducted revealed abrasive wear at lower temperatures while the transition from abrasive to adhesive is observed at higher temperatures. © 2019 IOP Publishing Ltd.
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    High-temperature wear and frictional behavior of partially oxidized Al with NiCr composite coating
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Medabalimi, S.R.; Ramesh, M.R.; Kadoli, R.
    The influence of composite coating in improving wear and frictional behavior from room temperature to 600 °C was investigated. Partially oxidized Al powder was prepared with a flame spray process by spraying pure Al powder into distilled water. The composite powder is the mixture of 30 weight percent of partially oxidized Al and 70 weight percent of NiCr alloy powder. The composite powder was subsequently coated on MDN321 steel by air plasma spray process. The composite coatings are characterized with respect to adhesion strength, porosity, micro-hardness, and density. Wear and frictional behavior of coatings are evaluated under disc speed of 1 and 2 m s-1, loads of 10, 20 and 30 N and 3000 m sliding distance. The test results indicated that at room temperature, frictional heat generated due to applied load produce three-body abrasion at the interface caused to increase the wear and friction in the coating. The oxide film formed at high temperature due to plastic deformation avoids surface degradation at the interface and reduce the wear and friction. The worn surfaces at 600 °C consist phases of ?-Al2O3, NiO, and Cr3O. These phases are contributing to improving the wear resistance of the coating more than 4-times compared to uncoated steels under varying load and sliding velocities. The coefficient of friction reduced with increase in temperature due to generated oxides act as lubricants at the interface. © 2019 IOP Publishing Ltd.
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    Microstructure and tribological behavior of flame sprayed and microwave fused CoMoCrSi/CoMoCrSi-Cr3C2 coatings
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    This present work deals with the investigation of dry sliding wear behavior of CoMoCrSi and CoMoCrSi-Cr3C2 depositing on titanium substrate through Flame spray process, subsequently fused by the microwave hybrid heating process. Prior to the deposition of the coating, CoMoCrSi powder is milled by using high energy ball milling (HEBM) process and later 30% of Cr3C2 powder is added. Microstructural features and phase analysis of milled powders, as-coated and microwave fused coatings are inspected by using SEM with EDS and XRD process respectively. The coatings before and after fusing are tested for microhardness and bond strength by using a Vickers microhardness and universal tensile machines respectively. Dry sliding wear behavior of coatings before and after fusing is conducted against alumina counter face at ambient and elevated temperatures, also normal load is varied. The wear mechanism of both coatings is examined by employing XRD, SEM-EDS techniques. The fused coatings exhibit lower friction and better wear resistance compared with as-deposited coatings. The detailed results of each test of their coatings are discussed in this paper. © 2018 IOP Publishing Ltd.
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    Effects of Wire Electro-Discharge Machining Process Parameters on the Machined Surface of Ti 50 Ni 49 Co 1 Shape Memory Alloy
    (Springer Netherlands rbk@louisiana.edu, 2019) Soni, H.; Narendranath, S.; Ramesh, M.R.
    Wire electro-discharge machining is one of the advanced machining processes which can machine all conductive materials without changing their internal properties. Pulse on time and servo voltage are the most influential process parameters of wire electro-discharge machining. In the present study, attempts have been made to study the effects of these process parameters on the machined surface of Ti 50 Ni 49 Co 1 shape memory alloy by adopting a two process parameters experimental design approach. Cutting speed and surface roughness were considered as output parameters; surface crack density, microhardness and XRD analysis were carried out at the higher and lower values of these parameters. Higher surface crack density has been found at high values of cutting speed (125 ?s pulse on time and 20 V servo voltage) while it is lower at the lower value of cutting speed (105 ?s pulse on time and 60 V servo voltage). Moreover, a harder surface was found near the machined surface. By XRD analysis it was found that the crystal size of the WED machined surface was reduced at high T on and lower SV. © 2018, Springer Science+Business Media B.V., part of Springer Nature.
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    Investigation of dry sliding wear properties of multi-directional forged Mg–Zn alloys
    (National Engg. Reaserch Center for Magnesium Alloys zhangdingfei@cqu.edu.cn, 2019) Ramesh, S.; Anne, G.; Shivananda Nayaka, H.S.; Sahu, S.; Ramesh, M.R.
    Effect of multi-directional forging (MDF) on wear properties of Mg–Zn alloys (with 2, 4, and 6 wt% Zn) is investigated. Dry sliding wear test was performed using pin on disk machine on MDF processed and homogenized samples. Wear behavior of samples was analyzed at loads of 10 N and 20 N, with sliding distances of 2000 m and 4000 m, at a sliding velocity of 3 m/s. Microstructures of worn samples were observed under scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and x-ray diffraction (XRD) and the results were analyzed. Mechanical properties were evaluated using microhardness test. After 5 passes of MDF, the average grain size was found to be 30 ± 4 µm, 22 ± 3 µm, and 18 ± 3 µm, in Mg–2%Zn, Mg–4%Zn, and Mg–6%Zn alloys, respectively, with significant improvement in hardness in all cases. Wear resistance was improved after MDF processing, as well as, with increment in Zn content in Mg alloy. However, it decreased when the load and the sliding distance increased. Worn surface exhibited ploughing, delamination, plastic deformation, and wear debris along sliding direction, and abrasive wear was found to be the main mechanism. © 2019
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    Development and Sliding Wear Behavior of Co-Mo-Cr-Si Cladding through Microwave Heating
    (Springer editorial@springerplus.com, 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    The aim of the present study is to improve the sliding wear resistance of pure titanium grade-2 substrate by developing CoMoCrSi (Tribaloy T400) cladding on it by using microwave hybrid heating technique. The developed cladding is characterized by microstructural features, phase analysis, measurement of microhardness by employing a scanning electron microscope (SEM), X-ray diffraction (XRD) and Vickers microhardness. The cladding and substrate are subjected to sliding wear test against alumina counterpart at elevated temperatures under dry conditions using a pin on disc tribometer. The test is performed by varying normal load and temperatures, whereas sliding speed is maintained constant. The developed clad shown partial melting of CoMoCrSi powders and obtained sound metallurgical bonding with the substrate. The high specific energy of microwave diluted the substrate atoms into cladding region which forms Cr3C2, Co3Ti, and TiC, phases confirmed by phase analysis. The cladding obtained better porosity and microhardness are 1.5 ± 0.2% ?m and 760 ± 35 Hv respectively. The substrate exhibits low microhardness of 182 ± 25 Hv. The cladding exhibits 6 times of lower volume loss and 70.14% of less wear rate with respect to the substrate. The cladding experienced least coefficient of friction is 0.55 compared with the substrate. The worn surfaces of cladding and substrate are examined. The detailed mechanism of wear is discussed in this paper. © 2019, Springer Nature B.V.
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    Experimental investigation of cryogenic end milling on maraging steel using cryogenically treated tungsten carbide-cobalt inserts
    (Springer, 2019) Varghese, V.; Ramesh, M.R.; Dupadu, D.
    The cryogenic machining and cryogenic treatment have already emerged as the sustainable manufacturing process of the future generation. The cryogenic treatment improves the cutting tool life, but the high cutting temperature developed during high-speed machining reduces the effect of cryogenic treatment of cutting tool. This study investigates the possible improvements in cutting tool life by combining cryogenic cooling and cryogenic treatment. The authors believe that these two techniques can replace conventional machining approaches using dry and wet machining conditions using coated carbide tools. The tungsten carbide-cobalt inserts are cryogenically treated (CT) at a soaking temperature of ? 195.8 °C for a period of 24 h and are used to evaluate milling performance under dry, wet, and cryogenic cutting environments. The machining experiments are conducted on maraging steel MDN 250 using one factor at a time approach by varying spindle speed and keeping feed rate and depth of cut as constant. The cutting force, surface roughness, tool wear, and subsurface microhardness are some of the machining responses evaluated and compared with an untreated cutting tool (UT). The tool life improved up to 24% during cryogenic machining using CT tools at a spindle speed of 270 rpm. © 2019, Springer-Verlag London Ltd., part of Springer Nature.