Faculty Publications
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Item Microstructure and mechanical properties of magnesium alloy processed by equal channel angular pressing (ECAP)(Elsevier Ltd, 2017) Gopi, K.R.; Shivananda Nayaka, H.Equal Channel Angular Pressing (ECAP) with different passes was carried out for Mg-Al-Mn (AM) series magnesium alloy to investigate the microstructure and mechanical properties. ECAP process was carried up to 4 passes using route BC, where the samples are rotated by 90° in the same direction between consecutive passes. Microstructures were studied using optical microscope (OM) and scanning electron microscope (SEM) and it was observed that the grain size was reduced from 100 μm to 1 μm after 4 passes. Tensile test was conducted and the ultimate tensile strength (UTS) increased up to 2 passes but decreased with higher passes, even though grain size became finer with increase in ECAP passes. Microhardness was carried out and it was observed that the hardness was increased up to 2 passes of ECAP and decreased with higher passes. © 2017 Elsevier Ltd.Item Influence of Multi Axial Forging (MAF) on Microstructure and Mechanical Properties of Cu-Ti Alloy(Elsevier Ltd, 2018) Ramesh, S.; Shivananda Nayaka, H.S.; Gopi, K.R.Multi axial forging (MAF) is one among the severe plastic deformation (SPD) processes, where large strains are imposed into the component. In the present work, as-received Cu-1.5%Ti alloy was subjected to MAF for 2 and 4 cycles at room temperature. Microstructure showed grain refinement after 2 and 4 cycles. Average grain size obtained for MAF processed samples after 2 and 4 cycles are 120 μm and 40 μm, respectively compared to initial grain size of 800 μm. The Mechanical properties were analyzed for as-received and MAF processed samples. Tensile test showed increased ultimate tensile strength (493 MPa) for MAF 4-cycle sample compared to as-received (191 MPa) condition with accumulated strain of 2.18 for 4 cycles. Increase in hardness was observed for MAF processed sample of 143 Hv for 4-cycle compared to as-received sample of 67 Hv. © 2018 Elsevier Ltd.Item Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2016) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.Magnesium alloy Mg-Al-Mn (AM70) was processed by equal channel angular pressing (ECAP) at 275 °C for up to 4 passes in order to produce ultrafine-grained microstructure and improve its mechanical properties. ECAP-processed samples were characterized for microstructural analysis using optical microscopy, scanning electron microscopy, and transmission electron microscopy. Microstructural analysis showed that, with an increase in the number of ECAP passes, grains refined and grain size reduced from an average of 45 to 1 µm. Electron backscatter diffraction analysis showed the transition from low angle grain boundaries to high angle grain boundaries in ECAP 4 pass sample as compared to as-cast sample. The strength and hardness values an showed increasing trend for the initial 2 passes of ECAP processing and then started decreasing with further increase in the number of ECAP passes, even though the grain size continued to decrease in all the successive ECAP passes. However, the strength and hardness values still remained quite high when compared to the initial condition. This behavior was found to be correlated with texture modification in the material as a result of ECAP processing. © 2016, ASM International.Item Microstructural Evolution and Strengthening of AM90 Magnesium Alloy Processed by ECAP(Springer Verlag, 2017) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.Equal-channel angular pressing (ECAP) was applied on AM90 magnesium alloy using processing route B C at 275?C up to four passes. Microstructural evolution and the corresponding modification in mechanical properties (strength, elongation and hardness) corresponding to the number of ECAP passes were evaluated using X-ray diffraction (XRD), electron backscatter diffraction, scanning electron microscopy, transmission electron microscopy, tensile test and microhardness test. Shear deformation was found to refine the microstructure by breaking it into smaller grains formed by dislocation reconstruction. Tensile strength and hardness were found to increase by ? 128 and 23%, respectively, for ECAP-processed 2-pass sample in comparison with that of the homogenized condition. After two passes, tensile strength and hardness started decreasing even though the grain size was still decreasing, which was found to be associated with texture modification during ECAP processing as observed by XRD analysis. © 2017, King Fahd University of Petroleum & Minerals.Item Investigation of microstructure and mechanical properties of the Cu-3% Ti alloy processed by multiaxial cryo-forging(Cambridge University Press, 2018) Ramesh, S.; Shivananda Nayaka, H.; Gopi, K.R.; Sahu, S.; Kuruveri, U.B.A Cu-3%Ti (wt%) alloy was processed by multiaxial forging (MAF) at cryogenic temperature up to 3 cycles, imposing a total strain of 1.6. Microstructure and mechanical properties of the unprocessed and cryo-forged samples were analyzed. X-ray diffraction results showed deviation in peak broadening and peak intensity of the cryo-forged samples in comparison to that of unprocessed, which are due to texture modification caused by grain refinement during the MAF process. Microstructural analysis showed reduction in grain size from 80 m in the as-received condition to 250 nm after 3 cycles. Electron backscatter diffraction results indicated the transformation of high angle grain boundaries to low angle grain boundaries in all 3 cycles when compared to the as-received condition. Reduction in ductility was observed after 1 cycle, but with an increase in the number of cycles, both strength and ductility increased. After 3 cycles, ultimate tensile strength and hardness reached 1126 MPa and 427 Hv as compared to 528 MPa and 224 Hv for the as-received condition. Fractography analysis showed decrement in dimple size after 1 cycle, in comparison to that of the as-received condition. However, it kept on increasing for higher number of cycles. © © Materials Research Society 2018.Item Effect of multiaxial cryoforging on microstructure and mechanical properties of a Cu-Ti Alloy(Institute of Physics Publishing helen.craven@iop.org, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Gopi, K.R.; Sahu, S.Cu-Ti alloy, processed by multiaxial forging (MAF) at cryogenic temperature with a cumulative strain up to 1.64, was investigated for microstructure and mechanical properties. The deformed microstructures were analyzed using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The average grain size of 2 ?m was achieved in the deformed sample after 3 cycles of MAF. TEM studies indicated that the shear bands width of the deformed sample after 3 cycles reduced to 1 ?m. Tests for mechanical properties indicated an increase in tensile strength and hardness and it was found to be correlated with an increase in dislocation density and grain boundary strengthening mechanism. Ultimate tensile strength (UTS) of 390 MPa, 480 MPa, and 590 MPa was observed in MAF processed samples after 1, 2, and 3 cycles, respectively. Hardness increased from 65 Hv (as-received) to 240 Hv after 3 cycles of MAF. Fractography analysis showed that, with an increase in number of MAF cycles, dimple size reduced up to 1 cycle and percentage elongation increased after 2 cycles of MAF. © 2018 IOP Publishing Ltd.Item Influence of Multiaxial Cryoforging on Microstructural, Mechanical, and Corrosion Properties of Copper-Titanium Alloy(Springer, 2019) Ramesh, S.; Shivananda Nayaka, H.S.; Sahu, S.; Gopi, K.R.; Shivaram, M.J.; Arya, S.Multiaxial forging (MAF) was used to process Cu-4.5%Ti (wt.%) alloy at cryogenic temperature up to three cycles with a cumulative strain of 1.64. Microstructures, mechanical, and corrosion properties of as-received and deformed samples were analyzed. Microstructural analysis showed that average grain size decreased from 70 µm to 200 nm, and electron backscattered diffraction (EBSD) analysis revealed the transformation of high-angle grain boundaries (HAGBs) to low-angle grain boundaries (LAGBs). Variations in intensity of peaks were observed by x-ray diffraction (XRD) technique. Microstructural investigation showed elongated grains with shear bands having width ~ 200 nm for 3-cycle sample. Tensile testing and micro-hardness tests showed improvements in ultimate tensile strength (UTS), yield strength (YS), and micro-hardness, with the increase in MAF cycles. Ultimate tensile strength and hardness increased from 605 MPa and 252 HV (for as-received) to 1284 MPa and 428 HV for three cycles of MAF-processed sample, respectively. Improvement in strength and hardness was attributed to refined grain structure. Corrosion study was carried out for different cycles of MAF-processed samples using potentiodynamic polarization, and corroded surfaces were analyzed using scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS) analysis. © 2019, ASM International.
