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Item Tribological Performance of Fe-Based Composite Coatings Under Elevated Temperature Conditions(Springer, 2025) Chandramouli, T.V.; Joladarashi, S.; Ramesh, M.R.The present study investigated the tribological performance of Fe-based coatings reinforced with carbides onto a maraging steel substrate using the HVOF spray technique. These materials are widely used in manufacturing various components in the aerospace and energy sectors. Commercially available SS316L and 17-4PH are reinforced with WC–Co feedstock powders to deposit these composite coatings on maraging steel substrate. The dry sliding wear tests were conducted using the ball-on-disc tribometer at varying temperatures (25 and 300 °C) with 10 N normal load using an alumina ball (Al2O3) as the counter body. The study includes micro-hardness, porosity, density, bond strength, and surface roughness of the coatings. The samples subjected to wear testing were analyzed using SEM/EDS and XRD techniques, and the wear scar volume was measured using a 3D profilometer to calculate the volume metric loss. The wear rate of SS316L30%WC–Co is 64.46% lower than that of 17-4PH30%WC–Co at room temperature and 67.33% lower at 300 °C under a load of 10 N. At room temperature, the worn surface exhibited abrasive wear, while at 300 °C, adhesive wear and oxidative wear were observed owing to the formation of protective layers. Therefore, SS316L-30%WC–Co demonstrates superior wear resistance compared to 17-4PH-30%WC–Co and offers enhanced mechanical strength, particularly in challenging environments. The deposition of these coatings effectively protects the maraging steel substrate. © The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd. 2025.Item Tribological aspects of Al and Mg composites(Elsevier, 2025) Koppad, P.G.; Joladarashi, S.; Ramesh, M.R.; Keshavamurthy, R.It is well known that the technical function of a large number of engineering components/parts depends on motion. However, the term motion here is not as simple as it sounds, because it comes with consequences in the form of friction and wear. Along with lubrication, the science that deals with friction and wear is known as tribology. Therefore, it is necessary to pay more attention to tribology and acquire knowledge on the tribological behavior of materials, as the tribological characteristics such as friction and wear have been causing poor efficiency in engineering structures, huge economic losses, and environmental impacts. One way of addressing these issues lies in the development of lightweight materials based on metals such as aluminum and magnesium. Although one cannot employ these metals in their pure form, but modification in their microstructure and properties can certainly address the needs required for tribological applications. Keeping this in mind, this chapter covers the properties of aluminum and magnesium metals, basic aspects of tribology and most importantly, the work carried out on the friction and wear behavior of aluminum- and magnesium-based composites. The importance of this chapter lies in promoting better knowledge of the tribological behavior of aluminum and magnesium composites, especially from a various wear parameters point of view. The influence of material composition and wear parameters on tribological behavior is covered with a follow-up section on numerical and optimization methods employed for predicting tribological characteristics. © 2026 Elsevier Inc. All rights reserved..Item Tribological behaviour of monolayer and multilayer Ti-based thin solid films deposited on alloy steel(Institute of Physics Publishing helen.craven@iop.org, 2019) V Badiger, P.V.; Desai, V.; Ramesh, M.R.; Joladarashi, S.; Gourkar, H.The fretting wear and adhesive wear resistance of Ti-based thin solid films deposited on MDN121 steel substrate are evaluated. Plasma-assisted cathodic arc evaporation technique is used to develop the TiC-C monolayer coating and Ti/TiN/TiCN/TiN/TiCN multilayer coatings used in the study. FESEM-EDS, nanoindentation, Raman spectroscopy, optical profiler, and confocal microscope are used to characterise the coatings and wear tracks. Diamond-like carbon is observed in the microstructure of both the coatings. During the fretting analysis, the coefficient of friction (COF) is reduced by 68.49% in the case of the TiC-C monolayer coating and 42.46% in the Ti multilayer coatings as compared to the substrate. The volumetric wear loss of the TiC-C monolayer coating is lower than the multilayer coating. The wear surface morphology reveals the abrasive form of the fretting wear mechanism in both the monolayer and multilayer coatings whereas the galling failure in the substrate. During adhesive wear, the COF is reduced by 71.73% in the monolayer coating and 59.33% in the multilayer coatings compared to the substrate. The monolayer coating exhibits low friction and low wear rate as compared to the multilayer coating. © 2018 IOP Publishing Ltd.Item Microstructure and tribological behavior of flame sprayed and microwave fused CoMoCrSi/CoMoCrSi-Cr3C2 coatings(Institute of Physics Publishing helen.craven@iop.org, 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.This present work deals with the investigation of dry sliding wear behavior of CoMoCrSi and CoMoCrSi-Cr3C2 depositing on titanium substrate through Flame spray process, subsequently fused by the microwave hybrid heating process. Prior to the deposition of the coating, CoMoCrSi powder is milled by using high energy ball milling (HEBM) process and later 30% of Cr3C2 powder is added. Microstructural features and phase analysis of milled powders, as-coated and microwave fused coatings are inspected by using SEM with EDS and XRD process respectively. The coatings before and after fusing are tested for microhardness and bond strength by using a Vickers microhardness and universal tensile machines respectively. Dry sliding wear behavior of coatings before and after fusing is conducted against alumina counter face at ambient and elevated temperatures, also normal load is varied. The wear mechanism of both coatings is examined by employing XRD, SEM-EDS techniques. The fused coatings exhibit lower friction and better wear resistance compared with as-deposited coatings. The detailed results of each test of their coatings are discussed in this paper. © 2018 IOP Publishing Ltd.Item Tribo-mechanical and physical characterization of filament wound glass/epoxy composites(Institute of Physics Publishing helen.craven@iop.org, 2019) Biradar, S.; Joladarashi, S.; Kulkarni, S.M.The present research aims to investigate mechanical, physical and tribological properties of filament wound Glass Fibre Reinforced Polymer (GFRP) composite pressure vessel as per respective ASTM standards. Here test coupons prepared from GFRP vessel are subjected to tensile, compression, flexural and impact testing to investigate mechanical properties. The physical properties are studied from density, ignition loss and water absorption tests. The tribological study was carried out using abrasive slurry erosion tester. All tests carried out in this study are as per respective ASTM standard. The results obtained from various mechanical testings are satisfactory and also almost equal in strength with respect to metallic pressure vessels. Particularly from impact testing, the strength of sea water treated sample has considerably increased. Fractography study was conducted on failed samples to study various mode of failure in detail. The physical characterization has elaborated the behavior of filament wound GFRP material under moisture environment which has observed a maximum of 0.5% water absorption rate. As per ignition loss study which reveals about 95%-98% weight of ignition loss is recorded, which indicates perfect fibre to resin ratio and almost nil or least % of void content. The slurry erosion test results are within the expected range and maximum wear of 9.67% is recorded under extreme case. The overall study reveals that the presence of voids, non-uniform distribution of fibre and matrix have an impact on the outcomes of many mechanical properties. From the above study we can conclude that filament wound GFRP pressure vessel can be used in many applications since it is a non-hydrophobic, better wear resistant and several strength parameters have also improved or unaltered under rigorous testing conditions. © 2019 IOP Publishing Ltd.Item Microstructural and Tribological Resistance of Flame-Sprayed CoMoCrSi/WC-CrC-Ni and CoMoCrSi/WC-12Co Composite Coatings Remelted by Microwave Energy(Springer, 2020) Prasad, C.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.The hard facing composite coatings such as CoMoCrSi/30%WC-CrC-Ni and CoMoCrSi/30%WC-12Co are coated on grade-2 titanium substrate through Flame spray technique. Prior to deposition of coatings CoMoCrSi feedstock were processed using high energy ball milling to obtain intermetallic laves phases. The sprayed coatings are subjected to post-heat treatment through microwave energy to homogenize coating structure which reduces surface defects and to achieve metallurgical bonding. The as-sprayed and microwave treated coatings are examined for metallography analysis by using XRD, SEM–EDS and mechanical properties are estimated by using microhardness, universal tensile equipment. The high-temperature sliding wear tests are performed against alumina counterpart under dry conditions. The sliding wear test is conducted with normal loads of 10 N and 20 N at a sliding velocity of 1.5 m/s with a constant sliding distance of 3000 m. Microwave treated coatings obtained homogeneous structure and metallurgical bonding with improved hardness. Fused coatings revealed better wear resistance due to formation of oxides and fatigue spalling mechanism. © 2020, Springer Nature Switzerland AG.Item Phase evolution and high-temperature wear behavior of non-equiatomic metastable CoCrNiTiMox HEA coatings fabricated by high-velocity oxy-fuel technique(Elsevier Ltd, 2023) Addepalli, S.N.; Joladarashi, S.; Ramesh, M.R.The current research aims to enhance the tribological performance of maraging steels at high temperatures by surface modification techniques. CoCrNiTiMox (x; molar fraction, x = 0.5, 1.5) high-entropy alloy (HEA) coatings with dense lamellar microstructures were deposited onto maraging steels using high-velocity oxy-fuel spray (HVOF). In order to achieve a uniform distribution of constituent elements for thermal spray deposition, mechanical alloying was employed to synthesize the HEA feedstock. The phases and microstructure of the synthesized HEA powder, as-sprayed coatings, and worn surfaces were examined using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The as-sprayed HEA coatings exhibited metastability, with a BCC phase solid solution, NiTiO3 spinel, and an intermetallic MoNi phase for CoCrNiTiMo0.5 and Co2Mo3 phase for CoCrNiTiMo1.5. The average microhardness of CoCrNiTiMo0.5 and CoCrNiTiMo1.5 HEA coatings were 841 ± 62 HV0.3 and 952 ± 23 HV0.3, respectively. The specific wear rate and friction coefficients of CoCrNiTiMox HEA coatings exhibited a decreasing trend with an increase in temperature, owing to the formation of tribofilms on the worn surface. X-ray diffraction studies revealed the formation of NiMoO4 spinel for CoCrNiTiMo0.5 and MoO2, Co3O4 phases for CoCrNiTiMo1.5 HEA at a wear temperature of 600 °C. The investigation of worn surfaces showed a transformation in wear mechanisms from abrasive wear at room temperature to oxidative wear with mild fatigue at elevated temperatures. © 2023 Elsevier LtdItem Effect of temperature on wear and friction performance of WC-Co and Cr3C2 reinforced with 17-4PH Fe-based composite coatings(Springer Science and Business Media Deutschland GmbH, 2024) Chandramouli, T.V.; Joladarashi, S.; Ramesh, M.R.; Rahman, M.R.Surface protection is crucial in industrial equipment and tools to prevent wear and friction in harsh environments, particularly at high temperatures, where anti-friction coatings are essential for optimal performance. The present research investigates the tribological properties of high-velocity oxy-fuel sprayed coatings of 17-4PH stainless steel reinforced with tungsten carbide and chromium carbide powders. The coatings are deposited onto a maraging steel substrate. A dry sliding wear test was performed using an alumina ball as a counter body under various test temperatures (25 °C, 300 °C, and 600 °C) and loads (10 N and 30 N). The coating is characterized by employing SEM, XRD, micro-hardness tester, particle analyzer, and bond strength tester, and the mechanism of wear reduction was discussed. The post-wear analysis was carried out on the wear track using SEM/EDS and 3D non-contact optical profilometers. The micro-hardness and bond strength of both (17-4PH-30%WC-Co and 17-4PH-30%Cr3C2) coatings are compared. The test results revealed that at all temperatures and loads, 17-4PH-30%WC-Co coating shows better wear resistance and lower friction coefficient than the 17-4PH-30%Cr3C2 coating. The significant influence of the tribo-oxide layer at high temperatures, which contributed to decreasing wear rate and coefficient of friction, was premeditated. © 2023, International Institute of Welding.Item Elevated temperature tribological performance of non-equiatomic CoCrNiTiWx high entropy alloy coatings developed by mechanical alloying and high-velocity oxy-fuel spray(Elsevier B.V., 2024) Addepalli, S.N.; Joladarashi, S.; Ramesh, M.R.High entropy alloys (HEA) have applications in multiple fields owing to their exceptional mechanical and physical properties. In the current study, mechanical alloyed CoCrNiTiWx (x; a molar fraction, x = 0.5 and 1.5) HEA feedstock powders were deposited on maraging steel substrate using high-velocity oxy-fuel spray (HVOF). The phase evolution and the microstructure of the milled powders and as-sprayed coatings were analysed by X-ray diffraction (XRD) and scanning electron microscope (SEM). The tribological behaviour of CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings at elevated temperatures was studied extensively using a Pin-on-Disc tribometer. The CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings retained the BCC solid solution phases formed during the milling stage. However, additional oxide and intermetallic phases were formed owing to the in-flight oxidation and high temperatures experienced during the HVOF deposition. The deposited coatings exhibited a lamellar structure and good mechanical bonding with the substrate. The porosities of CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings were found to be 1.69 ± 0.32 % and 1.51 ± 0.37 % respectively.Consequently, the CoCrNiTiW0.5 and CoCrNiTiW1.5 HEA coatings displayed average microhardness values of 863 ± 52 HV0.3 and 1025 ± 39 HV0.3, respectively. Further, the wear rates of coatings exhibited a significant reduction at elevated temperatures, owing to the formation of TiO2, NiCr2O4 oxide tribofilms for CoCrNiTiW0.5, and CoCr2O4, NiWO4, WO3 oxides for CoCrNiTiW1.5. The specific wear rate of CoCrNiTiW0.5 HEA coating dropped by 73.6 % from 22.7 ± 2.6 × 10−6 mm3/N-m to 5.99 ± 1.9 × 10−6 mm3/N-m, while CoCrNiTiW1.5 dropped by 78.8 % from 11.86 ± 3.5 × 10−6 mm3/N-m to 2.51 ± 1.5 × 10−6 mm3/N-m, with a rise in the temperature from RT to 600 °C. Likewise, The frictional coefficients of CoCrNiTiW0.5 HEA dropped from 0.504 ± 0.015 to 0.397 ± 0.005, while CoCrNiTiW1.5 HEA dropped from 0.578 ± 0.025 to 0.471 ± 0.004, with a rise in temperature from RT to 600 °C. At room temperature, the wear mechanisms of the as-sprayed CoCrNiTiWx coatings were dominated by adhesive wear. However, at elevated temperatures, a shift towards oxidative wear was observed. © 2023 Elsevier B.V.Item Microstructure, Mechanical Properties, and Tribological Properties of Fe-Based Composite Coatings Reinforced with WC-Co and Cr3C2(Springer, 2025) Chandramouli, T.V.; Joladarashi, S.; Ramesh, M.R.; Rahman, M.R.Fe-based (stainless steel 316L) coatings are widely employed in the aerospace, chemical processing, petrochemical, and marine industries owing to their low and stable price, excellent corrosion resistance, and durability. However, at elevated temperatures, their performance is limited due to wear. Thus, the current investigation incorporates tungsten carbide (WC-Co) and chromium carbide (Cr3C2) into the Fe-based coating to enhance its wear resistance at high temperatures. SS316L reinforced by 30% of WC-Co and Cr3C2 by mechanical mixture, then sprayed using high-velocity oxy fuel spraying method. Coating characteristics, such as microstructures and phase analysis, were measured using FESEM/EDS and XRD. Coating density, microhardness, and bond strength were examined by water immersion, Vickers indentation, and ASTM C-633 methods, respectively. A ball-on-disk tribometer was employed to conduct wear examination at various temperatures (25, 300, and 600 °C) and loads (10 and 30 N) against the alumina counter body. The wear rate and friction coefficient of SS316L-30%WC-Co decrease from 25 to 600 °C, while the wear rate of SS316L-30%Cr3C2 increases with temperature up to 300 °C and then decreases at 600 °C. The oxide phase adheres strongly to underlying surfaces forming a protective layer (Cr2O3, NiWO4, Fe2O3, and NiMO4), changing the mode of wear mechanism. At higher temperatures and loads, the coating exhibited oxidation modified adhesive wear, and coatings provide excellent wear resistance along with reduction in friction. This research provides a novel approach for future standardization and evaluation of coatings on metal alloys for industrial applications. © ASM International 2024.