Faculty Publications
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Item Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2016) Gopi, K.R.; Shivananda Nayaka, H.S.; Sahu, S.Magnesium alloy Mg-Al-Mn (AM70) was processed by equal channel angular pressing (ECAP) at 275 °C for up to 4 passes in order to produce ultrafine-grained microstructure and improve its mechanical properties. ECAP-processed samples were characterized for microstructural analysis using optical microscopy, scanning electron microscopy, and transmission electron microscopy. Microstructural analysis showed that, with an increase in the number of ECAP passes, grains refined and grain size reduced from an average of 45 to 1 µm. Electron backscatter diffraction analysis showed the transition from low angle grain boundaries to high angle grain boundaries in ECAP 4 pass sample as compared to as-cast sample. The strength and hardness values an showed increasing trend for the initial 2 passes of ECAP processing and then started decreasing with further increase in the number of ECAP passes, even though the grain size continued to decrease in all the successive ECAP passes. However, the strength and hardness values still remained quite high when compared to the initial condition. This behavior was found to be correlated with texture modification in the material as a result of ECAP processing. © 2016, ASM International.Item Tribological and corrosion properties of AM70 magnesium alloy processed by equal channel angular pressing(Cambridge University Press, 2017) Gopi, K.R.; Shivananda Nayaka, H.Wear and corrosion properties of AM70 magnesium alloy subjected to equal channel angular pressing (ECAP) were investigated using pin-on-disc dry sliding wear test and electrochemical impedance spectroscopy (EIS), respectively. Wear test was conducted with 30 and 40 N loads with sliding distance of 5000 m and at a constant speed of 3 m/s. Reduced coefficient of friction (COF) and wear mass loss of ECAP processed samples showed increased wear resistance. Worn surface analysis by scanning electron microscope (SEM) showed the presence of delamination, wear debris, and plowing. Energy dispersive X-ray spectrometer (EDS) revealed the occurrence of oxidation, and the wear mechanism was identified as abrasion and oxidation wear. EIS plots showed the improvement in corrosion resistance of ECAP processed magnesium alloy compared to initial condition due to grain refinement and homogeneous distribution of secondary particles. © Materials Research Society 2017.Item Wear Properties of ECAP-Processed AM80 Magnesium Alloy(Springer New York LLC barbara.b.bertram@gsk.com, 2017) Gopi, K.R.; Shivananda Nayaka, H.; Sahu, S.AM80 magnesium alloy was subjected to equal-channel angular pressing (ECAP), and microstructural evolution was studied using scanning electron microscope (SEM). Grain size was found to decrease up to 3 µm after four passes. An increase in number of ECAP passes led to a corresponding increase in hardness of the processed samples. Unprocessed and ECAP-processed samples were subjected to wear test using pin-on-disk wear test machine to study the wear behavior. Effects of varying loads (30 and 40 N) with sliding distances (2500 and 5000 m) were studied. The results showed reduction in wear mass loss for the ECAP-processed samples in comparison with unprocessed condition. Coefficient of friction (COF) was studied for different loads, and improvement in COF values was observed for ECAP-processed samples compared to unprocessed condition. Worn surfaces were studied using SEM and energy-dispersive x-ray spectrometer, and they exhibited plastic deformation, delamination, plowing, wear debris and oxidation in the sliding direction. X-ray diffraction analysis was conducted on the worn surfaces to identify the phases. It revealed the presence of magnesium oxide and magnesium aluminum oxide which led to oxidation wear in the sliding direction. Wear mechanism was found to be abrasive and oxidation wear. © 2017, ASM International.Item Corrosion Behavior of ECAP-Processed AM90 Magnesium Alloy(Springer Verlag, 2018) Gopi, K.R.; Shivananda Nayaka, H.; Sahu, S.Magnesium AM90 alloy was subjected to equal-channel angular pressing (ECAP) using route B C. Microstructural characterization revealed refined grains having average grain size ?3?m after ECAP 4 passes. Samples were subjected to electrochemical measurements to study the corrosion behavior. Potentiodynamic polarization test showed reduced corrosion current density (Icorr) for processed samples up to ECAP 3 pass due to grain refinement. Electrochemical impedance spectroscopy showed an increase in the diameter of the capacitive arcs and charge-transfer resistance (Rt) for ECAP-processed 3 pass sample indicating the reduction in corrosion rate. Increase in corrosion resistance is due to refined microstructure and uniform distribution of secondary particles forming a protective passivation layer (Mg (OH) 2) on the sample’s surface. Immersion test indicated lower hydrogen evolution from ECAP-processed samples compared to the unprocessed condition indicating decreased corrosion rate. © 2018, King Fahd University of Petroleum & Minerals.Item Strength enhancement of magnesium alloy through equal channel angular pressing and laser shock peening(Elsevier B.V., 2020) Praveen, T.R.; Shivananda Nayaka, H.; Swaroop, S.; Gopi, K.R.AM80 magnesium alloy was processed by Equal Channel Angular Pressing up to 2 passes under route BC and C, to study the effect of change in microstructure. Microstructures were examined under optical microscope. Samples processed by route BC showed heterogeneous grain structure with good tensile strength compared to that processed by route C. Tensile tests of 2-pass equal channel angular pressed samples showed high tensile strength under route BC. Laser shock peening without coating was carried out on route BC sample for further grain refinement on the surface. Laser pulses with power density of 8 GW cm?2, under different percentages of cover, were used to peen the surface at high strain rate. Microstructures were analysed through scanning and transmission electron microscope, and fine grains of less than 100 nm were observed. Tensile tests indicated that the laser shock peened samples had increased strength and ductility. Fracture details from tensile tested specimens, were examined under SEM. Mixed mode of brittle and ductile fractures was observed in ECAP processed samples. Fracture surface of Laser shock peening without coating treated on equal channel angular pressed samples showed small dimples near the peened surface and intensity of dimples increased with increase in percentage of cover. Wear test was carried out on before and after Laser shock peening without coating processed samples, on pin-on-disc wear test machine. Increase in friction coefficients and wear rate was observed due to roughness induced by peening effect and it decreased after increase in sliding distance due to increase in hardness. Nano indentation experiments were carried out to examine the mechanical characterization at nano level, and it expose the effect of LSPwC in terms of increase in hardness at peened region. © 2020