Faculty Publications
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Item High-Temperature Erosive Behavior of Plasma Sprayed Cr3C2-NiCr/Cenosphere Coating(Springer New York LLC barbara.b.bertram@gsk.com, 2018) Mathapati, M.; Doddamani, M.; Ramesh, M.R.This research examines the deposition of Cr3C2-NiCr/cenosphere and Cr3C2-NiCr coatings on MDN 321 steel through the process of plasma spray. In this process, the solid particle erosion test is established at 200, 400, 600 °C with 30° and 90° impact angles. Alumina erodent is adopted to investigate the erosive behavior of the coating at higher temperatures. The properties of the Cr3C2-NiCr/cenosphere coating are established based on the microhardness, the adhesive strength, the fracture toughness, and the ductility. To quantify volume loss as a result of erosion, an optical profilometer is used. At higher temperature, decrease in the erosion volume loss of Cr3C2-NiCr/cenosphere and Cr3C2-NiCr coatings is observed. The erosion-resistive property of Cr3C2-NiCr/cenosphere coating is higher than that of MDN 321 steel by 76%. This property is influenced by high-temperature stability of mullite, alumina, and protective oxide layer that is formed at elevated temperatures. The morphology of eroded coating discloses a brittle mode of material removal. © 2018, ASM International.Item Microstructure and tribological behavior of plasma sprayed NiCrAlY/WC-Co/cenosphere/solid lubricants composite coatings(Elsevier B.V., 2018) Doddamani, M.; Mathapati, M.; Ramesh, M.R.Present investigation deal with NiCrAlY/WC-Co/Cenosphere/MoS2/CaF2, NiCrAlY/WC-Co/Cenosphere/MoS2/CaSO4 and NiCrAlY/WC-Co/Cenosphere coatings deposited on MDN 321 steel using atmospheric plasma spraying. Tribological properties of MDN 321 steel and coatings are evaluated from room temperature (RT) to 600 °C under dry lubrication conditions using a pin on disc high-temperature tribometer. Scanning Electron Microscopy (SEM), X-ray diffraction (XRD) and Energy Dispersive Spectroscopy (EDS) are used to characterize the coatings. Presence of cenospheres in these coatings might effectively reduce wear acting as localized regions accumulating wear debris. The result shows that wear rate of all the coatings are lower as compared to MDN 321 substrate at all the test conditions. NiCrAlY/WC-Co/Cenosphere/MoS2/CaF2 and NiCrAlY/WC-Co/Cenosphere/MoS/CaSO4 coatings registered lower friction coefficient as compared to NiCrAlY/WC-Co/Cenosphere coating and MDN 321 substrate. Characterization of the NiCrAlY/WC-Co/Cenosphere/MoS2/CaF2 and NiCrAlY/WC-Co/Cenosphere/MoS2/CaSO4 coatings worn out surface suggests that MoS2 provides lubrication at 200 °C and formation of CaMoO4, MoO3 through tribo chemistry reaction at higher temperature provides lubrication at 600 °C. SEM micrograph of worn surface demonstrates that the main wear mechanism is plowing and delamination. © 2018 Elsevier B.V.Item Plasma sprayed Cr3C2-NiCr/fly ash cenosphere coating: Cyclic oxidation behavior at elevated temperature(Institute of Physics Publishing helen.craven@iop.org, 2018) Doddamani, M.; Mathapati, M.; Ramesh, M.R.Oxidation is one of the major degradation phenomena observed in components subjected to higher temperatures like in thermal power plants (boiler tubes), steam and gas turbines blades etc. Developing protective coatings for such components mitigate oxidation. In the present study, plasma spray technique is utilized to deposit the Cr3C2-NiCr/Cenospheres coating on MDN 321 steel substrate. Thermo cyclic oxidation test is conducted at 600 °C (20 cycles) on both the coating and MDN 321 steel substrate. The thermogravimetric methodology is employed to estimate the oxidation kinetics. Energy Dispersive Spectroscopy (EDS), x-ray Diffraction (XRD), Scanning Electron Microscope (SEM) and x-ray mapping technique is employed to characterize the oxidized samples. Cr3C2-NiCr/Cenosphere coating displayed lower rate of oxidation as compared to substrate implying its suitability in high-temperature applications. Protective oxides like Al2O3, Cr2O3, and NiCr2O4 are observed on the uppermost layer of the coating lowering the oxidation rate in the developed coating. © 2018 IOP Publishing Ltd.Item Experimental investigation and optimization of machining parameters for sustainable machining(Taylor and Francis Inc. 325 Chestnut St, Suite 800 Philadelphia PA 19106, 2018) Varghese, V.; Ramesh, M.R.; Dupadu, D.A detailed investigation on the effects of cutting parameters and different cooling environments on machinability of austenitic stainless steel AISI 304 is presented in this study. The need for sustainable manufacturing and better surface quality urged to explore the merits of cryogenic cooling over the other conventional cooling techniques. The end milling experiments were designed based on three parameter and three-level design considering dry, wet, and cryogenic machining environments to have a comparative study. The machinability studies such as surface roughness, tool wear, cutting forces, chip morphology, and chip reduction coefficient were investigated and compared with different machining environments. The machining parameters were optimized using Taguchi-based grey relational analysis. The cryogenic machining had the most influence on milling of AISI 304 steel and resulted in the reduction of cutting forces, surface roughness, and chip reduction coefficient in comparison with the conventional wet and dry machining. © 2018, © 2018 Taylor & Francis.Item Tribological performance of wire arc additive manufactured 347 austenitic stainless steel under unlubricated conditions at elevated temperatures(Elsevier Ltd, 2020) Duraisamy, R.; Subramaniyan, S.; Kannan, A.; Siva Shanmugam, N.; Sankaranarayanasamy, K.; Ramesh, M.R.Wire Arc Additive Manufacturing (WAAM) is an effective metal additive manufacturing process. In this research, 347 Austenitic Stainless Steel (ASS) walls were manufactured with ER347 consumable material. The microstructure of the WAAM processed 347 plate is entirely heterogeneous with changing grain morphology along the building direction and this is attributed to the complex cyclic thermal history during WAAM process. The microstructure is composed of columnar, cellular and equiaxed structures at various regions. The hardness decreased gradually from bottom to top along the building direction. The volume fraction of ferrite ranged from 0.5% to 4.2% at various regions and the presence of niobium carbide (NbC) was confirmed. The aim of the current work is to provide an outline of the WAAM processed 347 steel under dry sliding conditions at elevated temperatures. The elevated temperature wear mechanism has mild oxidative wear characteristic due to the formation of tribo-oxides on the wearing and sliding surfaces. However, the average coefficient of friction (COF) is lower for the WAAM processed 347 compared to 347 substrate. In all cases after initial running-in, the wear debris from the wearing and sliding surface forms mechanically mixed composite layer of tribo-oxides (Fe2O3, Fe3O4 and Al2O3). The worn surface at 200 °C presents different wear behavior compared to the samples at 400 °C and 600 °C. The wear at 200 °C is a typical adhesive wear, while the wear at 400?600 °C is mild oxidative wear. The increase in the percentage of Fe3O4 helps to heal the wear surface by forming a mechanically mixed composite layer. The characteristics of mild oxidative wear were elucidated. © 2020 The Society of Manufacturing EngineersItem Phase evolution and high-temperature wear behavior of non-equiatomic metastable CoCrNiTiMox HEA coatings fabricated by high-velocity oxy-fuel technique(Elsevier Ltd, 2023) Addepalli, S.N.; Joladarashi, S.; Ramesh, M.R.The current research aims to enhance the tribological performance of maraging steels at high temperatures by surface modification techniques. CoCrNiTiMox (x; molar fraction, x = 0.5, 1.5) high-entropy alloy (HEA) coatings with dense lamellar microstructures were deposited onto maraging steels using high-velocity oxy-fuel spray (HVOF). In order to achieve a uniform distribution of constituent elements for thermal spray deposition, mechanical alloying was employed to synthesize the HEA feedstock. The phases and microstructure of the synthesized HEA powder, as-sprayed coatings, and worn surfaces were examined using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The as-sprayed HEA coatings exhibited metastability, with a BCC phase solid solution, NiTiO3 spinel, and an intermetallic MoNi phase for CoCrNiTiMo0.5 and Co2Mo3 phase for CoCrNiTiMo1.5. The average microhardness of CoCrNiTiMo0.5 and CoCrNiTiMo1.5 HEA coatings were 841 ± 62 HV0.3 and 952 ± 23 HV0.3, respectively. The specific wear rate and friction coefficients of CoCrNiTiMox HEA coatings exhibited a decreasing trend with an increase in temperature, owing to the formation of tribofilms on the worn surface. X-ray diffraction studies revealed the formation of NiMoO4 spinel for CoCrNiTiMo0.5 and MoO2, Co3O4 phases for CoCrNiTiMo1.5 HEA at a wear temperature of 600 °C. The investigation of worn surfaces showed a transformation in wear mechanisms from abrasive wear at room temperature to oxidative wear with mild fatigue at elevated temperatures. © 2023 Elsevier Ltd