Faculty Publications

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    Investigation of microstructural and tribological behavior of Metco 41C+WC-12Co composite coatings sprayed via HVOF process
    (CRC Press, 2021) Prasad, C.D.; Mathapati, M.; Ramesh, M.R.; Joladarashi, S.
    The present work deals with developing an elevated-temperature sliding, wear-resistant, iron-based (Metco 41C) composite coating on the boiler steel substrate using high-velocity oxy fuel (HVOF) system. Prior to coating, Metco 41C (70%) and WC-12Co (30%) were mixed mechanically using ball milling process. Later, feedstock was employed into the HVOF system to develop the coating. The coating samples were subjected to metallurgical and mechanical characterization techniques under required conditions. Further substrate and coating were taken for wear test without employing lubrication through pin on disc apparatus. Wear test was carried out by selecting 10 and 20 N loads at room temperature, 200°C, and 300°C parameters. The sliding distance and the velocity were kept constant. The worn-out samples were analyzed for microstructural changes and formation of phases using SEM and XRD methods, respectively. The wear properties of friction coefficient, wear rate, and loss of volume were calculated. Deposited coating exhibited hard phases such as Cr3C2, Ni3C, W2C, Fe2C, and SiC along with intermetallic phases like Mo2C and Co3W3C. The result is improvement in hardness and better wear resistance with respect to the substrate. © 2022 selection and editorial matter, Lalit Thakur, Hitesh Vasudev. All rights reserved.
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    Evaluation of microstructural and dry sliding wear resistance of iron-based SiC-reinforced composite coating by HVOF process wear resistance of Fe-based coatings
    (CRC Press, 2021) Prasad, C.D.; Jerri, A.; Ramesh, M.R.
    The current work describes the evaluation of microstructural and sliding wear resistance of iron-based composite coatings. The feedstock having (70%) Metco 41C and (30%) SiC were blended mechanically through ball milling process. Further, the prepared feedstock was sprayed by HVOF method on ASTM-SA213-T11 steel substrate. Fabricated coating samples and substrate were characterized on different metallurgical and mechanical methods. The coating and substrate were taken into sliding test using pin on disc tribometer by varying parameters of normal load 10 and 20 N at temperatures 200°C, 300°C as well as room conditions without applying lubrication. The tested samples were analyzed in terms of its microstructural and phase formation using SEM and XRD techniques, respectively. The wear properties such as friction coefficient, loss of material in terms of volume and wear rate of coating and substrate were estimated utilizing system-generated data. The hardness and wear resistance of coating improved due to the existence of hard carbide phases, such as SiC and Fe2C in coating area, were detected. © 2022 selection and editorial matter, Lalit Thakur, Hitesh Vasudev. All rights reserved.
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    High temperature gradient cobalt based clad developed using microwave hybrid heating
    (American Institute of Physics Inc. subs@aip.org, 2018) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Sarkar, A.
    The development of cobalt based cladding on a titanium substrate using microwave cladding technique is benchmark in coating area. The developed cladding would serve the function of a corrosion resistant coating under high temperatures. Clads of thickness 500 μm have been developed by microwave hybrid heating. A microwave furnace of 2.45GHz frequency was used at a 900W power level for processing. Impact of processing time on melting and adhesion of clad has been discussed. The study also extended to static thermal analysis of simple parts with cladding using commercial Finite Element analysis (FEA) software. A comparative study is explored between four variants of the clad being developed. The analysis has been conducted using a square sample. Similar temperature gradient is also shown for a proposed multi-layer coating, which includes a thermal barrier coating yttria stabilized zirconia (YSZ) on top of the corrosion resistant clad. The YSZ coating would protect the corrosion resistant cladding and substrate from high temperatures. © 2018 Author(s).
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    Comparative investigation of HVOF and flame sprayed CoMoCrSi coating
    (American Institute of Physics Inc. subs@aip.org, 2020) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.
    Present studies deals with comparison of high velocity oxy fuel and flame spray coating process by developing CoMoCrSi (Tribaloy T400) coating on a titanium grade-15 substrate. Prior to coating, feedstock is processed to obtain higher fraction intermetallics through high energy ball milling technique under controlled atmosphere. Processed feedstock material is sprayed on a Ti-15 substrate through HVOF and Flame spray process. The coated specimens are subjected to metallurgical and mechanical characterization using optical microscope, scanning electron microscope, energy dispersive spectroscopy, x-ray diffraction, Vickers mico hardness tester and bond strength using pull off test method. HVOF sprayed coating exhibits superior properties compared to Flame sprayed coating in terms of surface roughness, porosity, micro hardness and adhesion strength. The detailed studies of two coating systems is discussed. © 2020 Author(s).
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    Influence of microwave hybrid heating on the sliding wear behaviour of HVOF sprayed CoMoCrSi coating
    (Institute of Physics Publishing helen.craven@iop.org, 2018) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    CoMoCrSi superalloy powder (Tribaloy-T400) consists of intermetallic laves phase and primary eutectic phase of Co-rich solid solution. Processing of Tribaloy-T400 powder is carried out through high-energy ball milling (HEBM) technique to obtain a higher volume fraction of intermetallic laves phases. The feedstock is sprayed using high-velocity-oxy-fuel (HVOF) process on titanium grade-15 substrate. The coating microstructure is homogenized by microwave hybrid heating technique. Characterization of feedstock, as-sprayed and microwave fused coatings is done by using Scanning Electron Microscopy (SEM), Energy dispersive spectroscopy (EDS) and x-ray Diffraction (XRD). Porosity, surface roughness, microhardness, and bond strength are measured. Adhesive wear behavior of the coatings under the dry sliding condition is evaluated at an applied load of l0 and 20 N and temperature of 200, 400 and 600 °C Fused coating exhibit higher wear resistance than the as-sprayed coatings and substrate. The hard intermetallic laves phases which are amorphous (bulk metallic glass) in nature strengthen the coating at high temperatures. © 2018 IOP Publishing Ltd.
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    Microstructure and tribological behavior of flame sprayed and microwave fused CoMoCrSi/CoMoCrSi-Cr3C2 coatings
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    This present work deals with the investigation of dry sliding wear behavior of CoMoCrSi and CoMoCrSi-Cr3C2 depositing on titanium substrate through Flame spray process, subsequently fused by the microwave hybrid heating process. Prior to the deposition of the coating, CoMoCrSi powder is milled by using high energy ball milling (HEBM) process and later 30% of Cr3C2 powder is added. Microstructural features and phase analysis of milled powders, as-coated and microwave fused coatings are inspected by using SEM with EDS and XRD process respectively. The coatings before and after fusing are tested for microhardness and bond strength by using a Vickers microhardness and universal tensile machines respectively. Dry sliding wear behavior of coatings before and after fusing is conducted against alumina counter face at ambient and elevated temperatures, also normal load is varied. The wear mechanism of both coatings is examined by employing XRD, SEM-EDS techniques. The fused coatings exhibit lower friction and better wear resistance compared with as-deposited coatings. The detailed results of each test of their coatings are discussed in this paper. © 2018 IOP Publishing Ltd.
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    Effect of microwave heating on microstructure and elevated temperature adhesive wear behavior of HVOF deposited CoMoCrSi-Cr3C2 coating
    (Elsevier B.V., 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    This research reports the improvement of high-temperature sliding wear resistance of a grade 15 titanium alloy protected by an HVOF sprayed CoMoCrSi-Cr3C2 coating. The coatings have been tested in as-sprayed condition and after a post-deposition microwave heating step. The powder feedstock has been manufactured by high energy ball milling. X-ray diffraction (XRD) and Scanning Electron Microscopy (SEM) equipped with the Energy Dispersive Spectroscopy (EDS) methods were used for coatings characterization. Surface roughness, microhardness, adhesion strength, and porosity of coatings were also measured. The wear test was conducted at an applied load of l0 N and 20 N with varying temperatures of 200 °C, 400 °C, and 600 °C under dry sliding conditions. Co3Mo2Si, Co7Mo6, Mo3Si, Co3Mo, and Co2Mo3 were the intermetallic laves phases generated in the CoMoCrSi feedstock during HEBM process. The microwave-fused coating exhibited metallurgical bonding, homogeneous structure, less porosity, and greater hardness as compared to as-sprayed coating. Microwave-treated coating revealed better wear property than an as-sprayed coating. This was mainly due to the intermetallic formation and metallurgical bonding in coatings. The fused coatings exhibit tribo-oxide layers during sliding action which was the main phenomenon of improving the wear resistance of the fused composite coatings. © 2019 Elsevier B.V.
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    Development and Sliding Wear Behavior of Co-Mo-Cr-Si Cladding through Microwave Heating
    (Springer editorial@springerplus.com, 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    The aim of the present study is to improve the sliding wear resistance of pure titanium grade-2 substrate by developing CoMoCrSi (Tribaloy T400) cladding on it by using microwave hybrid heating technique. The developed cladding is characterized by microstructural features, phase analysis, measurement of microhardness by employing a scanning electron microscope (SEM), X-ray diffraction (XRD) and Vickers microhardness. The cladding and substrate are subjected to sliding wear test against alumina counterpart at elevated temperatures under dry conditions using a pin on disc tribometer. The test is performed by varying normal load and temperatures, whereas sliding speed is maintained constant. The developed clad shown partial melting of CoMoCrSi powders and obtained sound metallurgical bonding with the substrate. The high specific energy of microwave diluted the substrate atoms into cladding region which forms Cr3C2, Co3Ti, and TiC, phases confirmed by phase analysis. The cladding obtained better porosity and microhardness are 1.5 ± 0.2% ?m and 760 ± 35 Hv respectively. The substrate exhibits low microhardness of 182 ± 25 Hv. The cladding exhibits 6 times of lower volume loss and 70.14% of less wear rate with respect to the substrate. The cladding experienced least coefficient of friction is 0.55 compared with the substrate. The worn surfaces of cladding and substrate are examined. The detailed mechanism of wear is discussed in this paper. © 2019, Springer Nature B.V.
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    Characterization and Sliding Wear Behavior of Iron-Based Metallic Coating Deposited by HVOF Process on Low-Carbon Steel Substrate
    (Springer, 2020) Prasad, C.D.; Jerri, A.; Ramesh, M.R.
    The main aim of this work is to improve the sliding wear resistance of boiler steel material. The iron-based or Metco 41C metallic feedstock was deposited over the ASTM-SA213-T11 steel substrate using high-velocity oxy-fuel spraying process. The resultant deposits were subsequently characterized for microstructure, density, hardness, porosity and surface roughness. These characterizations were carried out with the help of XRD, SEM and Vickers’s microhardness tester. The sliding wear performance of the substrate and coatings were investigated by varying normal loads of 10 N and 20 N at temperatures of 200 °C, 300 °C as well as room conditions by employing pin-on-disk tribometer. The friction coefficient, volume of wear loss and wear rate were being found out. The wear results were compared among the substrate and coating. The formation of additional carbide phases such as Fe2C and SiC in Metco 41C coating led to higher hardness results in better wear resistance compared with the substrate. © 2020, Springer Nature Switzerland AG.
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    Comparison of Microstructural and Sliding Wear Resistance of HVOF Coated and Microwave Treated CoMoCrSi-WC + CrC + Ni and CoMoCrSi-WC + 12Co Composite Coatings Deposited on Titanium Substrate
    (Springer Science and Business Media B.V. editorial@springerplus.com, 2020) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.
    CoMoCrSi-WC + CrC + Ni and CoMoCrSi-WC + 12Co composite coatings are coated on titanium substrate by high velocity oxygen fuel method (HVOF). Prior to spraying, CoMoCrSi feedstock are processed through high energy ball milling (HEBM) in order improve the intermetallic laves phases and to reduce its particle size. The processed feedstock exhibits amorphous nature by improving laves phases and particle size of 60.12 ?m. Microwave heating energy is utilized as post heat treatment technique to improve the mechanical and metallurgical properties of as-sprayed coatings. Fused coatings reveals better properties in terms of surface roughness, porosity, microhardness and adhesion strength compared to as-sprayed coatings. Metallurgical bonding is observed in case of fused coatings due to diffusion of substrate elements. Frictional and wear behaviors have been investigated by a pin on disc apparatus at temperatures of 200 °C, 400 °C, and 600 °C under normal loads of 10 N and 20 N. Both wear trace and friction coefficients of the fused coatings are smaller than as-sprayed coatings and substrate at all test temperatures. The wear traces of fused coatings decreased with increasing the surface temperature due to the lubricant effect of cobalt oxides formed on the sliding surface. As a result, cobalt based cermet coatings are highly recommended as a durability improvement coating for the protection of sliding surface, such as high speed spindle. © 2020, Springer Nature B.V.