Faculty Publications
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Item Influence of microwave hybrid heating on the sliding wear behaviour of HVOF sprayed CoMoCrSi coating(Institute of Physics Publishing helen.craven@iop.org, 2018) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.CoMoCrSi superalloy powder (Tribaloy-T400) consists of intermetallic laves phase and primary eutectic phase of Co-rich solid solution. Processing of Tribaloy-T400 powder is carried out through high-energy ball milling (HEBM) technique to obtain a higher volume fraction of intermetallic laves phases. The feedstock is sprayed using high-velocity-oxy-fuel (HVOF) process on titanium grade-15 substrate. The coating microstructure is homogenized by microwave hybrid heating technique. Characterization of feedstock, as-sprayed and microwave fused coatings is done by using Scanning Electron Microscopy (SEM), Energy dispersive spectroscopy (EDS) and x-ray Diffraction (XRD). Porosity, surface roughness, microhardness, and bond strength are measured. Adhesive wear behavior of the coatings under the dry sliding condition is evaluated at an applied load of l0 and 20 N and temperature of 200, 400 and 600 °C Fused coating exhibit higher wear resistance than the as-sprayed coatings and substrate. The hard intermetallic laves phases which are amorphous (bulk metallic glass) in nature strengthen the coating at high temperatures. © 2018 IOP Publishing Ltd.Item Effect of microwave heating on microstructure and elevated temperature adhesive wear behavior of HVOF deposited CoMoCrSi-Cr3C2 coating(Elsevier B.V., 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.This research reports the improvement of high-temperature sliding wear resistance of a grade 15 titanium alloy protected by an HVOF sprayed CoMoCrSi-Cr3C2 coating. The coatings have been tested in as-sprayed condition and after a post-deposition microwave heating step. The powder feedstock has been manufactured by high energy ball milling. X-ray diffraction (XRD) and Scanning Electron Microscopy (SEM) equipped with the Energy Dispersive Spectroscopy (EDS) methods were used for coatings characterization. Surface roughness, microhardness, adhesion strength, and porosity of coatings were also measured. The wear test was conducted at an applied load of l0 N and 20 N with varying temperatures of 200 °C, 400 °C, and 600 °C under dry sliding conditions. Co3Mo2Si, Co7Mo6, Mo3Si, Co3Mo, and Co2Mo3 were the intermetallic laves phases generated in the CoMoCrSi feedstock during HEBM process. The microwave-fused coating exhibited metallurgical bonding, homogeneous structure, less porosity, and greater hardness as compared to as-sprayed coating. Microwave-treated coating revealed better wear property than an as-sprayed coating. This was mainly due to the intermetallic formation and metallurgical bonding in coatings. The fused coatings exhibit tribo-oxide layers during sliding action which was the main phenomenon of improving the wear resistance of the fused composite coatings. © 2019 Elsevier B.V.Item Characterization and Sliding Wear Behavior of Iron-Based Metallic Coating Deposited by HVOF Process on Low-Carbon Steel Substrate(Springer, 2020) Prasad, C.D.; Jerri, A.; Ramesh, M.R.The main aim of this work is to improve the sliding wear resistance of boiler steel material. The iron-based or Metco 41C metallic feedstock was deposited over the ASTM-SA213-T11 steel substrate using high-velocity oxy-fuel spraying process. The resultant deposits were subsequently characterized for microstructure, density, hardness, porosity and surface roughness. These characterizations were carried out with the help of XRD, SEM and Vickers’s microhardness tester. The sliding wear performance of the substrate and coatings were investigated by varying normal loads of 10 N and 20 N at temperatures of 200 °C, 300 °C as well as room conditions by employing pin-on-disk tribometer. The friction coefficient, volume of wear loss and wear rate were being found out. The wear results were compared among the substrate and coating. The formation of additional carbide phases such as Fe2C and SiC in Metco 41C coating led to higher hardness results in better wear resistance compared with the substrate. © 2020, Springer Nature Switzerland AG.Item Comparison of Microstructural and Sliding Wear Resistance of HVOF Coated and Microwave Treated CoMoCrSi-WC + CrC + Ni and CoMoCrSi-WC + 12Co Composite Coatings Deposited on Titanium Substrate(Springer Science and Business Media B.V. editorial@springerplus.com, 2020) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.CoMoCrSi-WC + CrC + Ni and CoMoCrSi-WC + 12Co composite coatings are coated on titanium substrate by high velocity oxygen fuel method (HVOF). Prior to spraying, CoMoCrSi feedstock are processed through high energy ball milling (HEBM) in order improve the intermetallic laves phases and to reduce its particle size. The processed feedstock exhibits amorphous nature by improving laves phases and particle size of 60.12 ?m. Microwave heating energy is utilized as post heat treatment technique to improve the mechanical and metallurgical properties of as-sprayed coatings. Fused coatings reveals better properties in terms of surface roughness, porosity, microhardness and adhesion strength compared to as-sprayed coatings. Metallurgical bonding is observed in case of fused coatings due to diffusion of substrate elements. Frictional and wear behaviors have been investigated by a pin on disc apparatus at temperatures of 200 °C, 400 °C, and 600 °C under normal loads of 10 N and 20 N. Both wear trace and friction coefficients of the fused coatings are smaller than as-sprayed coatings and substrate at all test temperatures. The wear traces of fused coatings decreased with increasing the surface temperature due to the lubricant effect of cobalt oxides formed on the sliding surface. As a result, cobalt based cermet coatings are highly recommended as a durability improvement coating for the protection of sliding surface, such as high speed spindle. © 2020, Springer Nature B.V.Item EFFECT of LASER POST-TREATMENT on MICROSTRUCTURAL and SLIDING WEAR BEHAVIOR of HVOF-SPRAYED NiCrC and NiCrSi COATINGS(World Scientific, 2022) Naik, T.; Mathapati, M.; Prasad, C.D.; Nithin, H.S.; Ramesh, M.R.In this study, NiCrC and NiCrSi coatings are deposited on the MDN 310 steel using High-Velocity Oxy-Fuel (HVOF) process. Laser Surface Melting (LSM) post-heat treatment is carried out on as-sprayed coatings using Laser Engineered Net Shaping (LENSTM) with a power of 300W. The characteristics of both coatings in terms of mechanical and metallurgical properties have been investigated. The thicknesses of the as-sprayed NiCrC and NiCrSi coatings are in the range of 170-200μm. Laser-treated NiCrC and NiCrSi coatings exhibit a thickness range of 162-185μm, respectively. The microstructure of laser-treated NiCrC-300W coating clearly shows a dendrite-like structure, whereas the laser-treated NiCrSi coating exhibits hard layer and columnar homogeneity. Microhardness of as-sprayed NiCrC coating is 515±15 HV0.3 and that of NiCrSi coating is 645±25 HV0.3. Microhardness of laser-treated NiCrC coating is 720±30 HV0.3 and that of NiCrSi coating is 890±15 HV0.3. Dry sliding wear tests are conducted at room temperature (RT) and 400°C with 10-N and 20-N loads. The wear rates at 400°C temperature of laser-treated NiCrC and NiCrSi coatings produced are slightly below (1-2.2)×10-3mm3/m and (0.8-1.6)×10-3mm3/m, respectively. Laser-treated coatings produced better dry sliding wear behavior compared with as-sprayed coatings owing to dense microstructure. Formation of SiC phase in NiCrSi coating imparts high wear and frictional resistance compared to the NiCrC coating. © 2022 World Scientific Publishing Company.Item Cyclic Oxidation and Hot-Corrosion Behavior of HVOF-Sprayed NiCrAl Coating on Industrial Boiler Tube Steels(Springer, 2024) Ramesh, M.R.; Medabalimi, S.; Rupanagudi, R.S.; Prasad, C.D.; Sollapur, S.B.At high temperatures, coatings provide a protective scale development on surfaces to maintain long-term stability. In the current study, ASTM-SA210-Grade A1 (GrA1) and ASTM-SA213-T-11 (T11) boiler tube steels were coated with NiCrAl alloy with high-velocity oxy-fuel (HVOF) to prevent oxidation and hot corrosion. For hot corrosion and oxidation, 50 cycles at 900°C were taken into account. Additionally, tests of hot-corrosion behavior were conducted in an atmosphere containing molten salt (Na2SO4-60%V2O5), while tests of oxidation behavior were conducted in static air. The kinetics of oxidation were calculated using the thermogravimetric method. Using XRD, EPMA, and SEM/EDAX methods, the produced oxide scales were characterized. The oxidation rate of NiCrAl-coated steels was found to be lower than that of uncoated steels. The coated steels subjected to oxidation in air exhibit slow scale growth kinetics and oxides of α-Al2O3 and Cr2O3 on the outermost surface, while accelerated oxidation caused by the molten salt exhibits metastable Al2O3. Along the nickel-rich splat boundary, Cr and Al were formed a preferential oxidation, which prevents other oxygen from entering the coating via pores and voids, resulting in steady-state oxidation. © The Minerals, Metals & Materials Society 2024.