Faculty Publications
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Item Mechanical Properties and Microstructural Characteristics of Friction Stir Welded Aluminium Matrix Composite(Springer Nature, 2021) Subramanya, B.; Shettigar, A.; Herbert, M.A.; Rao, S.S.Nowadays, friction stir welding process appears a promising technique to weld difficult materials by conventional welding techniques. Present study aims to analyse the significance of process variables on the mechanical behaviour of aluminium matrix composite joined by friction stir welding (FSW) technique. FSW is carried out at different welding conditions using conventional threaded cylindrical tool (TC). Microstructural study indicates several tiny reinforced particles are uniformly distributed in the nugget region. Recrystallization and grin refinement are observed in the weld area. Nugget region exhibits higher hardness compared to the base material. Joint efficiency of up to 89% is obtained for the FS-welded composite. The fracture surface reveals that the matrix undergoes a ductile fracture whereas reinforced particles exhibit brittle fracture. © 2021, Springer Nature Singapore Pte Ltd.Item Study on Mechanical and microstructural characteristics of Friction Stir Welded Aluminium Matrix composite(Elsevier Ltd, 2020) Prabhu B, S.R.B.; Shettigar, A.K.; Herbert, M.A.; Rao, S.S.Aluminium matrix composites (AMCs) are part of advanced materials, possesses capabilities to serve the present industrial needs due to its superior properties. Potential use of these AMCs in a particular application is limited if it is unable to join properly. In the present study AMCs are prepared by stir casting technique and welded by friction stir welding (FSW) process. FSW is performed using combined threaded and square profiled pin (CTSP). Further the welded joints were examined for microstructure and joint strength. Tensile test indicates that joint efficiency of 97 % is obtained, normal to the weld direction. Compare to the base material the nugget zone of weld region shows higher hardness. The microstructural study reveals that uniform distribution of finer grains are visible at nugget zone. © 2018 Elsevier Ltd.Item Experimental investigation of joint properties of friction stir welded aluminium matrix composite(Elsevier Ltd, 2021) Prabhu B, S.R.; Shettigar, A.; Herbert, M.A.; Rao, S.S.The present study is focused on welding of particulate aluminium matrix composites using friction stir welding process and investigating the influence of various process variables on the joint properties. The microstructural study and mechanical behaviors such as tensile strength and hardness of the weld zone were measured. Microstructural studies showed that process variables play pivotal role in refinement of grains. Compared to the top of the weld region, smaller grains were formed at the bottom due to variation in the heating effect. Measurement of the tensile strength and hardness of the weld zone, indicated that process variables plays important role in controlling the joint properties. Beyond the optimum range of process variables, the joint strength of welded part deteriorates due to the insufficient stirring and lack of plasticization leads to defect formation. Joint welded with traverse speed of 100 mm/min and revolution speed of 1200 rpm exhibited better mechanical properties. © 2021 Elsevier Ltd. All rights reserved.Item A study of microstructure and mechanical properties of friction stir welded joint of Al-Ce-Si-Mg aluminium alloy plates and optimization cum prediction techniques using Taguchi and ANN(Elsevier Ltd, 2023) D’Souza, A.D.; Rao, S.S.; Herbert, M.A.In the current research work, the effect of friction stir welding (FSW) on joint strength and evolution of microstructure at the weld zone of the friction stir welded of Al-Ce-Si-Mg aluminium alloy (Al10Mg8Ce3.5Si and Al5Mg8Ce3.5Si) is studied. The experimentations demonstrated that the speed of tool revolution, contour of tool pin and tool movement rate have influence on the quality of the FSW joint of the alloy. It was noticed that the size of grains at nugget zone (NZ) depends upon the speed of tool spin, speed, of tool feed, tool pin contour and composition of the aluminium alloy. The grain size at the bottom of the NZ was discovered to be reducing when compared to that at the top of the NZ. It was also noted that highest hardness was reached at NZ. Lowest hardness was found at heat affected zone (HAZ) and most of the tensile specimens fractured at HAZ. The Taguchi orthogonal array-based design has demonstrated that the tool pin contour had the greatest influence in enhancing the joint strength, followed by speed of tool feed, material composition and speed of tool spin. A speed of revolution of tool of 1000 rpm, tool movement rate of 20 mm/min, triangular contour pin (TCP) tool and Al10Mg8Ce3.5Si aluminium alloy were concluded as the optimum variables of the process. The percentage contribution of each one of these input process parameters on optimum output quality characteristics was also found out and noticed to be lying well within the confidence interval of 95% suggested by the Taguchi design. The current study has shown that the prediction results with artificial neural network (ANN) are better compared to those predicted using statistical methods like Taguchi Techniques. © © 2023 Elsevier Ltd. All rights reserved.Item Correlation of Tribological Properties with Microstructure and Mechanical Properties of Graphite Cast Irons Centrifugally Cast for Engine Liner(Springer India sanjiv.goswami@springer.co.in, 2014) Desai Gowda, H.S.; Mukunda, P.G.; Herbert, M.A.This is a study of the influence of centrifugal process on the graphite morphology, mechanical and wear properties on flake graphite iron (FGI), spheroidal graphite iron (SGI) and compacted graphite iron (CGI). Melts of hypereutectic and almost of identical composition with or without melt treatment were centrifugally cast. The microstructure, mechanical and wear properties of these specimens were studied. In the microstructure for FG iron it has been observed that the centrifugal process produces flake size range class 2–3 (range 160–320 ?m) and graphite of flake type A by about 67.9 % (field %) and combined flakes of type B, C, D and E will be of 32.1 % (field %). While SGI has been observed to have 96.1 % nodules and 330.0 nodules per square millimeter. Similarly CGI has been seen to produce 52.0 % nodules and 113 nodules per square millimeter. SGI possess the highest tensile strength, rupture strain and hardness of 604 N/mm2, 6.1 %, 233 BHN respectively. Whereas FGI possess the least tensile strength, rupture strain and hardness of 303 N/mm2, 0.65 %, 185 BHN respectively among the irons. CGI has a tensile strength, rupture strain and hardness of 369 N/mm2, 1.2 % and 200 BHN respectively which lies in between those of FGI and SGI. During the wear test similar materials for both disk and pin combination show higher co-efficient of friction and wear rate than those for dissimilar material combinations. SGI disk and FGI pin combination show least wear. This combination would be ideally suited for engine liner and piston rings. © 2014, Indian Institute of Metals.Item Microstructure and hardness of friction stir welded aluminium-copper matrix-based composite reinforced with 10 wt-% SiCp(Maney Publishing, 2014) Shettigar, A.; Veeresh Nayak, C.; Herbert, M.A.; Rao, S.S.In the present work, an attempt has been made to join aluminium-copper matrix-based composite reinforced with 10 wt-% SiCp, by the friction stir welding technique, at different combinations of tool rotational speed (710, 1000 and 1400 rev mm1) and welding speed (50, 63 and 80 mm min1) using square profiled friction stir welding tool. Welding parameters play a predominant role in improving the mechanical strength by minimising the defects. A good number of defect free joints were obtained at various combinations of rotational speed and welding speed. It has been observed that, rotational speed and welding speed have strong influence on microstructure, Vickers hardness and quality of welds. © W. S. Maney &Son Ltd 2014.Item Microstructure and mechanical properties of rutile-reinforced AA6061 matrix composites produced via stir casting process(Nonferrous Metals Society of China B12 Fuxing Road Beijing 100814, 2019) Prabhu B, S.R.; Shettigar, A.K.; Herbert, M.A.; Rao, S.S.A novel process of fabricating aluminium matrix composites (AMCs) with requisite properties by dispersing rutile particles in the aluminum matrix was studied. A novel bi-stage stir casting method was employed to prepare composites, by varying the mass fractions of the rutile particles as 1%, 2%, 3% and 4% in AA6061 matrix. The density, tensile strength, hardness and microstructures of composites were investigated. Bi-stage stir casting method engendered AMCs with uniform distribution of the reinforced rutile particles in the AA6061 matrix. This was confirmed by the enhancement of the properties of AMCs over the parent base material. Rutile-reinforced AMCs exhibited higher tensile strength and hardness as compared with unreinforced parent material. The properties of the composites were enhanced with the increase in the mass fraction of the rutile particles. However, beyond 3 wt.% of rutile particles, the tensile strength decreased. The hardness and tensile strength of the AMCs reinforced with 3 wt.% of rutile were improved by 36% and 14% respectively in comparison with those of matrix alone. © 2019 The Nonferrous Metals Society of ChinaItem Evaluation of Microstructure, Hardness and Mechanical Properties of Friction Stir Welded Al–Ce–Si–Mg Aluminium Alloy(Korean Institute of Metals and Materials, 2020) D’Souza, A.D.; Rao, S.S.; Herbert, M.A.Abstract: A vast majority of the research on friction stir welding(FSW) is mainly focused on welding of aluminium alloys. The research studies in this paper are based on one such alloy known as Al–Ce–Si–Mg aluminium alloy, of which, the microstructure and other mechanical properties of the friction stir welded joints are yet to be studied. The plates of Al–Ce–Si–Mg aluminium alloy were friction stir welded using a non consumable, rotating tool with triangular profile pin and circular shoulder, with different combinations of tool rotation speeds and weld speeds. The microstructure, hardness and mechanical properties of the weld were analyzed. The microstructure of the weld zones revealed that, the average grain size at the bottom of the Nugget Zone (NZ) is 5 ± 0.12 ?m and gradually increases to 15 ± 0.23 ?m at the top of the NZ. In the TMAZ the grain size is 20 ± 0.14 ?m and is bigger compared to the NZ. In the HAZ, the grain size is around 37 ± 0.21 ?m and is bigger than that in the TMAZ. The maximum Vickers hardness value at the NZ center is 231.9 ± 2 Hv, and uniformly reduces to 100 ± 2.4 Hv in the TMAZ and 65 ± 1.3 Hv in the HAZ and then increases to 98 ± 1 Hv in the base material (BM). The maximum ultimate tensile strength (UTS) of FSW joint was found to be around 102.55 ± 3 MPa with elongation at fracture of 2.5%. The BM UTS was 154 ± 4.5 MPa. For a tool rotation speed of 800RPM and a weld speed of 20 mm/min a maximum joint efficiency of 67%. was obtained. Hence these were chosen as the optimum process parameters to join the alloy Al–Ce–Si–Mg by FSW. Graphic Abstract: [Figure not available: see fulltext.] © 2019, The Korean Institute of Metals and Materials.Item Effect of zirconium oxide particulate composites with Al-Si on the microstructural and mechanical properties of hot pressed, spray forming and stir casting methods(Taylor and Francis Ltd., 2023) Patil, I.S.; Anarghya, A.; Rao, S.S.; Herbert, M.A.; Kushwaha, R.This research work aims to investigate the aluminum and silicon alloy reinforced with the ZrO2 powder particles, which has been fabricated using stir casting and spray deposition method. The mechanical properties, micro hardness and microstructure of the developed metal matrix composite is investigated. The microstructural results indicate that the rich interface among the AlSi-ZrO2 particles and depicts the agglomeration of reinforced phase resulting to poor wettability of ZrO2 and observed decohesion. The mechanical testing results indicate that the tensile strength increases with the percentage of ZrO2. Moreover, as cast composites exhibit reverse tendency in compressive and hardness values. The highest compressive values for as cast and hot-pressed composites were 380 MPa and 337 MPa for 10% ZrO2. The highest tensile strength of 191.83 MPa was obtained for 5% ZrO2 as cast composite and 164 MPa for 15% ZrO2 hot pressed composite. It is to note that as cast composite method represented more homogenous data compared to the hot-pressed composites. Hot pressed samples exhibited the reduction in the porosity compared to the as cast. The developed method proved to be accurate, reduced time and efficient to predict the numerous samples. © 2021 Engineers Australia.Item Investigation of the effect of process parameters on the mechanical properties of friction stir additive manufactured (FSAM) AA8090 alloy(Elsevier B.V., 2025) D A P, P.; Shettigar, A.K.; Herbert, M.A.; Korgal, A.; Adiga, K.Friction Stir Additive Manufacturing (FSAM), an emerging technique, falls under the category of sheet lamination additive manufacturing. It employs a layer-by-layer fabrication where all the plates should be flat and of the same size. This process was developed to fabricate near-net-shaped components and refined microstructures. FSAM has been extensively used in the fabrication of aluminum alloys for aerospace applications. In this work, FSAM has been carried out for AA8090 aluminum alloy. AA8090 is the second-generation Al-Li alloy with 2.3 % Li, lightweight, 10 % lower density and 11 % higher modulus than the existing commercial 2014 and 2024 Al alloy. The experiments were carried out at rotational speed (1000 – 2000 rpm), traverse speed (45–55 mm/min) and 1° constant tilt angle. The macrostructure and microstructure analysis were carried out. This was followed by microhardness and tensile test analysis. The microhardness was carried out at nine points on each layer and tensile specimen was made according to ASTM E8 standard. The maximum reduction in grain size, which is 62 %, maximum hardness value 113 HV and maximum tensile value 346.8 MPa were observed at 2000 rpm. The size of the grains decreased from the top layer into the bottom layers. The maximum hardness for all the experiments was observed in the re-stir zone of the specimens. It was concluded that with increase in process parameters, better mechanical and microstructural properties can be achieved. The fractography analysis showed the presence of dimples and tear ridges indicating a ductile fracture. © © 2025. Published by Elsevier B.V.