Faculty Publications

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    Processing of cenosphere/HDPE syntactic foams using an industrial scale polymer injection molding machine
    (Elsevier Ltd, 2016) Bharath Kumar, B.R.; Doddamani, M.R.; Zeltmann, S.E.; Gupta, N.; Ramesh, M.R.; Ramakrishna, S.
    Rapid production of high quality components is the key to cost reduction in industrial applications. The present work is the first attempt of manufacturing syntactic foams, hollow particle filled lightweight composites, using an industrial scale injection molding machine. High density polyethylene (HDPE) is used as the matrix material and fly ash cenospheres are used as the filler. Development of syntactic foams with cenospheres serves dual purpose of beneficial utilization of industrial waste fly ash and reduction in the cost of the component. The pressure and temperature used in the injection molding process are optimized to minimize fracture of cenospheres and obtain complete mixing of cenospheres with HDPE. The optimized parameters are used for manufacturing syntactic foams with 20, 40 and 60 wt.% cenospheres. With increasing cenosphere content, density and strength reduce and modulus increases. Surface modification of constituents results in rise in strength with increasing filler content. A theoretical model based on a differential scheme is used to estimate the properties of cenospheres by conducting parametric studies because of inherent difficulties in direct measurement of cenosphere properties. The potential for using the optimized injection molding process is demonstrated by casting several industrial components. © 2015 Elsevier Ltd.
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    Wear response of walnut-shell-reinforced epoxy composites
    (ASTM International, 2017) Doddamani, M.; Parande, G.; Manakari, V.; Siddhalingeshwar, I.G.; Gaitonde, V.N.; Gupta, N.
    Present work utilizes agricultural by-product, walnut shell, as reinforcing filler in epoxy matrix for investigating dry sliding wear behavior using a pin-on disc wear-testing machine. Effects of sliding velocity (0.5-1.5 m/s), normal load (10-50 N), sliding distance (1000-3000 m) and filler content (10-30 wt. %) on wear rate (Wt), specific wear rate (Ws) and coefficient of friction (?) are investigated. The experiments were planned as per design of the experiments scheme and the wear characteristics were analyzed through response surface modeling (RSM) method. The lowest Wt of 1.1 mm3/km was noted for 1.5 m/s sliding velocity with 30-wt. % filler content. Sliding distance did not have a significant influence on Ws above a critical load of 40 N. The minimum ? was observed at 1-m/s sliding velocity, 40-N load, 1000-m sliding distance, and 30-wt. % filler. Lower values of Wt and ? at higher walnut-shell loadings support feasibility of using such composites in wear-prone applications. The wear mechanism was determined in the composites using extensive scanning electron microscopic observations. © © 2017 by ASTM International.
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    Development of glass microballoon/HDPE syntactic foams by compression molding
    (Elsevier Ltd, 2017) Jayavardhan, M.L.; Bharath Kumar, B.R.; Doddamani, M.; Singh, A.K.; Zeltmann, S.E.; Gupta, N.
    Thermoplastic resins are widely used in consumer products and industrial components. There is a significant interest in weight reduction of many of those components. Although glass hollow particle filled lightweight syntactic foams with thermoset matrices have been studied in detail, studies on thermoplastic syntactic foams are scarce. The present study is focused on developing a compression molding based processing method for glass microballoon/high density polyethylene (GMB/HDPE) syntactic foams and studying their mechanical properties to develop structure-property correlations. Blending of GMB in HDPE is carried out using a Brabender mixer with processing parameters optimized for minimal filler breakage. Flexural and tensile test specimens are compression molded with 20, 40 and 60 vol% of GMB. Particle fracture increases with increasing GMB content due to increased particle to particle interaction during processing. Additionally, increasing wall thickness makes GMBs stronger and results in reduced particle fracture. Flexural modulus increases while strength decreases with increasing filler content. Tensile strength decreases with increasing filler content, while tensile modulus is relatively unchanged. GMB volume fraction has a more prominent effect than the wall thickness on the mechanical properties of syntactic foams. Specific moduli of GMB/HDPE foams are superior while specific strength is comparable to neat HDPE. © 2017 Elsevier Ltd
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    Hole Quality Assessment in Drilling of Glass Microballoon/Epoxy Syntactic Foams
    (Minerals, Metals and Materials Society 184 Thorn Hill Road Warrendale PA 15086, 2018) Ashrith, H.S.; Doddamani, M.; Gaitonde, V.; Gupta, N.
    Syntactic foams reinforced with glass microballoons are used as alternatives for conventional materials in structural application of aircrafts and automobiles due to their unique properties such as light weight, high compressive strength, and low moisture absorption. Drilling is the most commonly used process of making holes for assembling structural components. In the present investigation, grey relation analysis (GRA) is used to optimize cutting speed, feed, drill diameter, and filler content to minimize cylindricity, circularity error, and damage factor. Experiments based on full factorial design are conducted using a vertical computer numerical control machine and tungsten carbide twist drills. GRA reveals that a combination of lower cutting speed, filler content, and drill diameter produces a good quality hole at optimum intermediate feed in drilling syntactic foams composites. GRA also shows that the drill diameter has a significant effect on the hole quality. Furthermore, damage on the hole exit side is analyzed using a scanning electron microscope. © 2018, The Minerals, Metals & Materials Society.
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    Effect of cenosphere filler surface treatment on the erosion behavior of epoxy matrix syntactic foams
    (John Wiley and Sons Inc. cs-journals@wiley.com, 2019) Shahapurkar, K.; Doddamani, M.; Mohan Kumar, G.C.; Gupta, N.
    Influence of cenosphere surface modification and volume fraction on the solid particle erosion of cenosphere/epoxy syntactic foams is investigated. Fly ash cenospheres are used as filler in both as received and silane surface modified configurations. Erosion behavior is studied at room temperature for different impact angles (30, 45, 60, and 90°) and velocities (30, 45, and 60 m/s). Neat epoxy shows the highest erosion rate compared with that of the syntactic foams. Results show a strong dependence of impact angle and velocity on erosion rate of syntactic foams. With increasing cenosphere content erosion rate decreases for all impact angles. Erosion rate decreases with increasing impact angle and with decreasing velocity. Good interfacial bonding of treated cenospheres enhances the erosion resistance. All the samples exhibit ductile erosive behavior, with maximum erosion at 30°. The velocity exponent and erosion efficiency parameters confirm the ductile behavior of syntactic foams. POLYM. COMPOS., 40:2109–2118, 2019. © 2018 Society of Plastics Engineers. © 2018 Society of Plastics Engineers