Faculty Publications

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Author: search.filters.author.Doddamani, M.Subject: search.filters.subject.Fillers

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    Wear response of walnut-shell-reinforced epoxy composites
    (ASTM International, 2017) Doddamani, M.; Parande, G.; Manakari, V.; Siddhalingeshwar, I.G.; Gaitonde, V.N.; Gupta, N.
    Present work utilizes agricultural by-product, walnut shell, as reinforcing filler in epoxy matrix for investigating dry sliding wear behavior using a pin-on disc wear-testing machine. Effects of sliding velocity (0.5-1.5 m/s), normal load (10-50 N), sliding distance (1000-3000 m) and filler content (10-30 wt. %) on wear rate (Wt), specific wear rate (Ws) and coefficient of friction (?) are investigated. The experiments were planned as per design of the experiments scheme and the wear characteristics were analyzed through response surface modeling (RSM) method. The lowest Wt of 1.1 mm3/km was noted for 1.5 m/s sliding velocity with 30-wt. % filler content. Sliding distance did not have a significant influence on Ws above a critical load of 40 N. The minimum ? was observed at 1-m/s sliding velocity, 40-N load, 1000-m sliding distance, and 30-wt. % filler. Lower values of Wt and ? at higher walnut-shell loadings support feasibility of using such composites in wear-prone applications. The wear mechanism was determined in the composites using extensive scanning electron microscopic observations. © © 2017 by ASTM International.
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    Development of glass microballoon/HDPE syntactic foams by compression molding
    (Elsevier Ltd, 2017) Jayavardhan, M.L.; Bharath Kumar, B.R.; Doddamani, M.; Singh, A.K.; Zeltmann, S.E.; Gupta, N.
    Thermoplastic resins are widely used in consumer products and industrial components. There is a significant interest in weight reduction of many of those components. Although glass hollow particle filled lightweight syntactic foams with thermoset matrices have been studied in detail, studies on thermoplastic syntactic foams are scarce. The present study is focused on developing a compression molding based processing method for glass microballoon/high density polyethylene (GMB/HDPE) syntactic foams and studying their mechanical properties to develop structure-property correlations. Blending of GMB in HDPE is carried out using a Brabender mixer with processing parameters optimized for minimal filler breakage. Flexural and tensile test specimens are compression molded with 20, 40 and 60 vol% of GMB. Particle fracture increases with increasing GMB content due to increased particle to particle interaction during processing. Additionally, increasing wall thickness makes GMBs stronger and results in reduced particle fracture. Flexural modulus increases while strength decreases with increasing filler content. Tensile strength decreases with increasing filler content, while tensile modulus is relatively unchanged. GMB volume fraction has a more prominent effect than the wall thickness on the mechanical properties of syntactic foams. Specific moduli of GMB/HDPE foams are superior while specific strength is comparable to neat HDPE. © 2017 Elsevier Ltd
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    Hole Quality Assessment in Drilling of Glass Microballoon/Epoxy Syntactic Foams
    (Minerals, Metals and Materials Society 184 Thorn Hill Road Warrendale PA 15086, 2018) Ashrith, H.S.; Doddamani, M.; Gaitonde, V.; Gupta, N.
    Syntactic foams reinforced with glass microballoons are used as alternatives for conventional materials in structural application of aircrafts and automobiles due to their unique properties such as light weight, high compressive strength, and low moisture absorption. Drilling is the most commonly used process of making holes for assembling structural components. In the present investigation, grey relation analysis (GRA) is used to optimize cutting speed, feed, drill diameter, and filler content to minimize cylindricity, circularity error, and damage factor. Experiments based on full factorial design are conducted using a vertical computer numerical control machine and tungsten carbide twist drills. GRA reveals that a combination of lower cutting speed, filler content, and drill diameter produces a good quality hole at optimum intermediate feed in drilling syntactic foams composites. GRA also shows that the drill diameter has a significant effect on the hole quality. Furthermore, damage on the hole exit side is analyzed using a scanning electron microscope. © 2018, The Minerals, Metals & Materials Society.
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    Influence of axial compressive loads on buckling and free vibration response of surface-modified fly ash cenosphere/epoxy syntactic foams
    (SAGE Publications Ltd info@sagepub.co.uk, 2018) Waddar, S.; Jeyaraj, P.; Doddamani, M.
    This work deals with experimental buckling and free vibration behavior of silane-treated cenosphere/epoxy syntactic foams subjected to axial compression. Critical buckling loads are computed from compressive load–deflection plots deduced using universal testing machine. Further, compressive loads are applied in the fixed intervals until critical loading point on different set of samples having similar filler loadings to estimate natural frequency associated with the first three transverse bending modes. Increasing filler content increases critical buckling load and natural frequency of syntactic foam composites. Increasing axial compressive load reduce structural stiffness of all the samples under investigation. Syntactic foams registered higher stiffness compared to neat epoxy for all the test loads. Similar observations are noted in case of untreated cenosphere/epoxy foam composites. Silane-modified cenosphere embedded in epoxy matrix registered superior performance (rise in critical buckling load and natural frequencies to the tune of 23.75% and 11.46%, respectively) as compared to untreated ones. Experimental results are compared with the analytical solutions that are derived based on Euler–Bernoulli hypothesis and results are found to be in good agreement. Finally, property map of buckling load as a function of density is presented by extracting values from the available literature. © The Author(s) 2018.
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    Influence of surface modification on wear behavior of fly ash cenosphere/epoxy syntactic foam
    (Elsevier Ltd, 2018) Shahapurkar, K.; Chavan, V.B.; Doddamani, M.; Mohan Kumar, G.C.M.
    The present study deals with investigating the surface modification effect of fly ash cenosphere (as received and surface treated) on the friction and wear response of epoxy syntactic foams. Such lightweight syntactic foams have the potential in using them as tribo-materials for friction applications like in brake pad composites. This study also addresses the environmental linked disposal issues of fly ash cenospheres by incorporating them (up to 60 vol%) in the epoxy matrix. Cenosphere content and surface modification influence on the friction and wear response of cenosphere/epoxy syntactic foams is investigated against EN31 steel disc under dry sliding conditions. Wear behavior is studied at room temperature for different velocities (2 and 5 m/s), applied loads (30 and 50 N) and sliding distances (3, 5 and 7 km). Neat epoxy exhibits maximum wear rate as compared to foams. Wear rate decreases with increasing sliding distance and cenosphere content at all tested conditions. With the increase in the applied load and the sliding velocity, higher wear rate is noted for neat epoxy samples while it decreases with increasing filler loading. Surface modified cenosphere reinforced foams exhibit better wear resistance compared to as received cenosphere dispersed foams and neat epoxy for all the operating conditions owing to the good interfacial bonding of treated cenospheres with epoxy matrix. Specific wear rate decreases significantly with an increase in applied load. Further, the coefficient of friction decreases with higher filler loading and surface modifications. Scanning electron microscopy is used to study the wear mechanisms. Wear debris is analyzed and disc temperature is also reported. Finally, wear rate results are summarised and compared with the data available from literature and are presented in a property map. © 2018 Elsevier B.V.
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    Influence of microballoon wall thickness on dynamic mechanical analysis of closed cell foams
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Doddamani, M.
    Thermoplastics are most commonly used in industrial and consumer products. The growing interest in making them lightweight is always a priority in industrial practices. Investigations on thermoplastic based closed cell foams wall thickness variations for dynamic mechanical analysis (DMA), and crystallinity are scarce. The present study investigates storage modulus, loss modulus, damping, and % crystallinity as a function of glass microballoon/high-density polyethylene (GMB/HDPE) foam wall thickness and volume fraction variations. Crystallinity percentage variation in HDPE and their foams are analyzed through DSC traces. GMBs are mixed with HDPE in plasticorder, and subsequently, GMB/HDPE composite blend is compression molded. Varying wall thickness (particle density variations) GMB particles across three different volume fractions (20, 40 and 60%) are prepared. Storage modulus, loss modulus, and damping are observed to be increasing with particle wall thickness and volume fraction as compared to HDPE matrix resin. Thick walled GMB particle with the highest GMB content registered enhanced storage modulus compared to thin walled ones at lower temperatures. DMA properties increase with increasing wall thickness. Damping is noted to be less sensitive than the storage and loss modulus. Crystallinity is observed to be decreasing with increasing wall thickness and GMB content. Higher crystalline phase contributes towards DMA properties at lower filler loadings while higher wall thickness plays a vital role at higher filler content. © 2020 IOP Publishing Ltd.
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    Effect of cenosphere filler surface treatment on the erosion behavior of epoxy matrix syntactic foams
    (John Wiley and Sons Inc. cs-journals@wiley.com, 2019) Shahapurkar, K.; Doddamani, M.; Mohan Kumar, G.C.; Gupta, N.
    Influence of cenosphere surface modification and volume fraction on the solid particle erosion of cenosphere/epoxy syntactic foams is investigated. Fly ash cenospheres are used as filler in both as received and silane surface modified configurations. Erosion behavior is studied at room temperature for different impact angles (30, 45, 60, and 90°) and velocities (30, 45, and 60 m/s). Neat epoxy shows the highest erosion rate compared with that of the syntactic foams. Results show a strong dependence of impact angle and velocity on erosion rate of syntactic foams. With increasing cenosphere content erosion rate decreases for all impact angles. Erosion rate decreases with increasing impact angle and with decreasing velocity. Good interfacial bonding of treated cenospheres enhances the erosion resistance. All the samples exhibit ductile erosive behavior, with maximum erosion at 30°. The velocity exponent and erosion efficiency parameters confirm the ductile behavior of syntactic foams. POLYM. COMPOS., 40:2109–2118, 2019. © 2018 Society of Plastics Engineers. © 2018 Society of Plastics Engineers
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    Wear behavior of glass microballoon based closed cell foam
    (Institute of Physics Publishing helen.craven@iop.org, 2019) Doddamani, M.
    Present work deals with dry sliding wear response of hollow glass microballoons reinforced lightweight epoxy syntactic (closed cell) foams using a pin on disc apparatus. Influence of glass microballoons content on wear behavior of hollow glass microballoons/epoxy foams in dry sliding mode is investigated. Effects of sliding velocity (1 and 3 m s-1), normal load (30-50 N), sliding distance (1 and 3 km) and glass microballoons content (20, 40 and 60 volume%) are investigated. The rate of wear declines with increasing glass microballoons content and sliding distance. Syntactic foams with perfectly spherical glass microballoons exhibit enhanced resistance to wear as compared to neat resin samples due to better constituents compatibility. Specific wear rate shows noticeably decreasing magnitude with higher applied load. Decrease in frictional coefficient is observed with higher filler loadings. Lowest wear rate of 1.6 mm3 km-1 is noted for sliding velocity and load of 3 m s-1 and 50 N respectively with 60 filler volume %. Low wear values with higher glass microballoon loadings support the feasibility of utilizing such foams in wear-prone applications in weight sensitive structures. Wear mechanisms are studied using scanning electron microscopy. Finally, property map is presented to compare the observed wear results with the existing studies available on dry sliding wear response. © 2019 IOP Publishing Ltd.
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    Eco-friendly lightweight filament synthesis and mechanical characterization of additively manufactured closed cell foams
    (Elsevier Ltd, 2019) Patil, B.; Bharath Kumar, B.R.; Bontha, S.; Balla, V.K.; Powar, S.; Hemanth Kumar, V.H.; Suresha, S.N.; Doddamani, M.
    Environmentally pollutant fly ash cenospheres (hollow microballoons) are utilized with most widely consumed, relatively expensive high density polyethylene (HDPE) for developing lightweight eco-friendly filament for 3D printing of closed cell foams. Cenospheres (20, 40 and 60 by volume %) are blended with HDPE and subsequently extruded in filament to be used for 3D printing. Cenosphere/HDPE blends are studied for melt flow index (MFI) and rheological properties. MFI decreases with cenospheres addition. Complex viscosity, storage and loss modulus increase with filler loading. DSC results on the filament and printed samples reveal increasing crystallization temperature and decreasing crystallinity % with no appreciable change in peak melting temperature. Cooling rate variations exhibit crystallinity differences between the filament and the prints. CTE decreases with increasing cenosphere content resulting in lower thermal stresses and under diffusion of raster leading to non-warped prints. Micrography on freeze fractured filament and prints show cenospheres uniform distribution in HDPE. Intact cenospheres lower the foam density making it lightweight. Tensile tests are carried out on filaments and printed samples while flexural properties are investigated for 3D prints. Cenospheres addition resulted in improved tensile modulus and decreased filament strength. Tensile and flexural modulus of printed foams increases with filler content. Results are also compared with injection molded samples. Printed foams registered comparable tensile strength. Specific tensile modulus is noted to be increased with cenospheres loading implying weight saving potential of 3D printed foams. Property map reveals printed foams advantage over other fillers and HDPE composites synthesized through injection and compression molding. © 2019 Elsevier Ltd
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    Mechanical behaviour of additively manufactured bioactive glass/high density polyethylene composites
    (Elsevier Ltd, 2020) Jeyachandran, P.; Bontha, S.; Bodhak, S.; Balla, V.K.; Kundu, B.; Doddamani, M.
    Bioactive glass (BAG) is a well-known biomaterial that can form a strong bond with hard and soft tissues and can also aid in bone regeneration. In this study, BAG is added to a polymer to induce bioactivity and to realize fused filament fabrication (FFF) based printing of polymer composites for potential orthopaedic implant applications. BAG (5, 10, and 20 wt%) is melt compounded with high density polyethylene (HDPE) and subsequently extruded into feedstock filament for FFF-printing. Tensile tests on developed filaments reveal that they are stiff enough to resist forces exerted during the printing process. Micrography of printed HDPE/BAG reveals perfect diffusion of raster interface indicating proper selection of printing parameters. Micrography of freeze fractured prints shows the homogeneous distribution and good dispersion of filler across the matrix. The tensile, flexural, and compressive modulus of FFF-printed HDPE/BAG parts increases with filler addition. BAG addition to the HDPE matrix enhances flexural and compressive strength. The tensile and flexural behaviour of FFF-prints is comparable to injection molded counterparts. Property maps exhibit the merits of present study over the existing literature pertaining to desired bone properties and polymer composites used in biomedical applications. It is envisioned that the development of HDPE/BAG composites for FFF-printing can lead to possible orthopaedic implants and scaffolds to mimic the bone properties in customised anatomical sites or injuries. © 2020 Elsevier Ltd