Faculty Publications
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Item ANN and RSM modeling methods for predicting material removal rate and surface roughness during WEDM of Ti50Ni40Co10 shape memory alloy(AMSE Press 16 Avenue Grauge Blanche Tassin-la-Demi-Lune 69160, 2017) Soni, H.; Narendranath, S.; Ramesh, M.R.Present study exhibits the comparison between experimental and predicted values. Where response surface method (RSM) and artificial neural network (ANN) were used as predictor for the prediction of wire electro discharge machining (WEDM) responses such as the material removal rate (MRR) and surface roughness (SR) during the machining of Ti50Ni40Co10 shape memory alloy. It has been noticed from the literature survey that pulse on time and servo voltage are most important process parameters for the machining of TiNiCo shape memory alloy, hence there are five levels of these process parameters were chosen for the present study. For the present study selected alloy has been developed through vacuum arc melting and L-25 orthogonal array has been created by using Taguchi design of experiment (DOE) for experimental plan. During the present study ANN predicted values have been found to very close to experimental values compare to RSM predicted values, hence it can be say that ANN predictor gives more accurate values compare to RSM predicted values. © 2017 AMSE Press. All rights reserved.Item Elevated temperature solid particle erosion behaviour of carbide reinforced CoCrAlY composite coatings(Institute of Physics Publishing helen.craven@iop.org, 2018) Nithin, H.S.; Desai, V.; Ramesh, M.R.CoCrAlY+WC-Co and CoCrAlY+Cr3C2-NiCr coatings are deposited on nickel based alloy using atmospheric plasma spray technique. Mechanical properties such as microhardness, adhesion strength and fracture toughness of coatings are evaluated. Elevated temperature solid particle erosion behaviour of these coatings are investigated at 600 °C using alumina erodent at 30 and 90° impact angle. Coatings are characterized utilizing Scanning electron microscope (SEM), x-ray diffraction (XRD) and Energy dispersive spectroscopy (EDS). CoCrAlY+WC-Co coating shows higher hardness, adhesion strength and fracture toughness than CoCrAlY+Cr3C2-NiCr coating. CoCrAlY+WC-Co coating exhibited approximately 3 times higher erosion resistance than CoCrAlY+Cr3C2-NiCr coating at 90° and 30° impact angles. SEM images of eroded surfaces of coatings reveals the combination of ductile and brittle fracture. CoCrAlY+Cr3C2-NiCr coating shows severe cracks, craters, carbide pull out and chipping than CoCrAlY+WC-Co coating. High temperature erosion is a combination of simultaneous building up of material by oxidation and removal of material by erosion process. Thus reforming the erosion process to oxidation modified erosion process. © 2018 IOP Publishing Ltd.Item Influence of microwave hybrid heating on the sliding wear behaviour of HVOF sprayed CoMoCrSi coating(Institute of Physics Publishing helen.craven@iop.org, 2018) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.CoMoCrSi superalloy powder (Tribaloy-T400) consists of intermetallic laves phase and primary eutectic phase of Co-rich solid solution. Processing of Tribaloy-T400 powder is carried out through high-energy ball milling (HEBM) technique to obtain a higher volume fraction of intermetallic laves phases. The feedstock is sprayed using high-velocity-oxy-fuel (HVOF) process on titanium grade-15 substrate. The coating microstructure is homogenized by microwave hybrid heating technique. Characterization of feedstock, as-sprayed and microwave fused coatings is done by using Scanning Electron Microscopy (SEM), Energy dispersive spectroscopy (EDS) and x-ray Diffraction (XRD). Porosity, surface roughness, microhardness, and bond strength are measured. Adhesive wear behavior of the coatings under the dry sliding condition is evaluated at an applied load of l0 and 20 N and temperature of 200, 400 and 600 °C Fused coating exhibit higher wear resistance than the as-sprayed coatings and substrate. The hard intermetallic laves phases which are amorphous (bulk metallic glass) in nature strengthen the coating at high temperatures. © 2018 IOP Publishing Ltd.Item Cyclic Oxidation and Hot Corrosion Behavior of Plasma-Sprayed CoCrAlY + WC-Co Coating on Turbine Alloys(Springer New York LLC barbara.b.bertram@gsk.com, 2018) Nithin, H.S.; Vijay, D.; Ramesh, M.R.Components in energy-producing systems suffer a variety of degradation processes such as oxidation and molten salt-induced corrosion as a consequence of complex multi-component gaseous environment. Coatings provide a composition that will grow the protective scale at high temperatures having long-term stability. Plasma spraying was used to deposit CoCrAlY + WC-Co composite coatings on turbine alloys of Hastelloy X and AISI 321. The thermocyclic oxidation behavior of coated alloys was investigated in static air and in molten salt (Na2SO4-60%V2O5) environment at 700 °C. The thermogravimetric technique was used to approximate the kinetics of oxidation in 50 cycles, each cycle consisting of heating and cooling. X-ray diffraction and SEM/EDAX techniques are used to characterize the oxide scale formed. Coated alloys showed a lower corrosion rate as compared to uncoated alloys. The coatings subjected to oxidation and hot corrosion showed slow scale growth kinetics. Preferential oxidation of Co, Cr, W and its spinel blocks the transport of oxygen and corrosive species into the coating by providing a barrier, thereby making the oxidation rate to reach steady state. As compared to the substrate alloys, coatings show better hot corrosion resistance. © 2018, ASM International.Item Experimental Investigation on Effects of Wire Electro Discharge Machining of Ti50Ni45Co5 Shape Memory Alloys(Springer Netherlands rbk@louisiana.edu, 2018) Soni, H.; Narendranath, S.; Ramesh, M.R.TiNiCo shape memory alloy is most popular shape memory alloy for biomedical applications due to their outstanding properties such as shape memory effect, pseudoelasticity and transformation temperature. Machining of such kind of alloys is very difficult through conventional machining process is very difficult because they may affect their internal properties of these alloys. However conventional machining processes give poor surface quality during the machining hence non-conventional machining processes such as (wire electro discharge machining, water jet machining and electro discharge machining etc.) are more suitable for machining of such kind of alloy. From the literature it has been found that Wire electro discharge machining (WEDM) is more suitable non-conventional machining process for such kind of alloy. Present study exhibits the effects WEDM characteristics of Ti50Ni45Co5 shape memory alloy. L-9 orthogonal array has been created by using Taguchi as a design method for machining of selected alloy and machined surface characterization has been carried out at the optimized process parameters with respect to microstructures, surface topography, microhardness, XRD analysis and residual stresses. To find the optimum setting of the input process parameters a couple of optimization techniques are used, namely principal component analysis (PCA) and Gray relational analysis (GRA) technique. 125?s pulse on time (Ton), 35?s pulse off time (Toff) and 40V servo voltage (SV) were found as an optimal setting for the higher material removal rate (MRR) with better surface roughness (SR) in the present study. Moreover, characterization of the machined surface is performed with respect to microstructures, surface topography, microhardness analysis, XRD and residual stresses. Harder surface observed near the cutting edge and TiNio3 Tio2 and CuZn were noticed on the surface of machined component through XRD analysis. However, compressive residual stress has been noticed on the machined surface during WEDM process. © 2018, Springer Science+Business Media B.V., part of Springer Nature.Item Effects of Wire Electro-Discharge Machining Process Parameters on the Machined Surface of Ti 50 Ni 49 Co 1 Shape Memory Alloy(Springer Netherlands rbk@louisiana.edu, 2019) Soni, H.; Narendranath, S.; Ramesh, M.R.Wire electro-discharge machining is one of the advanced machining processes which can machine all conductive materials without changing their internal properties. Pulse on time and servo voltage are the most influential process parameters of wire electro-discharge machining. In the present study, attempts have been made to study the effects of these process parameters on the machined surface of Ti 50 Ni 49 Co 1 shape memory alloy by adopting a two process parameters experimental design approach. Cutting speed and surface roughness were considered as output parameters; surface crack density, microhardness and XRD analysis were carried out at the higher and lower values of these parameters. Higher surface crack density has been found at high values of cutting speed (125 ?s pulse on time and 20 V servo voltage) while it is lower at the lower value of cutting speed (105 ?s pulse on time and 60 V servo voltage). Moreover, a harder surface was found near the machined surface. By XRD analysis it was found that the crystal size of the WED machined surface was reduced at high T on and lower SV. © 2018, Springer Science+Business Media B.V., part of Springer Nature.Item Elevated temperature tribological performance of non-equiatomic CoCrNiTiWx high entropy alloy coatings developed by mechanical alloying and high-velocity oxy-fuel spray(Elsevier B.V., 2024) Addepalli, S.N.; Joladarashi, S.; Ramesh, M.R.High entropy alloys (HEA) have applications in multiple fields owing to their exceptional mechanical and physical properties. In the current study, mechanical alloyed CoCrNiTiWx (x; a molar fraction, x = 0.5 and 1.5) HEA feedstock powders were deposited on maraging steel substrate using high-velocity oxy-fuel spray (HVOF). The phase evolution and the microstructure of the milled powders and as-sprayed coatings were analysed by X-ray diffraction (XRD) and scanning electron microscope (SEM). The tribological behaviour of CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings at elevated temperatures was studied extensively using a Pin-on-Disc tribometer. The CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings retained the BCC solid solution phases formed during the milling stage. However, additional oxide and intermetallic phases were formed owing to the in-flight oxidation and high temperatures experienced during the HVOF deposition. The deposited coatings exhibited a lamellar structure and good mechanical bonding with the substrate. The porosities of CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings were found to be 1.69 ± 0.32 % and 1.51 ± 0.37 % respectively.Consequently, the CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings displayed average microhardness values of 863 ± 52 HV0.3 and 1025 ± 39 HV0.3, respectively. Further, the wear rates of coatings exhibited a significant reduction at elevated temperatures, owing to the formation of TiO2, NiCr2O4 oxide tribofilms for CoCrNiTiW0.5, and CoCr2O4, NiWO4, WO3 oxides for CoCrNiTiW1.5. The specific wear rate of CoCrNiTiW0.5 HEA coating dropped by 73.6 % from 22.7 ± 2.6 × 10−6 mm3/N-m to 5.99 ± 1.9 × 10−6 mm3/N-m, while CoCrNiTiW1.5 dropped by 78.8 % from 11.86 ± 3.5 × 10−6 mm3/N-m to 2.51 ± 1.5 × 10−6 mm3/N-m, with a rise in the temperature from RT to 600 °C. Likewise, The frictional coefficients of CoCrNiTiW0.5 HEA dropped from 0.504 ± 0.015 to 0.397 ± 0.005, while CoCrNiTiW1.5 HEA dropped from 0.578 ± 0.025 to 0.471 ± 0.004, with a rise in temperature from RT to 600 °C. At room temperature, the wear mechanisms of the as-sprayed CoCrNiTiWx coatings were dominated by adhesive wear. However, at elevated temperatures, a shift towards oxidative wear was observed. © 2023 Elsevier B.V.Item Elevated temperature wear and friction performance of WC-CoCr/Mo and WC-Co/NiCr/Mo coated Ti-6Al-4V alloy(Elsevier Inc., 2024) Behera, N.; Ramesh, M.R.; Rahman, M.R.The effect of adding Mo to WC-based coatings on the microstructure and dry sliding wear performance at elevated temperatures is investigated. The WC-based coatings are deposited using a high-velocity oxy-fuel process on the titanium-31 substrate. The coating was characterized by microstructure, microhardness, porosity, surface roughness, density, and bond strength. The wear and friction behavior of coatings was evaluated using a ball-on disc tribometer at temperatures of 200, 400, 600, and 800 °C and loads of 20 and 30 N. SEM-EDS and an optical profilometer were utilized to evaluate the wear rate and mechanism. The microhardness and bond strength of WC-CoCr/10%Mo coating is more than that of WC-Co/20%NiCr/10%Mo coatings. The WC-CoCr, WC-CoCr/10%Mo, and WC-Co/20%NiCr/10%Mo coatings exhibited decreasing wear rates up to 600 °C, transitioning to an increase at 800 °C. The oxide phases of CoWO4 WO3 MoO3, CoMoO4, and NiMoO4, formed at 600 °C, aid in reducing the rate of wear and friction coefficient. However, the wear rate slightly increased at 800 °C due to vigorous oxidation and softness of coatings. The friction coefficient of WC-CoCr, WC-CoCr/10%Mo, and WC-Co/20%NiCr/10%Mo coating decreases with increasing temperatures due to the lubricating properties of oxide phases on the worn surface. The WC-CoCr/10%Mo coating demonstrates a lower friction and wear rate than the WC-CoCr and WC-Co/20%NiCr/10%Mo coating. At 200 °C, the predominant wear mechanisms were abrasive and fatigue wear, while at 800 °C, oxidative wear, abrasive wear, and adhesive wear were observed. © 2024Item Characterization and evaluation of carbide-based composite coatings for high-temperature wear resistance on Titanium substrate(SAGE Publications Ltd, 2025) Behera, N.; Ramesh, M.R.Titanium alloys are used in the automotive and aerospace industries, but perform poorly at high temperatures due to inadequate wear and friction properties. This study investigates Cr3C2-25%CoNiCrAlY and WC-CoCr coatings applied via High-velocity oxygen Fuel on a titanium-31 substrate. Coatings were evaluated from 200–800?°C under 20?N and 30?N using a ball-on-disc tribometer. Characterization techniques included scanning electron microscope, X-ray diffraction, microhardness, porosity, and bond strength. WC-CoCr coating showed higher hardness and bond strength than Cr3C2-25%CoNiCrAlY. Both coatings exhibited reduced wear rates until 600?°C, after which the wear rates increased at 800?°C due to enhanced oxidation. The coefficient of Friction decreased with increasing temperature. At 600?°C, oxide phases helped reduce wear and friction. WC-CoCr coating shows better wear resistance than Cr3C2-25%CoNiCrAlY coating and the substrate. Wear mechanisms changed from abrasive and fatigue at 200?°C to oxidative and adhesive at 800?°C. Volumetric ball loss was higher for WC-CoCr due to its greater hardness. © The Author(s) 2025Item Studies on high temperature erosion behavior of HVOF-sprayed (Cr?C?-NiCr)Si and WC-Co/NiCrAlY composite coatings(Elsevier Ltd, 2025) Medabalimi, S.; Hebbale, A.M.; Gudala, S.; Rokkala, U.; Ramesh, M.R.The present study investigates the high temperature erosion behavior of HVOF sprayed composite coatings on T11 steel substrates by studying (Cr?C?-NiCr)Si and WC-Co/NiCrAlY coatings. Phase composition, cross sectional microstructure, mechanical properties, and erosion resistance were analyzed by XRD, EDS, SEM and three-dimensional optical profilography. The results demonstrate that the WC-Co/NiCrAlY coating has higher erosion resistance and oxidation stability for all temperatures and impact angles tested. Its enhanced performance in high temperature and erosive conditions is attributable to the formation of stable protective oxides such as Al?O? and Cr?O? and intermetallic phases such as Ni?Al and Cr?C?. The NiCrAlY matrix prevents significant decarburization of WC particles, and hence phase stability and oxidation resistance. The (Cr?C?-NiCr)Si coating has higher microhardness due to silicide phases, but is more vulnerable to direct impacts and inferior oxidation resistance. The phase transformations for both coatings are favorable at elevated temperatures which enhances erosion resistance. The WC-Co/NiCrAlY coating is smooth and shallower in erosion craters and is perfectly suited for harsh environments demanding high toughness, impact resistance and oxidation stability. For applications in which high hardness is needed in less severe conditions, the (Cr?C?-NiCr)Si coating is more suitable. © 2024