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    Microstructural and Hardness evolution of AZ80 alloy after ECAP and post-ECAP processes
    (Elsevier Ltd, 2018) Naik, G.M.; Gote, G.D.; Narendranath, S.
    This research paper investigates the microstructure evolution and hardness variation of wrought AZ80 magnesium alloy after each ECAP passes. The strengthening effect of AZ80 alloy was examined after post-ECAP aging treatment. Alloys were severely deformed through equal channel angular press at 533K using route Bc with a die channel angle (φ) 1100 and corner angle (ψ) 300. Subsequently, the microstructural characterization was studied using optical microscope (OM) and scanning electron microscope (SEM). Further, post-ECAP aging treatment at 523K for 6h and 12h was performed and microhardness of the specimens was measured. It was found that the grain refinement through thermo-mechanical processing of ECAP and Post-ECAP treatment significantly improves the microhardness of the Mg alloy, which directly influences the properties of wrought AZ80 magnesium alloy. © 2018 Elsevier Ltd. All rights reserved.
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    A review on wrought magnesium alloys processed by equal channel angular pressing
    (Inderscience Publishers, 2015) Muralidhar, M.; Narendranath, S.; Shivananda Nayaka, H.S.
    Magnesium and its alloys with severe plastic deformation (SPD) techniques are more attractive as structural parts in many industrial applications because of their advantages. In this paper, the importance of wrought magnesium alloys with their applications to accomplish the essential development of components is reviewed. In addition, the different approaches of equal channel angular pressing (ECAP) process for refining the grain size to achieve the ultrafine grained material on the bulk metals are discussed. Recent developments in the ECAP process are outlined clearly with their importance to overcome many complexities. Various factors like processing temperature of a specimen, die geometry, ram speed, back pressure and processing routes influencing during ECAP process of wrought magnesium alloys at different conditions such as channel angle and corner or outer arc angle are discussed. Finally, the properties of ECAP processed wrought alloys are outlined for improving the microstructure in structural parts. © © 2015 Inderscience Enterprises Ltd.
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    Effect of equal channel angular pressing on AZ31 wrought magnesium alloys
    (National Engg. Reaserch Center for Magnesium Alloys zhangdingfei@cqu.edu.cn, 2013) Muralidhar, A.; Narendranath, S.; Shivananda Nayaka, H.
    AZ31 wrought magnesium alloys are light weight materials which play an important role in order to reduces the environmental burdens in modern society because of its high strength to weight ratio, corrosion resistance, and stiffness and machinability. Applications of this material are mainly in structural component i.e., in constructions, automobile, aerospace, electronics and marine industries. In the present work, the microstructure characterization of the AZ31 alloys up to four ECAP passes at temperature of 573 K was observed for route Bc. Average grain size of the material was reduced from 31.8 ?m to 8 ?m after four ECAP passes. Mechanical properties of the alloy improved with increase in number of ECAP passes. Moreover, X-ray diffraction analysis was carried out for as received and ECAP processed material. © 2013 National Engineering Research Center for Magnesium Alloys of China, Chongqing University.
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    Influence of Route-R on wrought magnesium AZ61 alloy mechanical properties through equal channel angular pressing
    (National Engg. Reaserch Center for Magnesium Alloys zhangdingfei@cqu.edu.cn, 2014) Muralidhar, M.; Narendranath, S.
    A new fundamental route entitled 'Route-R' is introduced to refine the grains in the material through Equal Channel Angular Pressing (ECAP) process. In route R, specimen is inverted to the original position in each ECAP pass. In the present work, AZ61 alloy is processed using ECAP process for three different fundamental routes mainly route A, route Bc, and route R. ECAP experiment is carried out on AZ61 alloy at lower temperature of 483 K up to two passes. Microstructural characterization is evaluated on unECAPed and ECAPed specimens for three routes. Average grain size of the alloy is to be reduced from 66 ?m to 16 ?m, 14.1 ?m and 10 ?m for route A routes Bc, and route R respectively. Vickers microhardness of the alloy is found to be 60 HV for as received material. This microhardness of the alloy is increased to 71 HV, 72 HV, and 74 HV for route A, route Bc, and route R respectively. Mechanical properties of the AZ61 alloy are observed to be route R is providing maximum YS, UTS, and percentage elongation than other route A and route Bc. Tensile fracture topography of the specimen is analyzed using three different routes for two passes. © 2014 National Engineering Research Center for Magnesium Alloys of China, Chongqing University.
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    Effect of Secondary Mg17Al12 Phase on AZ80 Alloy processed by Equal Channel Angular Pressing (ECAP)
    (Springer Netherlands, 2018) Muralidhar, M.; Narendranath, S.
    AZ80 alloy was subjected through Equal Channel Angular Pressing (ECAP) to refine the grains at three different temperatures 548 K, 573 K, and 623 K up to 4 passes for route Bc, where the specimen is rotated 90? counter-clockwise direction for each pass. In the present work, experiments have been continued with route Bc and the average grain size was obtained of 7 ?m, 9.5 ?m and 11.2 ?m for the temperatures of 548 K, 573 K, and 623 K respectively after 4 ECAP passes. The average grain size of the procured AZ80 alloy was found to be 44.5 ?m. Mechanical properties of AZ80 alloy have been improved to the corresponding various processing temperatures. X-ray diffraction studies have been done on a fourth ECAP processed specimen and compared with a zero pass specimen to know the phase transformation at different processing temperatures. Fracture behavior of each of the three materials was studied and it revealed brittle fracture by increasing the number of ECAP passes. © 2015, Springer Science+Business Media Dordrecht.
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    Effect of grain refinement on the performance of AZ80 Mg alloys during wear and corrosion
    (Techno-Press info@techno-press.com, 2018) Naik, G.M.; Gote, G.D.; Narendranath, S.; Satheesh Kumar, S.S.
    Magnesium and its alloys are attracted towards all engineering applications like automotive, marine, aerospace etc. due to its inherent high strength to weight ratio. But, extensive use of Mg alloys is limited to the current scenario because of low wear and corrosion resistance behavior. However, equal channel angular press is one of the severe plastic deformation technique which has been effective method to improve the wear and corrosion resistance by achieving fine grain structure. In this study, the effect of grain refinement on wear and corrosion resistance of AZ80 Mg alloys were investigated. The wear behavior of the coarse and fine-grained Mg alloys was examined through L9 orthogonal array experiments in order to comprehend the wear behavior under varies control parameters. It was shown that ECAPed alloy increased the wear and corrosion resistance of the Mg alloy through the formation of fine grain and uniform distribution of secondary beta - phase. Also, the performance of AZ80 Mg alloy for these changes was discussed through SEM morphology. © 2018 Techno-Press, Ltd.
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    Effect of ECAP Die Angles on Microstructure Mechanical Properties and Corrosion Behavior of AZ80 Mg Alloy
    (Springer New York LLC barbara.b.bertram@gsk.com, 2019) Naik, G.M.; Narendranath, S.; Kumar, S.S.S.
    In this article, the effect of channel angles on material properties was investigated during equal channel angular pressing of AZ80 magnesium alloy using processing route R at 325 °C processing temperature. Channel angles of 90° and 110° and common corner angle 30° have been considered for this study. It has been revealed that the channel angle has a significant influence on deformation homogeneity, microhardness, ultimate tensile strength, ductility and corrosion behavior of Mg alloys. Investigation with reference to as-received AZ80 Mg alloy indicates 18.47% improvement in UTS and 76.07% enhancement in ductility after processing through 3P-90° and 2P-110° ECAP, respectively. Also, the corrosion rate reduces to 89.47% after processing the sample with 3P-110° ECAP die. © 2019, ASM International.