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    Microstructural characterization and mechanical properties of cast Al-15Zn-2Mg alloy subjected to severe plastic deformation
    (Elsevier Ltd, 2018) Manjunath, G.K.; Udaya Bhat, K.; Preetham Kumar, G.V.
    In the present work, Al-15Zn-2Mg alloy was processed by ECAP technique for grain refinement. The ECAP processing was conducted at 150 °C. Microstructural characterization was carried out in OM, SEM, TEM and XRD. To evaluate the mechanical properties, hardness measurement and tensile tests were conducted at room temperature. Microstructural characterization showed that, ECAP processing leads to decrease in the grain size of the alloy. Also, small amount of dislocations were also observed in the ECAP processed material. After ECAP processing, precipitates nucleation in the material was identified in the XRD analysis. The strength and the hardness values were increased after ECAP processing. After ECAP processing, microhardness of the material is increased from 173 Hv to 252 Hv and the UTS of the material is increased from 166 MPa to 362 MPa. After tensile testing, fracture surface of the cast material showed dendritic structure and the fracture surface of the ECAP processed material showed dimples. © 2018 Elsevier Ltd. All rights reserved.
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    Effect of equal channel angular pressing on the microstructure and mechanical properties of Al-10Zn-2Mg alloy
    (American Institute of Physics Inc. subs@aip.org, 2018) Manjunath, G.K.; Preetham Kumar, G.V.; Bhat, K.U.
    The current investigation is focused on evaluating the mechanical properties and the microstructure of cast Al-10Zn-2Mg alloy processed through equal channel angular pressing (ECAP). The ECAP processing was attempted at minimum possible processing temperature. Microstructural characterization was carried out in optical microscopy, scanning electron microscopy, transmission electron microscopy and X-ray diffraction analysis. Hardness measurement and tensile tests were employed to estimate the mechanical properties. Experimental results showed that, ECAP processing leads to noticeable grain refinement in the alloy. Reasonable amount of dislocations were observed in the ECAP processed material. After ECAP processing, precipitates nucleation in the material was detected in the XRD analysis. ECAP leads to considerable enhancement in the mechanical properties of the material. After ECAP processing, microhardness of the material is increased from 144 Hv to 216 Hv. Also, after ECAP processing the UTS of the material is increased from 140 MPa to 302 MPa. The increase in the mechanical properties of the alloy after ECAP processing is due to the dislocation strengthening and grain refinement strengthening. Finally, fracture surface morphology of the tensile test samples also studied. © 2018 Author(s).
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    Severe plastic deformation of Al-15Zn-2Mg alloy: Effect on wear properties
    (Trans Tech Publications Ltd ttp@transtec.ch, 2019) Manjunath, G.K.; Bhat, K.U.; Preetham Kumar, G.V.
    In the present work, Al-Zn-Mg alloy having highest zinc content was deformed by one of the severe plastic deformation (SPD) technique, equal channel angular pressing (ECAP) and effect of ECAP on the microstructure evolution and the wear properties were studied. ECAP was performed in a split die and the channels of the die are intersecting at an angle of 120°. ECAP was attempted at least possible temperature and the alloy was successfully ECAPed at 423 K. Below this temperature samples were failed in the first pass itself. After ECAP, significant drop in the grain size was reported. Also, ECAP leads to significant raise in the microhardness of the alloy. Predominantly, after ECAP, upsurge in the wear resistance of the alloy was noticed. To figure out the response of ECAP on the wear properties of the alloy; worn surfaces of the wear test samples were analyzed in SEM. © 2019 Trans Tech Publications Ltd, Switzerland.
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    Influence of Multi-directional Room-Temperature Forging Process on Microstructure and Mechanical Behaviour of Eutectic Al-12Si Alloy
    (Springer, 2022) Kumara, B.; Preetham Kumar, G.V.
    In the present work, the influence of multi-directional forging on the microstructure and mechanical behaviour of eutectic Al-12Si alloy at ambient temperature has been examined. The sample for multi-directional forging was prepared by melting and pouring the commercially available LM-6 aluminum alloy ingot into a casting die. Prior to the forging process, the samples were solutionized for 3 h at 525 °C and then cooled in water. Light optical microscopy and scanning electron microscopy were used to examine the microstructure of materials. Microstructural observations have shown that effectively broken coarse needle-shaped plates like silicon particles with an average size of 11.7 µm in length of as-cast samples into fine particles with an average size of 2.8 µm in length after three cycles of forging (9 passes) and are evenly distributed in the α-Al phase. After three cycles, the tensile strength of the as-cast sample is enhanced from 192 to 382 MPa, and its hardness is enhanced from 66.6 to 100.2 Hv, respectively. X-ray diffraction analysis of Al-12Si alloys revealed the existence of α-Al and eutectic silicon (Si) phases. The peak broadening is also noted in X-ray diffraction pattern of three cycles, samples with cumulative strains of 2.43, which confirms the reduction in silicon particle size and grain size. Facets and tearing ridges are observed on the tensile fracture surface of forged samples. The improvement in the mechanical properties of forged samples can be attributed to the evenly distributed silicon particles and the work hardening of the aluminum phase. © 2022, ASM International.
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    Microstructure Evolution in Cast Al-Zn-Mg Alloys Processed by Equal Channel Angular Pressing
    (Springer New York LLC barbara.b.bertram@gsk.com, 2018) Manjunath, G.K.; Udaya Bhat, K.; Preetham Kumar, G.V.
    In the present work, microstructure development and enhancement in the microhardness of Al-Zn-Mg alloys (with 5, 10, and 15% zinc) during equal channel angular pressing (ECAP) were investigated. Dendritic morphology was observed in the cast condition of all three alloys, and precipitates were situated along the inter-dendritic regions. After homogenization, precipitates in the inter-dendritic regions were uniformly distributed in the aluminum matrix and grain boundaries were developed. After 4 passes in route BC, large reduction in the grain size was observed. X-ray diffractometry showed that MgZn2 precipitate was developed in the ECAP-processed samples. Increase in the intensity of MgZn2 peaks was observed when the quantity of zinc is increased in the material. Also, changes in the intensity of XRD peaks were observed in ECAP-processed samples due to shear deformation. After ECAP, substantial increase in the microhardness was perceived. After four passes, microhardness increased to 109, 67, and 58% from the initial condition in A1, A2, and A3 alloys, respectively. Also, improvement in the microhardness was also observed when the quantity of zinc is increased in the material. © 2017, Springer Science+Business Media, LLC, part of Springer Nature and ASM International.
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    Investigation on Microstructure and Mechanical Properties of Solution Heat-Treated and Multi Directional Forging-Processed LM-25 Aluminium Alloy
    (Springer, 2020) Kumara, B.; Preetham Kumar, G.V.
    The experimental study of hypoeutectic Al-7.3Si alloy on microstructure and mechanical properties processed by MDF at room temperature was reported in this paper. A commercial LM-25 aluminium alloy ingot was melted in an electric casting furnace and poured into a preheated rectangular casting die. The samples were then solutionized for 10 h at 535 °C and quenched in water for MDF processing. Microstructure analysis of the samples was done with the help of optical microscopy and scanning electron microscopy. Microstructural observation of MDF processed up to six passes sample showed that coarse eutectic silicon particles with an average length of 16 µm are effectively broken into fine particles with an average length of 4 µm and uniformly distributed in aluminium phase. After six passes, UTS of as-cast specimen is increased from 177 to 441 MPa and microhardness is increased from 75 to 127 Hv. XRD analysis of the samples confirmed the presence of Al phase and eutectic Si phase. Therefore, modification of eutectic Si particle with Al phase refinement has been demonstrated to be a very important factor for enhancing mechanical properties of aluminium–silicon alloy. © 2020, The Indian Institute of Metals - IIM.
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    Effect of zinc content on the microstructure and mechanical properties of Al-Zn-Mg alloy
    (Elsevier Ltd, 2022) Manjunath, G.K.; Udaya Bhat, K.; Preetham Kumar, G.V.
    In the present work, Aluminium-Zinc-Magnesium alloys (5 wt%, 10 wt% and 15 wt% Zinc and 2 wt% Magnesium) were prepared by casting process in a metal die. After casting process, heat treatment was conducted to the prepared alloys. To study the consequence of Zinc on the prepared alloys microstructure and mechanical properties were investigated. In as-cast state, in all three compositions, dendrite formation was noticed. While, after homogenization heat treatment, grain boundaries were noticed. Rise in the Zinc in the material leads to enhance the secondary particles. Microhardness and tension experiments were conducted to investigate the mechanical properties. Rise in the Zinc in the material leads to enhance the microhardness and tension strength. But ductility of the material declined with rise in the Zinc in the material. © 2021