Faculty Publications
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Item Effect of Equal Channel Angular Pressing on Properties Evaluation of Biodegradable Mg-Zn-Mn Alloy(Springer Science and Business Media Deutschland GmbH, 2021) Ramesh, S.; Kumar, G.; Jagadeesh, C.; Anne, G.; Shivananda Nayaka, H.Equal channel angular pressing (ECAP) was used to process Mg-4Zn-1Mn alloy at 300 °C using route Bc up to 4 pass with a cumulative strain of 3.2. Optical microscope (OM), microstructures results shows homogenized sample grain size was 260 µm, after 4 pass ECAP grain size was decreased to 6 µm. Electron back-scattered diffraction (EBSD) shows the misorientation angle converted from low-angle grain boundaries (LAGB) to high-angle grain boundaries (HAGB). Dislocation density and fine grains were observed from transmission electron microscope (TEM) images. Strength has been increased from 156 to 218 MPa and hardness increased to 68 Hv after 4 pass of ECAP. Fractography analysis revealed that dimple size decreases as ECAP passes increased. XRD analysis shows the peak broadening and intensity variation, because of grain refinement. The corrosion behavior of the homogenized and ECAP-processed samples were investigated by electrochemical tests using simulated body fluids (SBF) at 37 ± 1 °C. The lower corrosion resistance of ECAP-processed Mg-4Zn-1Mn alloy attributed to the strain-induced crystalline defects, subgrain boundaries and high-density dislocations. Enhanced strength and ductility combined with lower corrosion resistance of ECAP-processed Mg-4Zn-1Mn has greater potentials for biomedical implants. © 2021, The Author(s), under exclusive licence to Springer Nature Switzerland AG.Item Effect of Multi-directional Forging on the Evolution of Microstructural and Mechanical Properties of Lightweight Al-Cu-Li Alloy AA2050(Springer, 2023) Jagadeesh, C.; Shivananda Nayaka, H.S.; Ramesh, S.; Praveen, T.R.Microstructural evolution and the mechanical properties of recently developed lightweight AA2050 Al-Cu-Li alloy have been presented. A processing route of multi-directional forging (MDF) at 170 °C followed by artificial aging at 150 °C was employed. Systematic EBSD analysis revealed significant grain refinement with grain size reducing from 74.3 ± 12 to 22.1 ± 2.8 µm after 12 passes of MDF. Transformation of deformation bands into subgrains with dynamic recrystallization has led to grain refinement. TEM results show the presence of large dislocation clusters and deformation bands in MDF processed samples with a large number of fine precipitates in peak aged MDF processed samples. XRD analysis shows variation in peak intensities and occurrence of peak shifts due to induced lattice strain upon MDF. A substantial increase in microhardness and strength was observed with a minor trade-off with ductility after 12th MDF pass. Further, enhancement in strengths and microhardness were observed in post-MDF aged samples. Experimental results show the combined effect of strain hardening, grain size reduction, and precipitate hardening which influence the material strength. A combination of MDF and artificial aging has shown great potential to enhance the strength and ductility of AA2050. © 2023, ASM International.Item Enhancing surface characteristics of Mg-Zn-Sr alloy through cryo-ball burnishing; modeling and experimentation(Korean Society of Mechanical Engineers, 2024) Kudva, S.A.; Anne, G.; Ramesh, S.; Sharma, P.; Jagadeesh, C.; Ritti, L.; Naik, G.M.; Divya Deepak, G.D.In this investigation, the impact of the cryo-ball burnishing process on both the mechanical and corrosion properties of the Mg-4Zn-1Sr alloy was systematically explored. To better understand the plastic deformation occurring in Mg-4Zn-1Sr during cryo-burnishing, a finite element analysis (FEA) model was developed. The microstructure of cryo-ball burnished samples underwent characterization through scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffractometry (XRD), and surface properties were assessed using atomic force microscopy (AFM). Additionally, electrochemical impedance spectroscopy and potentiodynamic polarization tests were conducted in a simulated body fluid using an electrochemical workstation. Experimental findings revealed significant grain refinement and the presence of residual dislocations during the cryo-burnishing process, as evident in TEM analysis. XRD analysis indicated the presence of Mg, Mg17Sr2 and SrZn2 phases, with observable peak broadening in the cryo-burnished samples, attributed to structural refinement and lattice strain incorporation. Microhardness values increased with greater depth of press, with the DFN 1071 sample displaying a hardness of 80 ± 4 Hv (Ra = 1.853 µm), marking a 54 % improvement compared to the homogenized sample. The enhanced corrosion resistance of the Mg-4Zn-1Sr alloy due to cryo-burnishing is attributed to the combined effects of grain refinement, residual dislocations, and intermetallic phases. © The Korean Society of Mechanical Engineers and Springer-Verlag GmbH Germany, part of Springer Nature 2024.Item On the microstructure, texture and electrochemical properties of severely deformed and artificially aged lightweight AA2050 Al-Cu-Li alloy(Institute of Physics, 2024) Jagadeesh, C.; Shivananda Nayaka, H.; Sekar, P.; Ramesh, S.; Anne, G.Lightweight 3rd generation Al-Cu-Li alloy AA2050 was severely deformed via Multi Axial Forging (MAF) at 170 °C followed by artificial aging at 150 °C. Effect of MAF and post MAF aging on microstructure and precipitation was investigated using transmission electron microscopy (TEM). Formation of deformation bands and large dislocation cells were evident on MAF processed samples. Post MAF peak aging resulted in the distribution of fine T1 precipitates in grain interiors with reduction in grain boundary precipitation. Bulk texture studies reveal the formation of strong Goss and S texture components upon MAF processing. Further, low temperature artificial aging doesn’t exhibit significant changes in texture characteristics, either in terms of texture intensities or texture components. Polarization studies showed that peak aged samples exhibited better corrosion resistance compared to un-aged samples. Overall, 12 pass MAF processed and peak aged samples showed higher corrosion resistance. Further, corrosion surface morphologies examination revealed the change in corrosion mechanisms with thermomechanical treatments. Improved corrosion resistance after MAF and peak aging widens the requirements in aerospace and aircraft applications for such engineering alloys. © 2024 The Author(s). Published by IOP Publishing Ltd.Item Reciprocating wear behavior of multi-directionally forged and aged Al-Cu-Li alloy(Institute of Physics, 2024) Jagadeesh, C.; Shivananda Nayaka, H.; Ramesh, S.; Anne, G.Al-Cu-Li alloys have drawn attention because of their decreased density, which is a result of the growing need for lightweight material systems in aerospace and aircraft applications. The alloy was subjected to multi-directional forging (MDF) and post-MDF artificial aging. Reciprocating sliding wear tests were conducted to investigate the effects of these processes on wear properties under different load conditions. After MDF, a decrease in wear resistance was noticed, on the other hand, 12 pass MDF treated samples showed improved wear resistance upon aging treatment. Wear scars and counter ball surfaces were examined using scanning electron microscope (SEM) to understand the wear mechanism and wear mode. The findings demonstrated that, at lower loads, adhesion and abrasion were the main wear processes; at greater loads, delamination, adhesion, and abrasion were clearly visible. The study revealed that the MDF and subsequent aging have a substantial effect on the wear behavior of Al-Cu-Li alloy and is an effective thermomechanical processing route to enhance wear resistance. © 2024 The Author(s). Published by IOP Publishing Ltd