Faculty Publications

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Author: search.filters.author.Prabhu, K.N.Subject: search.filters.subject.Stainless steel

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    Wetting behavior and evolution of microstructure of Sn-3.5Ag solder alloy on electroplated 304 stainless steel substrates
    (Springer India sanjiv.goswami@springer.co.in, 2012) Nayak, V.U.; Prabhu, K.N.; Stanford, N.; Satyanarayan, S.
    In the present study, wetting characteristics and evolution of microstructure of Sn-3.5Ag solder on Ag/Ni and Ni electroplated 304 stainless steel (304SS) substrates have been investigated. Solder alloy spread on Ag/Ni plated 304SS substrates exhibited better wetting as compared to Ni/304SS substrate. The formations of irregular shaped and coarser IMCs were found at the interface of solder/Ni/304SS substrate region whereas, solder/Ag/Ni/substrate interface showed continuous scallop and needle shaped IMCs. The precipitation of Ag3Sn, Ni-Sn, FeSn2 and lesser percentage of Fe-Cr-Sn IMCs were found at the interface of solder/Ag/Ni/substrate region whereas, solder/Ni/304 SS substrate exhibited predominantly FeSn2 and Fe-Cr-Sn IMCs. Presence of higher amount of Fe-Cr-Sn IMCs at the solder/Ni/304SS substrate interface inhibited the further wetting of solder alloy.
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    Effect of surface roughness on metal/quenchant interfacial heat transfer and evolution of microstructure
    (Elsevier Ltd, 2007) Prabhu, K.N.; Fernandes, P.
    In the present work, the effect of surface roughness on heat transfer rates in various quenchants was determined. The heat flux transients at the probe/quenchant interface were estimated by inverse modeling of heat conduction during end quenching of stainless steel probes with three different surface roughness (grooved, Ra = 3.0 and 1 ?m). Heat transfer during quenching was correlated with the hardness obtained for medium carbon AISI 1060 steel specimens. The effect of surface roughness on heat transfer rate during quenching in water and brine was significant for rough surface whereas its effect on heat transfer rate is only marginal in high viscosity oil quenchants. A fully martensitic structure was observed with grooved surface subjected to water quenching. With a smooth surface a mixed microstructure was obtained. The oil quenched specimens were found to be less sensitive to surface roughness. © 2005 Elsevier Ltd. All rights reserved.
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    Effect of substrate surface roughness on wetting behaviour of vegetable oils
    (2009) Prabhu, K.N.; Fernades, P.; Kumar, G.
    Vegetable oils are mainly used in the heat treating industry due to their environmental friendliness. In the present work the effect of surface roughness on spreading of vegetable oils on stainless steel substrates was investigated. Spreading phenomenon was digitally recorded and analyzed. All of the oils under investigation exhibited power law spreading behaviour of the type: A = ktn, where A, t, k and n represent the drop base contact area, spreading time, constant and exponent, respectively. The coconut and sunflower oils exhibited accelerated kinetics owing to their lower viscosity as compared to palm and mineral oils while peanut oil showed intermediate behaviour. Viscous regime was dominant during spreading of mineral and palm oils as compared to that of coconut oil. All the oils took longer period of time on rough surfaces than on smooth surfaces to relax to the same degree of wetting. Oils spreading on rough surfaces had to overcome the additional barrier due to asperities of the rough surface. Contact angle decreased with increase in roughness supporting the Wenzel's proposition. The decrease was significant for increase in roughness from 0.25 ?m to 0.50 ?m for all oils. However, the effect was negligible with further increase in roughness particularly for high viscosity oils. A spread parameter (?) is proposed to account for the variation of contact angle with surface roughness of the substrate and momentum diffusivity of the spreading liquid. The result suggested that low viscosity liquids exhibit improved wetting characteristics during spreading on rough surfaces. A model is proposed to estimate dynamic contact angles on substrates having varying surface roughness. © 2008 Elsevier Ltd. All rights reserved.
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    Enhancement of heat transfer characteristics of transformer oil by addition of aluminium nanoparticles
    (2011) Rajesh, E.; Prabhu, K.N.
    A two step approach involving the synthesis of Al nanoparticles by mechanical milling followed by dispersion of the nanoparticles in the base fluid is adopted in the present work to prepare transformer oil based nanofluids. Stainless steel (AISI 304) probes of diameter 15 mm and height 70 mm were used to determine the cooling rate intensities of nanofluids. Heat transfer coefficients were determined using Kobasko's method. A dynamic contact angle analyzer was used to determine the contact angle of the droplet on the substrate. The addition of Al nanoparticles to the base fluid decreases the wettability and improves its heat transfer capability. The vapour phase stage existed for a longer period of time for transformer oil than for Al-transformer oil based nanofluids. The dispersion of nanoparticles in the base fluid is believed to disrupt the vapour blanket stage in the early stage of the cooling process. The peak heat transfer coefficient increases with an increase in the Al nanoparticle content in the oil. The addition of 0.5 vol % nanoparticles enhances the peak heat transfer coefficient by about 70 %. Copyright © 2011 by ASTM International.
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    Comparison of Grossmann and lumped heat capacitance methods for assessment of heat transfer characteristics of quench media
    (2011) Prabhu, K.N.; Ali, I.
    The suitability of Grossmann and lumped heat capacitance (LHC) methods for estimation of quench severity of nanofluids, brine solutions and a laboratory detergent based medium was investigated. The study involved the assessment of the effect of section thickness of the probe on heat transfer coefficients for different quench media. Computer aided cooling curve analysis during quenching of type 304 stainless steel probes was carried out. The measured thermal history data were used to estimate heat transfer coefficients by Grossmann and LHC methods. The LHC method based on a 10 mm diameter stainless steel probe was found to be applicable for characterising media having quench severity less than 20 m-1. Although Grossmann method is based on the concept of average heat transfer coefficient, it can be used for quench media having varying severity of quenching. Grossmann method is found to be more sensitive to the effect of section thickness on heat transfer. © 2011 IHTSE Partnership.
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    Heat transfer at the casting/chill interface during solidification of commercially pure Zn and Zn base alloy (ZA8)
    (2012) Ramesh, G.; Prabhu, K.N.
    Casting/chill interfacial heat transfer during solidification of commercially pure zinc and ZA8 alloy against copper, hot die steel, stainless steel and aluminiuminstrumented chills was investigated. The peak heat flux strongly depends on the thermophysical properties of chill, chill surface condition and superheat of the castingmaterial. Contact angles of alumina coatingmeasured on various substrates suggested that the adhesion of the coating material on copper chill was significantly better as compared to other chill materials. The heat flux curve in the case of coated chills is characterised by a double peak indicating remelting of the solidified casting shell. The second peak in the HTC curve is lower for high conductivity and higher for low conductivity chills as compared to the first peak. It is possible that solid shell formation and remelting occurred in the case of high thermal conductivity chills, whereas shell remelting did not happen in lower thermal conductivity chills. © 2012 W. S. Maney & Son Ltd.
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    Wettability and Interfacial Heat Transfer During Solidification of Al–Si Alloy (A413) Melt Droplets on Metallic Substrates
    (Springer Science and Business Media Deutschland GmbH, 2024) Shamil, K.M.; Kamala Nathan, D.; Prabhu, K.N.
    Wetting and heat transfer during solidification were studied with Al–Si alloy (A413) melt droplets on copper and stainless steel cylindrical substrates. As the molten metal cools down and solidifies, the interface changes from the initial liquid/solid contact to solid/solid contact, leading to variations in the rate of interfacial heat transfer. The effect of substrate roughness and melt superheat on the droplet contact angle and heat flux was investigated. A smooth substrate surface resulted in higher casting surface roughness, and the contact angle of solidified droplets increased with an increase in substrate roughness. Surface profile analysis indicated the presence of an air gap between the substrate and solidified droplet. The gap width was used to determine the variation of heat transfer coefficient (HTC) along the radial direction of the substrate surface at the end of solidification. Deformation of the solidified droplet was inverse for copper versus stainless steel resulting in an increase in HTC for copper and a decrease for stainless steel. © 2023, American Foundry Society.