Faculty Publications

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    Development of clay based nanofluids for quenching
    (2012) Ramesh, G.; Prabhu, K.N.
    In the present work the effect of addition of nanoclay particles having concentrations of 0.001, 0.01 and 0.1 vol% on cooling performance of water during immersion quenching was investigated. Cooling curve analyses were carried out by using standard ISO/DIS 9950 quench probe. Wetting behavior of nanoquenchant was studied using dynamic contact angle analyzer. The spreading behavior of droplets of quench media on INCONEL 600 substrate indicates improved wetting behavior of nanofluids. The peak cooling rate and cooling rate at 700°C for water decreased by addition of nanoparticles. Further, quenching in nanofluid shows longer vapour blanket stage as compared to water. The estimated flux transients and Grossmann H factor clearly show that decreased cooling performance of water by addition of nanoparticles. Copyright © 2012 ASM International® All rights reserved.
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    Characterisation of water base copper nanoquenchants by standard cooling curve analysis
    (2011) Ramesh, G.; Prabhu, K.N.
    Water base copper nanofluids having concentrations varying from 0?001 to 0?1 vol.-% were prepared and used as quench media for immersion quenching. Cooling curve analyses were carried out by using a standard ISO/DIS 9950 quench probe. An inverse heat conduction model is employed to estimate the metal/nanoquenchant interfacial heat flux transients from the measured temperature field and thermophysical properties of the quench probe material. The addition of copper nanoparticles had a significant effect on the occurrence of the vapour blanket stage and nucleate boiling stage. Furthermore, all six cooling curve parameters were found to be altered by adding nanoparticles to water. The contact angle of water decreased from 67 to 39° by adding 0?1 vol.-% of copper nanoparticles indicating the improved wettability of nanofluids. The heat flux curve shows a maximum initially then drops rapidly during quenching. The peak cooling rate and heat flux of water increased by adding copper nanoparticles up to 0?01 vol.-%. Both parameters decreased with further increase in concentration of nanoparticles. The results suggest that the quench severity of water could be altered by adding copper nanoparticles. © 2011 IHTSE Partnership.
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    Effect of addition of aluminum nanoparticles on cooling performance and quench severity of water during immersion quenching
    (ASTM International, 2012) Ramesh, G.; Prabhu, K.N.
    In the present work, the effect of the addition of aluminum nanoparticles in concentrations varying from 0.001 to 0.5 vol. % on the cooling performance and quench severity of water during immersion quenching is investigated. The results of cooling curve analyses show that an increase in nanoparticle concentration increased the cooling rates at critical temperatures up to 0.05 vol. % and decreased them thereafter. The transition from the vapor blanket stage to the nucleate boiling stage was also altered by quenching in nanofluids. A finite difference heat transfer program was employed to generate cooling curves at different values of heat transfer coefficient from thermo-physical properties of the quench probe material. A Grossmann H quench severity versus cooling rate curve was established, and from this curve, the H factors of prepared nanofluids were estimated. An increase in nanoparticle concentration up to 0.05 vol. % resulted in an increase of the H value of water from 63 m -1 to 93 m-1, and any further increase in the concentration of nanoparticles resulted in a decrease in H. The results suggest both the enhancement and the deterioration of the cooling performance of water by the addition of aluminum nanoparticles. Copyright © 2012 by ASTM International.
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    Effect of addition of aluminum nanoparticles on cooling performance and quench severity of water during immersion quenching
    (2012) Ramesh, G.; Prabhu, K.N.
    In the present work, the effect of the addition of aluminum nanoparticles in concentrations varying from 0.001 to 0.5 vol. % on the cooling performance and quench severity of water during immersion quenching is investigated. The results of cooling curve analyses show that an increase in nanoparticle concentration increased the cooling rates at critical temperatures up to 0.05 vol. % and decreased them thereafter. The transition from the vapor blanket stage to the nucleate boiling stage was also altered by quenching in nanofluids. A finite difference heat transfer program was employed to generate cooling curves at different values of heat transfer coefficient from thermo-physical properties of the quench probe material. A Grossmann H quench severity versus cooling rate curve was established, and from this curve, the H factors of prepared nanofluids were estimated. An increase in nanoparticle concentration up to 0.05 vol. %resulted in an increase of the H value of water from 63 m 1 to 93 m 1, and any further increase in the concentration of nanoparticles resulted in a decrease in H. The results suggest both the enhancement and the deterioration of the cooling performance of water by the addition of aluminum nanoparticles. Copyright © 2012 by ASTM International.
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    Effect of thermal conductivity and viscosity on cooling performance of liquid quench media
    (Maney Publishing Suite 1C, Joseph's Well, Hanover Walk Leeds LS3 1AB, 2014) Ramesh, G.; Prabhu, K.
    In this present work, the effect of the thermophysical properties of quenchants on its cooling performance was investigated. Water, brine solutions, polymer solutions and mineral oils were chosen to have quench media with varying thermophysical properties. Cooling curve analyses were carried out by using standard ISO/DIS 9950 quench probe. Grossmann H quench severity of the quench media was determined from the relation of H and cooling rate. Cooling curve analysis results showed that the change in thermophysical properties of the quench media had significant effect on the cooling history of the quench probe. The viscosity of the quenchant used for immersion quenching is the most important factor that controls the cooling performance of the quenchant compared to thermal conductivity of the quench medium. © 2014 IHTSE Partnership.
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    Wetting kinetics, kinematics and heat transfer characteristics of pongamia pinnata vegetable oil for industrial heat treatment
    (Elsevier Ltd, 2014) Ramesh, G.; Prabhu, K.
    The suitability of pongamia pinnata vegetable oil as cooling medium for quench heat treatment was investigated. Wetting kinetics, kinematics and heat transfer characteristics of pongamia oil during immersion quenching of hot Inconel probe were determined and compared with palm and mineral oils. A comparison of the relaxation of contact angle indicated early attainment of equilibrium contact angle for pongamia oil droplet on Inconel substrate. The equilibrium contact angle value of pongamia oil was in between mineral and palm oils. However, the spreading kinetics was faster with pongamia oil. Pongamia oil showed the formation of a stable vapour film on the probe surface during quenching. This phenomenon was not observed in palm oil and other vegetable oils reported in literature. Pongamia pinnata oil exhibits uniform nature of wetting front, intermediate rewetting temperature and less variations in rewetting temperatures during quenching. The hardening power of pongamia oil was higher than palm and mineral oils and the cooling of the probe was more uniform during quenching in pongamia oil. The heat transfer characteristics of pongamia oil were found to be superior to palm and mineral oils after film/transition boiling. Pongamia oil showed lower heat transfer but more uniform cooling during film boiling. © 2014 Elsevier B.V.
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    Wetting and cooling performance of mineral oils for quench heat treatment of steels
    (Iron and Steel Institute of Japan, 2014) Ramesh, G.; Prabhu, K.
    In the present work, wetting kinetics, kinematics and heat transfer characteristics of mineral oils having varying thermo-physical properties sourced from different suppliers were investigated using contact angle, online video imaging and cooling curve analysis techniques. The relaxation behavior of mineral oils of low viscosity and surface tension on Inconel substrate indicated improved wettability and fast spreading kinetics while mineral oils of high viscosity and surface tension showed reduced wettability and slower spreading kinetics. Further, the spreading behavior of mineral oils of lower viscosity and density showed the absence of viscous regime. During rewetting, formation of double wetting fronts and more uniform nature of wetting front were observed with mineral oils of high viscosity and flash point whereas no additional wetting front was observed for mineral oils of low viscosity and flash point. Among the convectional/fast/hot mineral oils, higher wetting front velocity and cooling rate were obtained for low viscosity mineral oil. The heat extracting capability of high viscosity mineral oils was higher during vapour and nucleate boiling and lower during liquid cooling stage. Further, highly viscous mineral oils showed uniform heat transfer compared to mineral oils having low viscosity. © 2014 ISIJ.
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    Spatial dependence of heat flux transients and wetting behavior during immersion quenching of inconel 600 probe in brine and polymer media
    (Springer Boston, 2014) Ramesh, G.; Prabhu, K.
    Cooling curve analysis of Inconel 600 probe during immersion quenching in brine and polymer quench media was carried out. Thermal histories at various axial and radial locations were recorded using a high-speed data acquisition system and were input to an inverse heat-conduction model for estimating the metal/quenchant heat flux transients. A high performance smart camera was used for online video imaging of the immersion quenching process. Solution to two-dimensional inverse heat-conduction problem clearly brings out the spatial dependence of boundary heat flux transients for a Inconel 600 probe with a simple cylindrical geometry. The estimated heat flux transients show large variation on axial as well as radial directions of quench probe surface for brine quenching. Polymer quenching showed less variation in metal/quenchant heat flux transients. Shorter durations of vapor film, higher rewetting temperatures, and faster movement of wetting front on quench probe surface were observed with brine quenching. Measurement of dynamic contact angle showed better spreading and good wettability for polymer medium as compared to brine quenchant. The solid-liquid interfacial tension between polymer medium and Inconel substrate was lower compared with that of solution. Rewetting and boiling processes were nonuniform and faster on quench probe surface during immersion quenching in brine solution. For the polymer quench medium, slow rewetting, uniform boiling and repeated wetting were observed. © 2014 The Minerals, Metals & Materials Society and ASM International.
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    Assessment of axial and radial heat transfer during immersion quenching of Inconel 600 probe
    (2014) Ramesh, G.; Prabhu, K.
    The time-temperature data at axial and radial locations were measured during immersion quenching of Inconel 600 probe in a mineral oil quench medium. The cooling of probe was not uniform during quenching. The variation of cooling rate along the axial direction was found to be higher than around the radial location. Inverse heat conduction problem (IHCP) was solved for estimating heat flux transients from the temperature data and thermo-physical properties of the Inconel probe. Single and multiple unknown heat fluxes were assigned on the metal/quenchant boundary. The error between the estimated and measured temperatures reduced significantly with increase in number of unknown surface heat flux components. The peak heat flux was about 50% lower for assignment of single unknown heat flux compared to multiple unknown heat fluxes at the metal/quenchant boundary. A plot of isotherms indicated gradual and uniform cooling of the quench probe when single heat flux boundary was used. With increase in the number of heat flux components, non-uniform and large temperature variations in the quench probe were observed. The present work outlines the importance of estimation of spatially dependent boundary heat flux transients during quench heat treatment. © 2014 Elsevier Inc.
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    Experimental and numerical heat transfer studies on quenching of Inconel 600 probe
    (Springer Verlag, 2015) Ramesh, G.; Prabhu, K.
    The effect of heat transfer coefficient and quench start temperature on cooling behaviour of Inconel 600 quench probe was assessed by numerical experiments. A quantitative model that relates the mean cooling rate and quench start temperature of the probe with the boundary heat transfer coefficient was proposed. Computed aided cooling curve analysis was carried out by heating Inconel 600 probe to temperatures varying from 100 to 850 °C followed by quenching in water. The results of quenching experiments and the data available in the literature were used to validate the proposed model. A good agreement between the measured and estimated value was observed. The results showed that the film and transition boiling of cooling stages were significantly influenced by quench start temperature of the material while nucleate boiling and convective cooling stages were strongly dependent on the boundary heat transfer coefficient. © 2014, Springer-Verlag Berlin Heidelberg.