Faculty Publications
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Item Influence of microwave hybrid heating on the sliding wear behaviour of HVOF sprayed CoMoCrSi coating(Institute of Physics Publishing helen.craven@iop.org, 2018) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.CoMoCrSi superalloy powder (Tribaloy-T400) consists of intermetallic laves phase and primary eutectic phase of Co-rich solid solution. Processing of Tribaloy-T400 powder is carried out through high-energy ball milling (HEBM) technique to obtain a higher volume fraction of intermetallic laves phases. The feedstock is sprayed using high-velocity-oxy-fuel (HVOF) process on titanium grade-15 substrate. The coating microstructure is homogenized by microwave hybrid heating technique. Characterization of feedstock, as-sprayed and microwave fused coatings is done by using Scanning Electron Microscopy (SEM), Energy dispersive spectroscopy (EDS) and x-ray Diffraction (XRD). Porosity, surface roughness, microhardness, and bond strength are measured. Adhesive wear behavior of the coatings under the dry sliding condition is evaluated at an applied load of l0 and 20 N and temperature of 200, 400 and 600 °C Fused coating exhibit higher wear resistance than the as-sprayed coatings and substrate. The hard intermetallic laves phases which are amorphous (bulk metallic glass) in nature strengthen the coating at high temperatures. © 2018 IOP Publishing Ltd.Item Tribological behaviour of monolayer and multilayer Ti-based thin solid films deposited on alloy steel(Institute of Physics Publishing helen.craven@iop.org, 2019) V Badiger, P.V.; Desai, V.; Ramesh, M.R.; Joladarashi, S.; Gourkar, H.The fretting wear and adhesive wear resistance of Ti-based thin solid films deposited on MDN121 steel substrate are evaluated. Plasma-assisted cathodic arc evaporation technique is used to develop the TiC-C monolayer coating and Ti/TiN/TiCN/TiN/TiCN multilayer coatings used in the study. FESEM-EDS, nanoindentation, Raman spectroscopy, optical profiler, and confocal microscope are used to characterise the coatings and wear tracks. Diamond-like carbon is observed in the microstructure of both the coatings. During the fretting analysis, the coefficient of friction (COF) is reduced by 68.49% in the case of the TiC-C monolayer coating and 42.46% in the Ti multilayer coatings as compared to the substrate. The volumetric wear loss of the TiC-C monolayer coating is lower than the multilayer coating. The wear surface morphology reveals the abrasive form of the fretting wear mechanism in both the monolayer and multilayer coatings whereas the galling failure in the substrate. During adhesive wear, the COF is reduced by 71.73% in the monolayer coating and 59.33% in the multilayer coatings compared to the substrate. The monolayer coating exhibits low friction and low wear rate as compared to the multilayer coating. © 2018 IOP Publishing Ltd.Item Effect of microwave heating on microstructure and elevated temperature adhesive wear behavior of HVOF deposited CoMoCrSi-Cr3C2 coating(Elsevier B.V., 2019) Prasad, C.D.; Joladarashi, S.; Ramesh, M.R.; Srinath, M.S.; Channabasappa, B.H.This research reports the improvement of high-temperature sliding wear resistance of a grade 15 titanium alloy protected by an HVOF sprayed CoMoCrSi-Cr3C2 coating. The coatings have been tested in as-sprayed condition and after a post-deposition microwave heating step. The powder feedstock has been manufactured by high energy ball milling. X-ray diffraction (XRD) and Scanning Electron Microscopy (SEM) equipped with the Energy Dispersive Spectroscopy (EDS) methods were used for coatings characterization. Surface roughness, microhardness, adhesion strength, and porosity of coatings were also measured. The wear test was conducted at an applied load of l0 N and 20 N with varying temperatures of 200 °C, 400 °C, and 600 °C under dry sliding conditions. Co3Mo2Si, Co7Mo6, Mo3Si, Co3Mo, and Co2Mo3 were the intermetallic laves phases generated in the CoMoCrSi feedstock during HEBM process. The microwave-fused coating exhibited metallurgical bonding, homogeneous structure, less porosity, and greater hardness as compared to as-sprayed coating. Microwave-treated coating revealed better wear property than an as-sprayed coating. This was mainly due to the intermetallic formation and metallurgical bonding in coatings. The fused coatings exhibit tribo-oxide layers during sliding action which was the main phenomenon of improving the wear resistance of the fused composite coatings. © 2019 Elsevier B.V.Item An experimental study on adhesion, flexibility, interlaminar shear strength, and damage mechanism of jute/rubber-based flexible “green” composite(SAGE Publications Ltd, 2022) Mahesh, V.; Joladarashi, S.; Kulkarni, S.M.Determining the interlaminar shear strength (ILSS) of the composite laminates is vital for deciding their usage in any engineering applications. The matrix used and its curing characteristics are vital in deciding the ILSS of the composite. Present work deals with an experimental study on adhesive behavior, degree of flexibility, ILSS, and damage mechanism of the novel jute/rubber-based flexible “green” composite. The proposed flexible composites were prepared in three different stacking sequences, namely jute/rubber/jute (JRJ), jute/rubber/rubber/jute (JRRJ), and jute/rubber/jute/rubber/jute (JRJRJ), using compression molding technique. After determining the optimal curing characteristics of the proposed rubber-based matrix, the constituents are tested for their adhesive strength with the matrix which showed that rubber matrix system is compatible with jute fabric and natural rubber sheet. Composites are prepared and degree of flexibility for each stacking sequence is found out. Results pertaining to ILSS show that JRJRJ has better ILSS compared to JRJ and JRRJ. Fractographic analysis using scanning electron microscope reveals the mode of failure of the composites and the mechanism governing their failure. Fourier transform infrared spectroscopic study reveals the bonding between the constituents is good enough to be used in composites with flexibility. © The Author(s) 2019.Item Microstructure, Mechanical Properties, and Tribological Properties of Fe-Based Composite Coatings Reinforced with WC-Co and Cr3C2(Springer, 2025) Chandramouli, T.V.; Joladarashi, S.; Ramesh, M.R.; Rahman, M.R.Fe-based (stainless steel 316L) coatings are widely employed in the aerospace, chemical processing, petrochemical, and marine industries owing to their low and stable price, excellent corrosion resistance, and durability. However, at elevated temperatures, their performance is limited due to wear. Thus, the current investigation incorporates tungsten carbide (WC-Co) and chromium carbide (Cr3C2) into the Fe-based coating to enhance its wear resistance at high temperatures. SS316L reinforced by 30% of WC-Co and Cr3C2 by mechanical mixture, then sprayed using high-velocity oxy fuel spraying method. Coating characteristics, such as microstructures and phase analysis, were measured using FESEM/EDS and XRD. Coating density, microhardness, and bond strength were examined by water immersion, Vickers indentation, and ASTM C-633 methods, respectively. A ball-on-disk tribometer was employed to conduct wear examination at various temperatures (25, 300, and 600 °C) and loads (10 and 30 N) against the alumina counter body. The wear rate and friction coefficient of SS316L-30%WC-Co decrease from 25 to 600 °C, while the wear rate of SS316L-30%Cr3C2 increases with temperature up to 300 °C and then decreases at 600 °C. The oxide phase adheres strongly to underlying surfaces forming a protective layer (Cr2O3, NiWO4, Fe2O3, and NiMO4), changing the mode of wear mechanism. At higher temperatures and loads, the coating exhibited oxidation modified adhesive wear, and coatings provide excellent wear resistance along with reduction in friction. This research provides a novel approach for future standardization and evaluation of coatings on metal alloys for industrial applications. © ASM International 2024.Item Surface enhancement of SS304 for high-temperature wear resistance using laser cladded Mo-alloyed stellite 6 coatings(Elsevier B.V., 2025) Aprameya, C.R.; Joladarashi, S.; Ramesh, M.R.Severe wear often limits the high-temperature durability of SS304 components, necessitating the development of surface-engineered solutions. In this investigation, Mo-reinforced Stellite 6 claddings were developed using Laser Directed Energy Deposition (L-DED) to provide enhanced surface protection. Claddings with (3, 6, and 9 wt%) Mo reinforcement enhanced hardness by 2.9, 3.1, and 3.3 times, respectively, compared to the SS304 substrate. This improvement is attributed to Mo-induced solid solution strengthening and the formation of hard intermetallic phases. Dry sliding wear tests were conducted at RT and 600 °C under (10 and 20 N) loads. Wear characterisation of the clads was performed using OM, XRD, FE-SEM, EDX, and Raman spectroscopy. At RT, claddings primarily exhibited abrasive wear with minor plastic deformation. However, at 600 °C, the wear mechanism evolved into a combination of severe adhesive, oxidative, abrasive, and plastic deformation modes, with oxidative wear governing the tribological behavior. Stellite 6 with 9 wt% Mo clads exhibited better tribological performance than the other two variants, owing to the development of oxide glaze layers of Cr2O3, NiO, CoO2, and Co3O4. Enhanced performance of the claddings is attributed to solid solution strengthening, Cr-rich carbide formation, increased dislocation density, and the L-DED technology enabling refined microstructure and strong metallurgical bonding. These findings highlight the potential for further advancements in Mo-reinforced Stellite 6 L-DED claddings for high-temperature wear applications. © 2025 Elsevier B.V.