Faculty Publications

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    Development of clay based nanofluids for quenching
    (2012) Ramesh, G.; Prabhu, K.N.
    In the present work the effect of addition of nanoclay particles having concentrations of 0.001, 0.01 and 0.1 vol% on cooling performance of water during immersion quenching was investigated. Cooling curve analyses were carried out by using standard ISO/DIS 9950 quench probe. Wetting behavior of nanoquenchant was studied using dynamic contact angle analyzer. The spreading behavior of droplets of quench media on INCONEL 600 substrate indicates improved wetting behavior of nanofluids. The peak cooling rate and cooling rate at 700°C for water decreased by addition of nanoparticles. Further, quenching in nanofluid shows longer vapour blanket stage as compared to water. The estimated flux transients and Grossmann H factor clearly show that decreased cooling performance of water by addition of nanoparticles. Copyright © 2012 ASM International® All rights reserved.
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    Heat flux transients and casting surface macro-profile during downward solidification of Al-12% Si alloy against chills
    (American Foundry Society, 2011) Prabhu, K.N.; Sharath, K.; Ramesh, G.
    Heat flux transients were estimated during downward solidificationofAl- 12%Sialloy(A413)againstaluminumand graphite chills. The thermal plot of graphite chill indicated one-dimensional heat flow in the initial stages which then changes to two-dimensional heat transfer. The heat transfer becomes one-dimensional again during the final stages of solidification. In aluminum chill, heat flow was nearly one- dimensional. Experiments were designed to verify whether the peak heat flux is an artifact of the experiment. The results clearly showed that the occurrence of the peak in the heat flux transients is not an artifact of the inverse model or the experimental technique. The macro-profile of the casting surface in contact with the chill revealed the occurrence of crests and troughs. A mechanism based on the convection within the liquid metal below the solid shell was proposed to account for the formation of wavy casting surface. Copyright © 2011 American Foundry Society.
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    Wetting kinetics, kinematics and heat transfer characteristics of pongamia pinnata vegetable oil for industrial heat treatment
    (Elsevier Ltd, 2014) Ramesh, G.; Prabhu, K.
    The suitability of pongamia pinnata vegetable oil as cooling medium for quench heat treatment was investigated. Wetting kinetics, kinematics and heat transfer characteristics of pongamia oil during immersion quenching of hot Inconel probe were determined and compared with palm and mineral oils. A comparison of the relaxation of contact angle indicated early attainment of equilibrium contact angle for pongamia oil droplet on Inconel substrate. The equilibrium contact angle value of pongamia oil was in between mineral and palm oils. However, the spreading kinetics was faster with pongamia oil. Pongamia oil showed the formation of a stable vapour film on the probe surface during quenching. This phenomenon was not observed in palm oil and other vegetable oils reported in literature. Pongamia pinnata oil exhibits uniform nature of wetting front, intermediate rewetting temperature and less variations in rewetting temperatures during quenching. The hardening power of pongamia oil was higher than palm and mineral oils and the cooling of the probe was more uniform during quenching in pongamia oil. The heat transfer characteristics of pongamia oil were found to be superior to palm and mineral oils after film/transition boiling. Pongamia oil showed lower heat transfer but more uniform cooling during film boiling. © 2014 Elsevier B.V.
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    Wetting and cooling performance of mineral oils for quench heat treatment of steels
    (Iron and Steel Institute of Japan, 2014) Ramesh, G.; Prabhu, K.
    In the present work, wetting kinetics, kinematics and heat transfer characteristics of mineral oils having varying thermo-physical properties sourced from different suppliers were investigated using contact angle, online video imaging and cooling curve analysis techniques. The relaxation behavior of mineral oils of low viscosity and surface tension on Inconel substrate indicated improved wettability and fast spreading kinetics while mineral oils of high viscosity and surface tension showed reduced wettability and slower spreading kinetics. Further, the spreading behavior of mineral oils of lower viscosity and density showed the absence of viscous regime. During rewetting, formation of double wetting fronts and more uniform nature of wetting front were observed with mineral oils of high viscosity and flash point whereas no additional wetting front was observed for mineral oils of low viscosity and flash point. Among the convectional/fast/hot mineral oils, higher wetting front velocity and cooling rate were obtained for low viscosity mineral oil. The heat extracting capability of high viscosity mineral oils was higher during vapour and nucleate boiling and lower during liquid cooling stage. Further, highly viscous mineral oils showed uniform heat transfer compared to mineral oils having low viscosity. © 2014 ISIJ.
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    Spatial dependence of heat flux transients and wetting behavior during immersion quenching of inconel 600 probe in brine and polymer media
    (Springer Boston, 2014) Ramesh, G.; Prabhu, K.
    Cooling curve analysis of Inconel 600 probe during immersion quenching in brine and polymer quench media was carried out. Thermal histories at various axial and radial locations were recorded using a high-speed data acquisition system and were input to an inverse heat-conduction model for estimating the metal/quenchant heat flux transients. A high performance smart camera was used for online video imaging of the immersion quenching process. Solution to two-dimensional inverse heat-conduction problem clearly brings out the spatial dependence of boundary heat flux transients for a Inconel 600 probe with a simple cylindrical geometry. The estimated heat flux transients show large variation on axial as well as radial directions of quench probe surface for brine quenching. Polymer quenching showed less variation in metal/quenchant heat flux transients. Shorter durations of vapor film, higher rewetting temperatures, and faster movement of wetting front on quench probe surface were observed with brine quenching. Measurement of dynamic contact angle showed better spreading and good wettability for polymer medium as compared to brine quenchant. The solid-liquid interfacial tension between polymer medium and Inconel substrate was lower compared with that of solution. Rewetting and boiling processes were nonuniform and faster on quench probe surface during immersion quenching in brine solution. For the polymer quench medium, slow rewetting, uniform boiling and repeated wetting were observed. © 2014 The Minerals, Metals & Materials Society and ASM International.
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    Comparative study of wetting and cooling performance of polymer-salt hybrid quench medium with conventional quench media
    (Taylor and Francis Ltd., 2015) Ramesh, G.; Prabhu, K.
    Wetting kinetics, kinematics, and cooling performance of a polymer-salt hybrid quenchant were investigated. The rewetting phenomenon for brine, water, polymer, and polymer-salt hybrid solutions was characterized as rapid uniform, fast non-uniform, slow uniform, and fast uniform processes, respectively. A dimensionless rewetting time was proposed to assess the nature of the wetting front. The hybrid quenchant showed higher heat transfer during vapor and transition boiling and lower heat transfer during nucleate boiling and convective cooling. The presence of salt in the hybrid solution resulted in early destabilization of the vapor film and an increase in wetting front velocity and rewetting temperature. The polymer constituent delayed the rewetting phenomenon. © 2015 Taylor & Francis Group, LLC.
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    Wetting and Cooling Performance of Vegetable Oils during Quench Hardening
    (John Wiley and Sons Inc. P.O.Box 18667 Newark NJ 07191-8667, 2016) Ramesh, G.; Prabhu, K.N.
    Wetting kinetics, kinematics, and cooling performance of vegetable oils (sunflower, gingelly, palm, and coconut oils) during quenching of Inconel 600 probe were studied using goniometry, online video imaging, and cooling curve analysis. The results were compared with a conventional mineral oil quench medium. Improved wettability was obtained for vegetable oils with lower viscosity. Cooling curve analyses showed three stages of cooling for both mineral and vegetable oils. Video imaging of the quenching process and differential scanning calorimetry analysis confirmed that the first stage of cooling was caused by the formation of vapor film in mineral oil and due to the occurrence of a heated liquid layer around the quench probe surface in vegetable oils. Vegetable oils showed continuous boiling phenomenon during the convective cooling stage of quenching. The cooling performance of vegetable oils was found to depend on the concentration of mono-unsaturated fatty acid. The heat extracting capability of vegetable oils with lower mono-unsaturated fatty acid oils was found to be higher. However, no correlation was observed between fatty acid composition and uniformity of heat transfer. When compared to mineral oil quenching, vegetable oil quenching produced faster wetting kinematics and better cooling performance. © 2016 Wiley Periodicals, Inc.
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    Assessment of spatiotemporal heat flux during quenching in TiO2 and AlN nanofluids
    (ASTM International, 2017) Nayak, U.V.; Ramesh, G.; Prabhu, K.N.
    In the present work, spatiotemporal heat flux transients were estimated during quenching of an Inconel 600 alloy probe in water-based titanium dioxide (TiO2) and aluminum nitride (AlN) nanofluids that have nanoparticle concentrations varying from 0.001 to 0.5 vol. %. The results showed reduced peak heat flux and a longer vapor phase stage during quenching with nanofluids compared to quenching with water. The peak heat flux for quenching in nanofluids was lowered with increase in the nanoparticle concentration. Quenching with TiO2 nanofluids resulted in slower heat extraction compared to quenching in AlN nanofluids at higher concentrations. Quenching with nanofluids resulted in a more uniform quench compared to quenching with water because of the reduction in the rewetting period. © © 2017 by ASTM International.