Faculty Publications
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Item Development and characteristics of accumulative roll bonded Mg-Zn/Ce/Al hybrid composite(Elsevier Ltd, 2017) Anne, G.; Ramesh, M.R.; Shivananda Nayaka, H.; Arya, S.B.; Sahu, S.Accumulative roll bonding (ARB) process have been used develop Mg-2%Zn/Ce/Al hybrid composite and microstructure, mechanical and corrosion properties were investigated. The electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) revealed that the grains are significantly reduced and reaches up to 1 ?m in Mg-2%Zn layer and 1.8 ?m in Al layer having high angle misorientation of grain boundaries after subjected to 5-passes of the ARB process. The Al17Mg12, AlMg4Zn11 and Al11Ce3 intermetallic phases were observed through the XRD analysis. Mechanical properties of the hybrid composite improved with increase in the number of ARB passes which is attributed to work hardening, grain refinement and uniform distribution of Ce particles. Presence of Ce in the hybrid composite restricts the phenomenon of dynamic recrystallization and prevents the grain growth during ARB process. The corrosion rate of Mg-Zn/Ce/Al hybrid composite (0.72 mm/y) improved about 3.3 times as compared to that of Mg-2%Zn alloy (2.37 mm/y). © 2017 Elsevier B.V.Item Elevated temperature solid particle erosion behaviour of carbide reinforced CoCrAlY composite coatings(Institute of Physics Publishing helen.craven@iop.org, 2018) Nithin, H.S.; Desai, V.; Ramesh, M.R.CoCrAlY+WC-Co and CoCrAlY+Cr3C2-NiCr coatings are deposited on nickel based alloy using atmospheric plasma spray technique. Mechanical properties such as microhardness, adhesion strength and fracture toughness of coatings are evaluated. Elevated temperature solid particle erosion behaviour of these coatings are investigated at 600 °C using alumina erodent at 30 and 90° impact angle. Coatings are characterized utilizing Scanning electron microscope (SEM), x-ray diffraction (XRD) and Energy dispersive spectroscopy (EDS). CoCrAlY+WC-Co coating shows higher hardness, adhesion strength and fracture toughness than CoCrAlY+Cr3C2-NiCr coating. CoCrAlY+WC-Co coating exhibited approximately 3 times higher erosion resistance than CoCrAlY+Cr3C2-NiCr coating at 90° and 30° impact angles. SEM images of eroded surfaces of coatings reveals the combination of ductile and brittle fracture. CoCrAlY+Cr3C2-NiCr coating shows severe cracks, craters, carbide pull out and chipping than CoCrAlY+WC-Co coating. High temperature erosion is a combination of simultaneous building up of material by oxidation and removal of material by erosion process. Thus reforming the erosion process to oxidation modified erosion process. © 2018 IOP Publishing Ltd.Item Cyclic Oxidation and Hot Corrosion Behavior of Plasma-Sprayed CoCrAlY + WC-Co Coating on Turbine Alloys(Springer New York LLC barbara.b.bertram@gsk.com, 2018) Nithin, H.S.; Vijay, D.; Ramesh, M.R.Components in energy-producing systems suffer a variety of degradation processes such as oxidation and molten salt-induced corrosion as a consequence of complex multi-component gaseous environment. Coatings provide a composition that will grow the protective scale at high temperatures having long-term stability. Plasma spraying was used to deposit CoCrAlY + WC-Co composite coatings on turbine alloys of Hastelloy X and AISI 321. The thermocyclic oxidation behavior of coated alloys was investigated in static air and in molten salt (Na2SO4-60%V2O5) environment at 700 °C. The thermogravimetric technique was used to approximate the kinetics of oxidation in 50 cycles, each cycle consisting of heating and cooling. X-ray diffraction and SEM/EDAX techniques are used to characterize the oxide scale formed. Coated alloys showed a lower corrosion rate as compared to uncoated alloys. The coatings subjected to oxidation and hot corrosion showed slow scale growth kinetics. Preferential oxidation of Co, Cr, W and its spinel blocks the transport of oxygen and corrosive species into the coating by providing a barrier, thereby making the oxidation rate to reach steady state. As compared to the substrate alloys, coatings show better hot corrosion resistance. © 2018, ASM International.Item Characterisation and performance evaluation of TiSiN &tiAlSiN coatings by RF magnetron sputtering deposition during end milling of maraging steel(Institute of Physics Publishing helen.craven@iop.org, 2019) Varghese, V.; Ramesh, M.R.; Dupadu, D.; Shaik, H.Monolayer nanostructured thin films of TiSiN & TiAlSiN were deposited on WC-Co milling inserts using RF magnetron sputtering for metal cutting. The alloy targets of TiSi (80/20 at%) & TiAlSi (34/56/10 at%) were used for the deposition in an Ar + N atmosphere. The deposition time and parameters are optimized to develop a uniform and homogenous coating. The mechanical and metallurgical properties are characterized to analyze the wear resistance of the coating. The machinability studies on MDN 250 maraging steel is carried out using TiSiN and TiAlSiN coated WC-Co inserts under dry and wet environment. The machining responses such as surface roughness, cutting force, tool wear and tool life are analyzed by varying spindle speed. The results showed that TiAlSiN coating had a higher wear resistance and machining performance compared to the TiSiN coating owing to the high hardness and plasticity index of the coating. © 2020 IOP Publishing Ltd.Item Effect of Ball Milling on the Tensile Properties of Aluminum-Based Metal Matrix Nanocomposite Developed by Stir Casting Technique(SAE International, 2021) Ravikumar, K.S.; Ghanaraja, S.; Ramesh, M.R.Combining ball milling with stir casting in the synthesis of nanocomposites is found effective in increasing the strength and ductility of the nanocomposites. In the first step, the nanoparticles used as reinforcement are generated by milling a mixture of aluminum (Al) and manganese dioxide (MnO2) powders. A mixture of Al and MnO2 powders are mixed in the ratio of 1:2.4 by weight and milled at 300 rpm in a high-energy planetary ball mill for different durations of 120 min, 240 min, and 360 min to generate nano-sized alumina (Al2O3) particles. It is supposed that the powders have two different roles during milling, firstly, to generate nano-sized Al2O3 by oxidation at the high-energy impact points due to collision between Al and MnO2 particles, and secondly, to keep nano-sized Al2O3 particles physically separate by the presence of coarser particles. In the second step, 0.5 weight percent (wt%), 1 wt%, 1.5 wt%, and 2 wt% of the generated Al2O3 nanoparticles are reinforced in molten aluminum-magnesium (Al-Mg) alloy matrix via stir casting to synthesize nanocomposites. The effect of milling on the microstructure of the powder mixture before and after milling has been studied with the use of a scanning electron microscope (SEM) and X-ray diffraction analysis (XRD). The microstructure of the cast composites is examined under SEM, and the fractured surface of the tensile specimens is analyzed through SEM fractographs. Ball milling of reinforcement before adding to the melt brings considerable improvement in the integration and uniform dispersion of the milled particle in the Al-Mg alloy matrix melt, which leads to improvement in the strength and ductility of the cast nanocomposites. ©Item Elevated temperature erosion performance of plasma sprayed NiCrAlY/TiO2coating on MDN 420 steel substrate(Institute of Physics, 2022) Reddy G, M.S.; Prasad, C.D.; Patil, P.; Naresh, N.; Ramesh, M.R.The current study deals with the erosion behaviour of a plasma-sprayed 70% NiCrAlY + 30% TiO2 coating on MDN 420 steel substrate at extreme temperatures. The coating was characterized by using an optical microscope, Scanning Electron Microscopy and X-ray diffraction methods. The coating's porosity, microhardness, surface roughness, and adhesion strength were all examined. The solid particle erosion experiments were carried out at temperatures of 300 °C, 500 °C, and 700 °C, with impact angles of 30° and 90°. The tests were conducted by using the alumina as an erodent in the hot air jet erosion testing machine. The erosion volume loss of coated and uncoated samples was measured using an optical profilometer. It is observed that erosion resistance of the coating was found to be more when compared to the substrate for the different test temperatures chosen. As the temperature increases, the erosion resistance of the coating also found increased from 300 °C to 700 °C at both impact angles of 30° and 90°. The morphology of the eroded coating surface reveals that the generalized behaviour of the coating is ductile in nature. © 2022 IOP Publishing Ltd.Item High temperature erosion performance of NiCrAlY/Cr2O3/YSZ plasma spray coatings(Taylor and Francis Ltd., 2023) Reddy, G.M.S.; Prasad, C.D.; Patil, P.; Shetty, G.; Naresh, N.; Ramesh, M.R.The current investigation's objective was to assess the air jet erosion tester's ability to measure the erosive behaviour of plasma sprayed coatings on titanium-15 alloy. 65% NiCrAlY, 30% Cr2O3, and 5% YSZ make up the coating's chemical composition. A study of microstructure and phases was carried out. Microhardness and adhesive strength have both been measured in this work. With impact angles of 30° and 90° at 300°C, 500°C, and 700°C, Al2O3 erodent was utilised in a solid particle erosion test. An optical profilometer was used to calculate the erosion volume loss. The coating erosion resistance was found to be higher than the substrate sample for the test temperature that was employed, and this was more obvious at higher impact angles and higher temperatures The ductile character of the coating is seen in the contour of the deteriorated coating surface. © 2023 Institute of Materials Finishing Published by Taylor & Francis on behalf of the Institute.Item Characterization and Wear Behavior of NiCrMoSiC Microwave Cladding(Springer, 2024) Sharanabasava, H.; Prasad, C.D.; Ramesh, M.R.A microwave hybrid heating technique has been employed to develop NiCr-Mo-SiC composite cladding on titanium alloy (Grade-5/Ti-6Al-4 V/Titan-31). The developed claddings have been characterized for microstructural features, phase analysis, microhardness measurements, and 3D optical profile parameters by employing scanning electron microscopy, x-ray diffraction, Vickers microhardness tester, and 3D optical profilometer, respectively. Microwave clads have been subjected to linear reciprocator ball on plate wear test with static alumina indenter. Wear track parameters and friction coefficients have been studied. A dense microstructure with uniform distribution of hard phases and good metallurgical bonding with no visible pores and cracks has been obtained. Cladding exhibits nearly 2 times higher hardness than the base alloy. Coefficient of friction studies revealed that higher molybdenum content enhances internal lubricity. © 2023, ASM International.Item Cyclic Oxidation and Hot-Corrosion Behavior of HVOF-Sprayed NiCrAl Coating on Industrial Boiler Tube Steels(Springer, 2024) Ramesh, M.R.; Medabalimi, S.; Rupanagudi, R.S.; Prasad, C.D.; Sollapur, S.B.At high temperatures, coatings provide a protective scale development on surfaces to maintain long-term stability. In the current study, ASTM-SA210-Grade A1 (GrA1) and ASTM-SA213-T-11 (T11) boiler tube steels were coated with NiCrAl alloy with high-velocity oxy-fuel (HVOF) to prevent oxidation and hot corrosion. For hot corrosion and oxidation, 50 cycles at 900°C were taken into account. Additionally, tests of hot-corrosion behavior were conducted in an atmosphere containing molten salt (Na2SO4-60%V2O5), while tests of oxidation behavior were conducted in static air. The kinetics of oxidation were calculated using the thermogravimetric method. Using XRD, EPMA, and SEM/EDAX methods, the produced oxide scales were characterized. The oxidation rate of NiCrAl-coated steels was found to be lower than that of uncoated steels. The coated steels subjected to oxidation in air exhibit slow scale growth kinetics and oxides of α-Al2O3 and Cr2O3 on the outermost surface, while accelerated oxidation caused by the molten salt exhibits metastable Al2O3. Along the nickel-rich splat boundary, Cr and Al were formed a preferential oxidation, which prevents other oxygen from entering the coating via pores and voids, resulting in steady-state oxidation. © The Minerals, Metals & Materials Society 2024.Item Elevated temperature wear and friction performance of WC-CoCr/Mo and WC-Co/NiCr/Mo coated Ti-6Al-4V alloy(Elsevier Inc., 2024) Behera, N.; Ramesh, M.R.; Rahman, M.R.The effect of adding Mo to WC-based coatings on the microstructure and dry sliding wear performance at elevated temperatures is investigated. The WC-based coatings are deposited using a high-velocity oxy-fuel process on the titanium-31 substrate. The coating was characterized by microstructure, microhardness, porosity, surface roughness, density, and bond strength. The wear and friction behavior of coatings was evaluated using a ball-on disc tribometer at temperatures of 200, 400, 600, and 800 °C and loads of 20 and 30 N. SEM-EDS and an optical profilometer were utilized to evaluate the wear rate and mechanism. The microhardness and bond strength of WC-CoCr/10%Mo coating is more than that of WC-Co/20%NiCr/10%Mo coatings. The WC-CoCr, WC-CoCr/10%Mo, and WC-Co/20%NiCr/10%Mo coatings exhibited decreasing wear rates up to 600 °C, transitioning to an increase at 800 °C. The oxide phases of CoWO4 WO3 MoO3, CoMoO4, and NiMoO4, formed at 600 °C, aid in reducing the rate of wear and friction coefficient. However, the wear rate slightly increased at 800 °C due to vigorous oxidation and softness of coatings. The friction coefficient of WC-CoCr, WC-CoCr/10%Mo, and WC-Co/20%NiCr/10%Mo coating decreases with increasing temperatures due to the lubricating properties of oxide phases on the worn surface. The WC-CoCr/10%Mo coating demonstrates a lower friction and wear rate than the WC-CoCr and WC-Co/20%NiCr/10%Mo coating. At 200 °C, the predominant wear mechanisms were abrasive and fatigue wear, while at 800 °C, oxidative wear, abrasive wear, and adhesive wear were observed. © 2024