Faculty Publications
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Item Compressive and flexural properties of functionally graded fly ash cenosphere-epoxy resin syntactic foams(John Wiley and Sons Inc, 2015) Doddamani, M.; Kishore; Shunmugasamy, V.C.; Gupta, N.; Vijayakumar, H.B.The present study focuses on developing functionally graded syntactic foams (FGSFs) based on a layered co-curing technique. The FGSFs were characterized for compressive and flexural properties and compared with plain syntactic foams. The results showed that the specific compressive modulus was 3-67% higher in FGSFs compared to plain syntactic foams. FGSF exhibited 5-34% and 34-87% higher specific modulus and strength, respectively in flexural mode. The microscopic examinations of comparative responses of the filler and matrix to deformation suggest that the failure is dominated by the matrix. The gradient in the composition of syntactic foams helps in effectively distributing the stress throughout the microstructure and results in improved mechanical performance of syntactic foams. From the microscopy studies, it is evident that, the failure mechanism in the FGSF under flexural loading is governed by a crack that initiated on the tensile side of the specimen and propagated through the thickness to cause complete fracture. The microscopic observations further clearly demonstrate the existence of seamless interfaces between the layers and a clear difference in the cenosphere concentration across the interface, affirming the gradation in the prepared samples. The results show that appropriate compositions of FGSFs can be selected to develop materials with improved mechanical performance. © 2014 Society of Plastics Engineers.Item Dry sliding wear of epoxy/cenosphere syntactic foams(Elsevier Ltd, 2015) Manakari, V.; Parande, G.; Doddamani, M.; Gaitonde, V.N.; Siddhalingeshwar, I.G.; Kishore; Shunmugasamy, V.C.; Gupta, N.Abstract Dry sliding wear behavior of epoxy matrix syntactic foams filled with 20, 40 and 60 wt% fly ash cenosphere is reported based on response surface methodology. Empirical models are constructed and validated based on analysis of variance. Results show that syntactic foams have higher wear resistance than the matrix resin. Among the parameters studied, the applied normal load (F) had a prominent effect on wear rate, specific wear rate (ws) and coefficient of friction (?). With increasing F, the wear rate increased, whereas ws and ? decreased. With increase in filler content, the wear rate and ws decreased, while the ? increased. With increase in sliding velocity as well as sliding distance, the wear rate and ws show decreasing trends. Microscopy revealed broken cenospheres forming debris and extensive deformation marks on the wear surface. © 2015 Elsevier Ltd.Item Enhancing the ignition, hardness and compressive response of magnesium by reinforcing with hollow glass microballoons(MDPI AG Postfach Basel CH-4005, 2017) Manakari, V.; Parande, G.; Doddamani, M.; Gupta, M.Magnesium (Mg)/glass microballoons (GMB) metal matrix syntactic foams (1.47-1.67 g/cc) were synthesized using a disintegrated melt deposition (DMD) processing route. Such syntactic foams are of great interest to the scientific community as potential candidate materials for the ever-changing demands in automotive, aerospace, and marine sectors. The synthesized composites were evaluated for their microstructural, thermal, and compressive properties. Results showed that microhardness and the dimensional stability of pure Mg increased with increasing GMB content. The ignition response of these foams was enhanced by -22 °C with a 25 wt % GMB addition to the Mg matrix. The authors of this work propose a new parameter, ignition factor, to quantify the superior ignition performance that the developed Mg foams exhibit. The room temperature compressive strengths of pure Mg increased with the addition of GMB particles, with Mg-25 wt % GMB exhibiting the maximum compressive yield strength (CYS) of 161 MPa and an ultimate compressive strength (UCS) of 232 MPa for a GMB addition of 5 wt % in Mg. A maximum failure strain of 37.7% was realized in Mg-25 wt % GMB foam. The addition of GMB particles significantly enhanced the energy absorption by -200% prior to compressive failure for highest filler loading, as compared to pure Mg. Finally, microstructural changes in Mg owing to the presence of hollow GMB particles were elaborately discussed. © 2017 by the authors. Licensee MDPI, Basel, Switzerland.Item Development of glass microballoon/HDPE syntactic foams by compression molding(Elsevier Ltd, 2017) Jayavardhan, M.L.; Bharath Kumar, B.R.; Doddamani, M.; Singh, A.K.; Zeltmann, S.E.; Gupta, N.Thermoplastic resins are widely used in consumer products and industrial components. There is a significant interest in weight reduction of many of those components. Although glass hollow particle filled lightweight syntactic foams with thermoset matrices have been studied in detail, studies on thermoplastic syntactic foams are scarce. The present study is focused on developing a compression molding based processing method for glass microballoon/high density polyethylene (GMB/HDPE) syntactic foams and studying their mechanical properties to develop structure-property correlations. Blending of GMB in HDPE is carried out using a Brabender mixer with processing parameters optimized for minimal filler breakage. Flexural and tensile test specimens are compression molded with 20, 40 and 60 vol% of GMB. Particle fracture increases with increasing GMB content due to increased particle to particle interaction during processing. Additionally, increasing wall thickness makes GMBs stronger and results in reduced particle fracture. Flexural modulus increases while strength decreases with increasing filler content. Tensile strength decreases with increasing filler content, while tensile modulus is relatively unchanged. GMB volume fraction has a more prominent effect than the wall thickness on the mechanical properties of syntactic foams. Specific moduli of GMB/HDPE foams are superior while specific strength is comparable to neat HDPE. © 2017 Elsevier LtdItem Compressive behavior of cenosphere/epoxy syntactic foams in arctic conditions(Elsevier Ltd, 2018) Shahapurkar, K.; Garcia, C.D.; Doddamani, M.; Mohan Kumar, G.C.; Prabhakar, P.In this paper, the effects of arctic condition on the compressive response of ceno-sphere/epoxy syntactic foams are investigated. Understanding the behavior of such foams under extreme conditions is critical for exploring their suitability for constructing lightweight platforms used in arctic explorations, which are exposed to subzero temperatures for extended periods of time potentially degrading their mechanical properties. In the research study presented here, samples of cenosphere/epoxy syntactic foams were conditioned under arctic environment at a temperature of ?60 °C for a period of 57 days. Compression tests were then conducted at room temperature as well as in-situ ?60 °C on the conditioned samples and compared against unconditioned samples tested at room temperature. Combinations of surface modification and cenosphere volume fractions were considered. For the case of unconditioned samples, compressive strength decreased with increasing cenosphere volume fraction for both surface modified and unmodified cenospheres. For the arctic conditioned samples, cenospheres/epoxy foams did not present visible signs of degradation prior to testing, but manifested a reduction in compressive modulus in a range of 47–57% and 47–65% for untreated and treated cenospheres/epoxy syntactic foams as compared to their unconditioned counterparts. On the other hand, the compressive strength increased in a range between 32–68% for untreated and 59–80% for treated cenosphere foams in arctic environment, which can be attributed to the matrix hardening introduced by frigid in-situ environment. Also, under in-situ arctic compressive loading, the post peak response for all foam types have shifted from a progressive failure to a brittle type behavior. © 2017 Elsevier LtdItem Additive Manufacturing of Syntactic Foams: Part 2: Specimen Printing and Mechanical Property Characterization(Minerals, Metals and Materials Society 184 Thorn Hill Road Warrendale PA 15086, 2018) Singh, A.K.; Saltonstall, B.; Patil, B.; Hoffmann, N.; Doddamani, M.; Gupta, N.High-density polyethylene (HDPE) and its fly ash cenosphere-filled syntactic foam filaments have been recently developed. These filaments are used for three-dimensional (3D) printing using a commercial printer. The developed syntactic foam filament (HDPE40) contains 40 wt.% cenospheres in the HDPE matrix. Printing parameters for HDPE and HDPE40 were optimized for use in widely available commercial printers, and specimens were three-dimensionally (3D) printed for tensile testing at strain rate of 10?3 s?1. Process optimization resulted in smooth operation of the 3D printer without nozzle clogging or cenosphere fracture during the printing process. Characterization results revealed that the tensile modulus values of 3D-printed HDPE and HDPE40 specimens were higher than those of injection-molded specimens, while the tensile strength was comparable, but the fracture strain and density were lower. © 2018, The Minerals, Metals & Materials Society.Item Additive Manufacturing of Syntactic Foams: Part 1: Development, Properties, and Recycling Potential of Filaments(Minerals, Metals and Materials Society 184 Thorn Hill Road Warrendale PA 15086, 2018) Singh, A.K.; Patil, B.; Hoffmann, N.; Saltonstall, B.; Doddamani, M.; Gupta, N.This work focuses on developing filaments of high-density polyethylene (HDPE) and their hollow particle-filled syntactic foams for commercial three-dimensional (3D) printers based on fused filament fabrication technology. Hollow fly-ash cenospheres were blended by 40 wt.% in a HDPE matrix to produce syntactic foam (HDPE40) filaments. Further, the recycling potential was studied by pelletizing the filaments again to extrude twice (2×) and three times (3×). The filaments were tensile tested at 10?4 s?1, 10?3 s?1, and 10?2 s?1 strain rates. HDPE40 filaments show an increasing trend in modulus and strength with the strain rate. Higher density and modulus were noticed for 2× filaments compared to 1× filaments because of the crushing of some cenospheres in the extrusion cycle. However, 2× and 3× filament densities are nearly the same, showing potential for recycling them. The filaments show better properties than the same materials processed by conventional injection molding. Micro-CT scans show a uniform dispersion of cenospheres in all filaments. © 2018, The Minerals, Metals & Materials Society.Item Hole Quality Assessment in Drilling of Glass Microballoon/Epoxy Syntactic Foams(Minerals, Metals and Materials Society 184 Thorn Hill Road Warrendale PA 15086, 2018) Ashrith, H.S.; Doddamani, M.; Gaitonde, V.; Gupta, N.Syntactic foams reinforced with glass microballoons are used as alternatives for conventional materials in structural application of aircrafts and automobiles due to their unique properties such as light weight, high compressive strength, and low moisture absorption. Drilling is the most commonly used process of making holes for assembling structural components. In the present investigation, grey relation analysis (GRA) is used to optimize cutting speed, feed, drill diameter, and filler content to minimize cylindricity, circularity error, and damage factor. Experiments based on full factorial design are conducted using a vertical computer numerical control machine and tungsten carbide twist drills. GRA reveals that a combination of lower cutting speed, filler content, and drill diameter produces a good quality hole at optimum intermediate feed in drilling syntactic foams composites. GRA also shows that the drill diameter has a significant effect on the hole quality. Furthermore, damage on the hole exit side is analyzed using a scanning electron microscope. © 2018, The Minerals, Metals & Materials Society.Item Influence of axial compressive loads on buckling and free vibration response of surface-modified fly ash cenosphere/epoxy syntactic foams(SAGE Publications Ltd info@sagepub.co.uk, 2018) Waddar, S.; Jeyaraj, P.; Doddamani, M.This work deals with experimental buckling and free vibration behavior of silane-treated cenosphere/epoxy syntactic foams subjected to axial compression. Critical buckling loads are computed from compressive load–deflection plots deduced using universal testing machine. Further, compressive loads are applied in the fixed intervals until critical loading point on different set of samples having similar filler loadings to estimate natural frequency associated with the first three transverse bending modes. Increasing filler content increases critical buckling load and natural frequency of syntactic foam composites. Increasing axial compressive load reduce structural stiffness of all the samples under investigation. Syntactic foams registered higher stiffness compared to neat epoxy for all the test loads. Similar observations are noted in case of untreated cenosphere/epoxy foam composites. Silane-modified cenosphere embedded in epoxy matrix registered superior performance (rise in critical buckling load and natural frequencies to the tune of 23.75% and 11.46%, respectively) as compared to untreated ones. Experimental results are compared with the analytical solutions that are derived based on Euler–Bernoulli hypothesis and results are found to be in good agreement. Finally, property map of buckling load as a function of density is presented by extracting values from the available literature. © The Author(s) 2018.Item Snap-through buckling of fly ash cenosphere/epoxy syntactic foams under thermal environment(Elsevier Ltd, 2018) Waddar, S.; Jeyaraj, P.; Doddamani, M.Experimental investigation on deflection behaviour of fly ash cenosphere/epoxy syntactic foam at room temperature and under thermal environment (three different heating conditions) is investigated. Influence of fly ash cenosphere volume fraction and nature of temperature variation on deflection behaviour of syntactic foam beam is discussed elaborately. Results reveal that the syntactic foam beam experience snap-through buckling under thermal environment and is reflected by two bifurcation points in temperature-deflection plot. It is observed that the time duration for which the foam beam stays in the first buckled position increases with increase in cenosphere content. Thermal environment induces compressive stresses in the samples causing such snap-through buckling. However, such phenomenon is not observed when mechanical compressive loads are applied under room temperature conditions. Temperature variation across the beam strongly influences snap-through buckling in syntactic foams in addition to volume fraction of filler content. © 2018 Elsevier Ltd
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