Faculty Publications

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    Characterisation of water base copper nanoquenchants by standard cooling curve analysis
    (2011) Ramesh, G.; Prabhu, K.N.
    Water base copper nanofluids having concentrations varying from 0?001 to 0?1 vol.-% were prepared and used as quench media for immersion quenching. Cooling curve analyses were carried out by using a standard ISO/DIS 9950 quench probe. An inverse heat conduction model is employed to estimate the metal/nanoquenchant interfacial heat flux transients from the measured temperature field and thermophysical properties of the quench probe material. The addition of copper nanoparticles had a significant effect on the occurrence of the vapour blanket stage and nucleate boiling stage. Furthermore, all six cooling curve parameters were found to be altered by adding nanoparticles to water. The contact angle of water decreased from 67 to 39° by adding 0?1 vol.-% of copper nanoparticles indicating the improved wettability of nanofluids. The heat flux curve shows a maximum initially then drops rapidly during quenching. The peak cooling rate and heat flux of water increased by adding copper nanoparticles up to 0?01 vol.-%. Both parameters decreased with further increase in concentration of nanoparticles. The results suggest that the quench severity of water could be altered by adding copper nanoparticles. © 2011 IHTSE Partnership.
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    Effect of boundary heat transfer coefficient and probe section size on cooling curves during quenching
    (ASTM International, 2012) Ramesh, G.; Prabhu, K.N.
    In the present work the effect of boundary heat transfer coefficient and section size of quench probe material on cooling curves was investigated by using finite difference heat transfer based SolidCast software. Simulations were carried out at different combinations of heat transfer coefficient and quench probe diameter and thermal history at the geometric center of the probe was estimated to generate cooling curves. Simulation results show that both boundary heat transfer coefficient and quench probe diameter had a significant effect on the average cooling rate. A relationship between Grossmann quench severity (H), thermal conductivity of material, size of the probe, and average cooling rate was established. By using this model, for a known quench medium, probe size, and material it is possible to predict the average cooling rate of the probe. On the other-hand, for a given material and required cooling rate, cooling severity required from the quench media could be predicted and accordingly an appropriate quench medium can be selected. © 2012 by ASTM International.
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    Wetting kinematics and spreading behaviour of water based aluminium nanofluids during immersion quenching
    (2013) Ramesh, G.; Prabhu, K.
    In the present work, wetting kinematics of water based aluminium nanofluids having nanoparticle concentrations varying from 0.001 to 0.5 vol.-% during immersion quenching of Inconel 600 probe was investigated by measuring the contact resistance. The contact resistance between the quench probe and counter electrode during quenching indicated that the duration of the film of water vapour decreased with increasing nanoparticle concentration as well as absence of stable vapour film formation with 0.05, 0.1 and 0.5 vol.-% of nanoparticles. The phenomenon of a repeated wetting process was observed during quenching in nanofluids. Further, quenching in 0.1 and 0.5 vol.-% nanofluids indicated the formation of a nanoparticle porous layer and its deposition on the quench probe. The spreading behaviour was studied by measuring the dynamic contact angle of nanofluids droplets on Inconel 600 substrate. Contact angle measurement showed that the addition of aluminium nanoparticles did not have a significant effect on the relaxation of contact angle of water droplet. However, lower static contact angles were obtained for nanofluids indicating improved wetting. © 2013 IHTSE Partnership.
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    Dimensionless cooling performance parameter for characterization of quench media
    (2013) Ramesh, G.; Prabhu, K.
    The effect of varying thermal properties and boundary heat transfer coefficients on temperature profiles inside cylindrical quench probes was simulated during immersion cooling. The results of simulation indicated that, for assessment of the cooling performance of the quench media, the ratio of the quench probe diameter to its thermal conductivity should be less than 0.0005 m2K/W. A simple dimensionless cooling parameter (D 2CR/??T) was proposed to assess the cooling performance of quench media. © 2013 The Minerals, Metals & Materials Society and ASM International.
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    Effect of thermal conductivity and viscosity on cooling performance of liquid quench media
    (Maney Publishing Suite 1C, Joseph's Well, Hanover Walk Leeds LS3 1AB, 2014) Ramesh, G.; Prabhu, K.
    In this present work, the effect of the thermophysical properties of quenchants on its cooling performance was investigated. Water, brine solutions, polymer solutions and mineral oils were chosen to have quench media with varying thermophysical properties. Cooling curve analyses were carried out by using standard ISO/DIS 9950 quench probe. Grossmann H quench severity of the quench media was determined from the relation of H and cooling rate. Cooling curve analysis results showed that the change in thermophysical properties of the quench media had significant effect on the cooling history of the quench probe. The viscosity of the quenchant used for immersion quenching is the most important factor that controls the cooling performance of the quenchant compared to thermal conductivity of the quench medium. © 2014 IHTSE Partnership.
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    Wetting kinetics, kinematics and heat transfer characteristics of pongamia pinnata vegetable oil for industrial heat treatment
    (Elsevier Ltd, 2014) Ramesh, G.; Prabhu, K.
    The suitability of pongamia pinnata vegetable oil as cooling medium for quench heat treatment was investigated. Wetting kinetics, kinematics and heat transfer characteristics of pongamia oil during immersion quenching of hot Inconel probe were determined and compared with palm and mineral oils. A comparison of the relaxation of contact angle indicated early attainment of equilibrium contact angle for pongamia oil droplet on Inconel substrate. The equilibrium contact angle value of pongamia oil was in between mineral and palm oils. However, the spreading kinetics was faster with pongamia oil. Pongamia oil showed the formation of a stable vapour film on the probe surface during quenching. This phenomenon was not observed in palm oil and other vegetable oils reported in literature. Pongamia pinnata oil exhibits uniform nature of wetting front, intermediate rewetting temperature and less variations in rewetting temperatures during quenching. The hardening power of pongamia oil was higher than palm and mineral oils and the cooling of the probe was more uniform during quenching in pongamia oil. The heat transfer characteristics of pongamia oil were found to be superior to palm and mineral oils after film/transition boiling. Pongamia oil showed lower heat transfer but more uniform cooling during film boiling. © 2014 Elsevier B.V.
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    Spatial dependence of heat flux transients and wetting behavior during immersion quenching of inconel 600 probe in brine and polymer media
    (Springer Boston, 2014) Ramesh, G.; Prabhu, K.
    Cooling curve analysis of Inconel 600 probe during immersion quenching in brine and polymer quench media was carried out. Thermal histories at various axial and radial locations were recorded using a high-speed data acquisition system and were input to an inverse heat-conduction model for estimating the metal/quenchant heat flux transients. A high performance smart camera was used for online video imaging of the immersion quenching process. Solution to two-dimensional inverse heat-conduction problem clearly brings out the spatial dependence of boundary heat flux transients for a Inconel 600 probe with a simple cylindrical geometry. The estimated heat flux transients show large variation on axial as well as radial directions of quench probe surface for brine quenching. Polymer quenching showed less variation in metal/quenchant heat flux transients. Shorter durations of vapor film, higher rewetting temperatures, and faster movement of wetting front on quench probe surface were observed with brine quenching. Measurement of dynamic contact angle showed better spreading and good wettability for polymer medium as compared to brine quenchant. The solid-liquid interfacial tension between polymer medium and Inconel substrate was lower compared with that of solution. Rewetting and boiling processes were nonuniform and faster on quench probe surface during immersion quenching in brine solution. For the polymer quench medium, slow rewetting, uniform boiling and repeated wetting were observed. © 2014 The Minerals, Metals & Materials Society and ASM International.
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    A dimensional parameter for prediction of cooling performance of quenchants
    (ASTM International, 2014) Prabhu, K.; Ramesh, G.
    Computer aided cooling curve analysis was carried out during immersion quenching of ISO/DIS 9950 quench probe. Water, brine solutions, polymer solutions, mineral oils, and vegetable oils were used as quench media. The results showed that the quench medium used had a significant effect on the quench probe cooling curve parameters. An empirical correlation was proposed to predict the average cooling rate from surface tension, wetting angle, thermal conductivity, and kinematic viscosity of the quench medium. © 2014 by ASTM International.
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    Experimental and numerical heat transfer studies on quenching of Inconel 600 probe
    (Springer Verlag, 2015) Ramesh, G.; Prabhu, K.
    The effect of heat transfer coefficient and quench start temperature on cooling behaviour of Inconel 600 quench probe was assessed by numerical experiments. A quantitative model that relates the mean cooling rate and quench start temperature of the probe with the boundary heat transfer coefficient was proposed. Computed aided cooling curve analysis was carried out by heating Inconel 600 probe to temperatures varying from 100 to 850 °C followed by quenching in water. The results of quenching experiments and the data available in the literature were used to validate the proposed model. A good agreement between the measured and estimated value was observed. The results showed that the film and transition boiling of cooling stages were significantly influenced by quench start temperature of the material while nucleate boiling and convective cooling stages were strongly dependent on the boundary heat transfer coefficient. © 2014, Springer-Verlag Berlin Heidelberg.
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    Effect of Polymer Concentration on Wetting and Cooling Performance During Immersion Quenching
    (Springer Boston, 2016) Ramesh, G.; Prabhu, K.N.
    The effect of varying concentrations (0 to 100 vol pct) of glycol polymer solution on wetting kinetics, kinematics, and cooling performance during immersion quenching was studied by using goniometry, online video imaging, and cooling curve analysis techniques. An increase in concentration of the polymer solution resulted in improved wettability and accelerated spreading kinetics of the quench medium. The quench medium showed medium-fast-nonuniform, fast-uniform, slow-uniform, explosive/rapid, repeated, and slow-nonuniform rewetting phenomena depending on the concentration of the polymer solution. The collapse of the vapor film was by an instantaneous rupture process in the quench medium containing more water and by nucleation of bubbles caused by the selective rupture process in the quench medium enriched with polymer. The quench medium consisting of an equal amount of water and polymer showed an explosive collapse of the vapor film on the quench probe surface. The nature of the wetting front was uniform with polymer quench media except at 100 vol pct concentration of polymer quenchant. There was enhancement in the cooling performance of the quench medium, which was enhanced for a lower volume concentration of the polymer solution. However, an increase in the concentration of the polymer resulted in a decreased cooling performance. The cooling of the probe was more uniform with polymer quenchants (5 to 25 vol pct), which exhibited fast and uniform rewetting. Polymer quenchants (75 to 100 vol pct) that exhibited repeated and slow-nonuniform rewetting showed large variation in heat transfer over the quench probe surface. © 2015, The Minerals, Metals & Materials Society and ASM International.