Faculty Publications

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Author: search.filters.author.Prasad, C.D.Subject: search.filters.subject.Chromium alloys

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    Influence of microwave hybrid heating on the sliding wear behaviour of HVOF sprayed CoMoCrSi coating
    (Institute of Physics Publishing helen.craven@iop.org, 2018) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    CoMoCrSi superalloy powder (Tribaloy-T400) consists of intermetallic laves phase and primary eutectic phase of Co-rich solid solution. Processing of Tribaloy-T400 powder is carried out through high-energy ball milling (HEBM) technique to obtain a higher volume fraction of intermetallic laves phases. The feedstock is sprayed using high-velocity-oxy-fuel (HVOF) process on titanium grade-15 substrate. The coating microstructure is homogenized by microwave hybrid heating technique. Characterization of feedstock, as-sprayed and microwave fused coatings is done by using Scanning Electron Microscopy (SEM), Energy dispersive spectroscopy (EDS) and x-ray Diffraction (XRD). Porosity, surface roughness, microhardness, and bond strength are measured. Adhesive wear behavior of the coatings under the dry sliding condition is evaluated at an applied load of l0 and 20 N and temperature of 200, 400 and 600 °C Fused coating exhibit higher wear resistance than the as-sprayed coatings and substrate. The hard intermetallic laves phases which are amorphous (bulk metallic glass) in nature strengthen the coating at high temperatures. © 2018 IOP Publishing Ltd.
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    High-Temperature Oxidation Studies of Plasma-Sprayed NiCrAlY/TiO2 and NiCrAlY/Cr2O3/YSZ Cermet Composite Coatings on MDN-420 Special Steel Alloy
    (Springer, 2021) Madhu Sudana Reddy, G.; Prasad, C.D.; Shetty, G.; Ramesh, M.R.; Rao, T.N.; Patil, P.
    The plasma spray process was used to form 70%NiCrAlY + 30%TiO2 and 70%NiCrAlY + 25%Cr2O3 + 5%YSZ cermet coatings on MDN-420 special steel alloy. Cyclic oxidation testing was conducted on coated and uncoated specimens at 700°C under a static air environment. Thermogravimetric analysis was applied to establish the oxidation kinetics. X-ray diffraction (XRD), scanning electron microscopy (SEM)/energy-dispersive x-ray spectroscopy (EDS), and electron probe microanalysis (EPMA) techniques were used to analyze the oxidized products. The NiCrAlY + Cr2O3 + YSZ coating was found to be most resistive when compared with the NiCrAlY + TiO2 coating in the aggressive oxidation environment. Net weight loss was observed for bare MDN-420 alloy due to sputtering. The oxidation resistance of the coatings was due to formation of Cr2O3, NiCr2O4, NiO, and Al2O3 phases. © 2021, ASM International.
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    EFFECT of LASER POST-TREATMENT on MICROSTRUCTURAL and SLIDING WEAR BEHAVIOR of HVOF-SPRAYED NiCrC and NiCrSi COATINGS
    (World Scientific, 2022) Naik, T.; Mathapati, M.; Prasad, C.D.; Nithin, H.S.; Ramesh, M.R.
    In this study, NiCrC and NiCrSi coatings are deposited on the MDN 310 steel using High-Velocity Oxy-Fuel (HVOF) process. Laser Surface Melting (LSM) post-heat treatment is carried out on as-sprayed coatings using Laser Engineered Net Shaping (LENSTM) with a power of 300W. The characteristics of both coatings in terms of mechanical and metallurgical properties have been investigated. The thicknesses of the as-sprayed NiCrC and NiCrSi coatings are in the range of 170-200μm. Laser-treated NiCrC and NiCrSi coatings exhibit a thickness range of 162-185μm, respectively. The microstructure of laser-treated NiCrC-300W coating clearly shows a dendrite-like structure, whereas the laser-treated NiCrSi coating exhibits hard layer and columnar homogeneity. Microhardness of as-sprayed NiCrC coating is 515±15 HV0.3 and that of NiCrSi coating is 645±25 HV0.3. Microhardness of laser-treated NiCrC coating is 720±30 HV0.3 and that of NiCrSi coating is 890±15 HV0.3. Dry sliding wear tests are conducted at room temperature (RT) and 400°C with 10-N and 20-N loads. The wear rates at 400°C temperature of laser-treated NiCrC and NiCrSi coatings produced are slightly below (1-2.2)×10-3mm3/m and (0.8-1.6)×10-3mm3/m, respectively. Laser-treated coatings produced better dry sliding wear behavior compared with as-sprayed coatings owing to dense microstructure. Formation of SiC phase in NiCrSi coating imparts high wear and frictional resistance compared to the NiCrC coating. © 2022 World Scientific Publishing Company.
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    High temperature erosion performance of NiCrAlY/Cr2O3/YSZ plasma spray coatings
    (Taylor and Francis Ltd., 2023) Reddy, G.M.S.; Prasad, C.D.; Patil, P.; Shetty, G.; Naresh, N.; Ramesh, M.R.
    The current investigation's objective was to assess the air jet erosion tester's ability to measure the erosive behaviour of plasma sprayed coatings on titanium-15 alloy. 65% NiCrAlY, 30% Cr2O3, and 5% YSZ make up the coating's chemical composition. A study of microstructure and phases was carried out. Microhardness and adhesive strength have both been measured in this work. With impact angles of 30° and 90° at 300°C, 500°C, and 700°C, Al2O3 erodent was utilised in a solid particle erosion test. An optical profilometer was used to calculate the erosion volume loss. The coating erosion resistance was found to be higher than the substrate sample for the test temperature that was employed, and this was more obvious at higher impact angles and higher temperatures The ductile character of the coating is seen in the contour of the deteriorated coating surface. © 2023 Institute of Materials Finishing Published by Taylor & Francis on behalf of the Institute.
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    Investigation of the effect of NiCrAlY/Cr2O3/YSZ plasma coatings on erosion performance of MDN 420 steel at high temperature
    (Inderscience Publishers, 2023) Reddy, G.M.S.; Prasad, C.D.; Patil, P.; Shetty, G.K.; Kakur, N.; Ramesh, M.R.
    The purpose of the current study was to use an air jet erosion tester to examine the erosive behaviour of plasma sprayed coatings on MDN-420 that were composed of 70% NiCrAlY, 25% Cr2O3, and 5% YSZ. Microstructure and phase studies were performed. Measurements were made on the microhardness and adhesion strength. Al2O3 erodent was used in a solid particle erosion test with impact angles of 30° and 90° at 300°C, 500°C, and 700°C. The erosion volume loss was measured using an optical profilometer. For the test temperature used, it was found that the coating’s erosion resistance was greater than that of the substrate and that it was more pronounced at higher impact angles and higher temperatures. The shape of the degraded coating surface reflects the coating’s ductile nature. © © 2023 Inderscience Enterprises Ltd.
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    Effect of Mo- and SiC-Reinforced NiCr Microwave Cladding on Microstructure, Mechanical and Wear Properties
    (Springer, 2023) Sharanabasava, H.; Prasad, C.D.; Ramesh, M.R.
    A microwave hybrid heating technique was applied to produce the NiCr-Mo-SiC composite cladding on Titan-31. The developed claddings were tested for microstructural features, phase analysis, microhardness, and surface roughness parameters using scanning electron microscopy (SEM), X-ray diffraction (XRD), Vickers Microhardness, and 3D optical profilometers, respectively. Using a static alumina indenter on microwave clads, the linear reciprocator ball on plate wear test was performed. Both friction and wear track metrics have been studied. A dense microstructure without observable holes or fractures has been achieved, together with a homogeneous distribution of hard phases and strong metallurgical bonding. Cladding is typically three times tougher than the underlying metal. Due to the formation of hard carbide phases, which increased hardness and internal lubricity, cladding has a lower coefficient of friction than the substrate. © 2023, The Institution of Engineers (India).
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    Cyclic Oxidation and Hot-Corrosion Behavior of HVOF-Sprayed NiCrAl Coating on Industrial Boiler Tube Steels
    (Springer, 2024) Ramesh, M.R.; Medabalimi, S.; Rupanagudi, R.S.; Prasad, C.D.; Sollapur, S.B.
    At high temperatures, coatings provide a protective scale development on surfaces to maintain long-term stability. In the current study, ASTM-SA210-Grade A1 (GrA1) and ASTM-SA213-T-11 (T11) boiler tube steels were coated with NiCrAl alloy with high-velocity oxy-fuel (HVOF) to prevent oxidation and hot corrosion. For hot corrosion and oxidation, 50 cycles at 900°C were taken into account. Additionally, tests of hot-corrosion behavior were conducted in an atmosphere containing molten salt (Na2SO4-60%V2O5), while tests of oxidation behavior were conducted in static air. The kinetics of oxidation were calculated using the thermogravimetric method. Using XRD, EPMA, and SEM/EDAX methods, the produced oxide scales were characterized. The oxidation rate of NiCrAl-coated steels was found to be lower than that of uncoated steels. The coated steels subjected to oxidation in air exhibit slow scale growth kinetics and oxides of α-Al2O3 and Cr2O3 on the outermost surface, while accelerated oxidation caused by the molten salt exhibits metastable Al2O3. Along the nickel-rich splat boundary, Cr and Al were formed a preferential oxidation, which prevents other oxygen from entering the coating via pores and voids, resulting in steady-state oxidation. © The Minerals, Metals & Materials Society 2024.